1065 results about "Austenite grain" patented technology

The invention relates to 700MPa high strength hot rolling Q&P steel and a manufacturing method thereof. The steel has the following chemical components in percentage by weight: 0.15-0.40% of C, 1.0-2.0% of Si, 1.5-3.0% of Mn, less than or equal to 0.015% of P, less than or equal to 0.005% of S, 0.3-1.0% of Al, less than or equal to 0.0065% of N, 0.005-0.015% of Ti and the balance of Fe. The yield strength is greater than or equal to 70MPa, the strength of extension is greater than or equal to 1300MPa, and the ductility is greater than 10%. According to the invention, through a reasonable compound design, based on common C-Mn steel components, austenite crystal is refined by micro Ti treatment by improving the content of Si to inhibit separation of cementite, so that the austenite transformation kinetics in the air cooling process is accelerated by improving the content of Al. Meanwhile, a hot continuous rolling process is matched with a sectional cooling process, so that proeutectoid ferrite+martensite+retained austenite tissues are obtained. The cost of the alloy is greatly lowered.

The invention relates to a display method used for preparing high-intensity ship plate metallographic samples and the original austenite grains, belonging to the technical field of metallographic sample preparation. The invention has the following technological steps: coarse grinding, fine grinding, polishing and corrosion; the polished specimen is put in the etching solution at 70-80 DEG C; the formula of the etching solution comprises 100ml of distilled water, 5-7g of picric acid, 0.5-1.5ml of hydrochloric acid, 3-5g of SDBS, 5-15g of Seagull paste shampoo and 0.3-1ml of hydrogen peroxide; after being etched for 1-2 minutes, the surface of the specimen is dimmed, and the specimen is taken out, cleaned with alcohol and then dried; and the relatively clear original austenite structure can be observed under a microscope. The invention has the advantages of solving the problem of different display of the high-intensity ship plate austenite grains and clearly displaying the austenite structure; besides, the invention is easy and simple to implement.

The invention relates to a controlled-forging controlled-cooling processing technology of a bearing ring prepared by GCr15, comprising the following steps of: quenching the bearing ring in cooling fluid at final forging temperature of 850-950 DEG C and at fluid outlet temperature of 350-550 DEG C; when heating the bearing ring to the temperature of 450-550 DEG C, after preserving the temperature for 1h-3h, discharging the bearing ring from a boiler and cooling the bearing ring to room temperature; when heating the bearing ring to the temperature of 650-690 DEG C again, preserving the temperature for 1h; when continuously heating the bearing ring to the temperature of 740-780 DEG C, after preserving the temperature for 2-3h, cooling the bearing ring to the temperature of 680-690 DEG C and preserving the temperature for 2-4 hours; finally, when cooling the bearing ring to the temperature of 550-600 DEG C at the speed of 10 DEG C/h, cooling o the bearing ring to the room temperature along with the boiler by air; quenching a machined semi-finished bearing ring; when heating to the temperature of 810-830 DEG C, after preserving the temperature for 45-60min, discharging the machined semi-finished bearing ring from the boiler and quenching the machined semi-finished bearing ring in oil; and when heating the machined semi-finished bearing ring to the temperature of 160-200 DEG C after being quenched, preserving the temperature of the machined semi-finished bearing ring for 4h, discharging the machined semi-finished bearing ring from the boiler and cooling the machined semi-finished bearing ring to the room temperature by air. According to the invention, carbides, martensite crystals and austenite crystals of the bearing ring are refined, network carbides are improved or eliminated and impact ductility and fatigue life are improved.

The purpose of the present invention is to provide a high strength thin steel sheet that has high hydrogen embrittlement resisting property. In order to achieve the above purpose, a high strength thin steel sheet having high hydrogen embrittlement resisting property comprises: C: 0.10 to 0.25%; Si: 1.0 to 3.0%; Mn: 1.0 to 3.5%; P: 0.15% or less; S: 0.02% or less; and Al: 1.5% or less (higher than 0%) in terms of percentage by weight, with balance of iron and inevitable impurities; and the metal structure comprises: residual austenite; 1% by area or more in proportion to the entire structure; bainitic ferrite and martensite: 80% or more in total; and ferrite and pearlite: 9% or less (may be 0%) in total, while the mean axis ratio (major axis/minor axis) of said residual austenite grains is 5 or higher, and the steel has tensile strength of 1180 MPa or higher.

The invention relates to a cold-rolled hot-galvanized dual-phase steel plate with a flanging property and a manufacturing method thereof. The steel plate comprises the following chemical components by weight percent: 0.06% to 0.095% of C, 0.3% to 0.6% of Si, 1.4% to 1.8% of Mn, greater than 0% and less than or equal to 0.02% of P, greater than 0% and less than or equal to 0.01% of S, 0.02% to 0.05% of Al, 0.35% to 0.55% of Cr, 0.02% to 0.04% of Nb, greater than 0% and less than or equal to 0.005% of N and the balance of Fe. According to the steel plate provided by the invention, the austenite is dispersedly distributed in a ferrite matrix via the refining of austenite grains by adding the Nb element and controlling temperatures during hot rolling and finish rolling and a rolling temperature; the amount of the austenite after annealing is increased by limiting the content of C and carrying out high-temperature annealing in a continuous hot-galvanized annealing furnace, so that tissues in low-C martensite are obtained after quenching. Thus, the hardness of the martensite is decreased. As a result, a hardness difference between the martensite phase and the ferrite phase is reduced.

The invention relates to an ultrahigh-strength thin steel sheet excellent in the hydrogen embrittlement resistance, the steel sheet including, by weight %, 0.10 to 0.60% of C, 1.0 to 3.0% of Si, 1.0 to 3.5% of Mn, 0.15% or less of P, 0.02% or less of S, 1.5% or less of Al, 0.003 to 2.0% of Cr, and a balance including iron and inevitable impurities; in which grains of residual austenite have an average axis ratio (major axis/minor axis) of 5 or more, the grains of the residual austenite have an average minor axis length of 1 μm or less, and the grains of the residual austenite have a nearest-neighbor distance between the grains of 1 μm or less.

The invention discloses a zinc-plated hot-formed steel plate or steel strip with excellent cold bending performance and a manufacturing method thereof. The zinc-plated hot-formed steel plate or steelstrip comprises a base plate with a surface decarburization layer thickness of 20 [mu]m or below and a zinc coating with an adhesion amount of 10-100 g/m<2> on the base plate. The constituent weight percentage of the base plate is C: 0.1-0.8%, Si: 0.05-2.0%, Mn: 0.5-3.0%, P: <=0.1%, S: <=0.05%, Al: <=0.1%, N: <=0.01%, and the balance Fe and unavoidable impurities. The average size of original austenite grains of the base plate is 15 [mu]m or below. The hot-formed steel plate or steel strip has a continuous and complete coating, no cracks extending to the base plate and excellent cold bending performance on the basis of meeting the conditions that the tensile strength of the base plate after hot-forming is 1500 MPa and the elongation after breaking is 5%.

The present invention provides a high strength steel used for spring steel that has excellent hydrogen embrittlement resistance. The high strength steel which spring steel having excellent hydrogen embrittlement resistance comprises 0.20 to 0.60% of C, 1.0 to 3.0% of Si, 1.0 to 3.5% of Mn, higher than 0% and not higher than 1.5% of Al, 0.15% or less P, 0.02% or less S, and balance of iron and inevitable impurities and the structure includes: 1% or more residual austenite; 80% or more in total of bainitic ferrite and martensite; and 10% or less (may be 0%) in total content of ferrite and pearlite in the proportion of area to the entire structure, and also the mean axis ratio (major axis/minor axis) of the residual austenite grains is 5 or higher and the steel tensile strength is 1860 MPa or higher.

The invention relates to the technical field of metallographical sample preparation and tissue observation. The invention relates to a tissue display method for ultra-supercritical steel with the advantages of high alloy content, high anti-corrosion and excellent oxidation resistance in particular. The technique steps of the method includes: firstly adopting a standard grinding-polishing method on an ultra-supercritical steel sample; then selecting a commonly used electrolyte to carry out electrolytic etching with high voltage and high current on the sample; finally combining a mechanical polishing method to finally display a clear original austenite crystal grain boundary. The invention can clearly, completely and independently display the original austenite crystal grain boundary of the ultra-supercritical steel; thereby being able to fully reflect the size and the distribution of the original austenite crystal grain and solving the problem of being harder to precisely assess the thickness and the uniformity of the ultra-supercritical steel tissue.

A metallographic corrosion method for displaying a GCr15 original austenitic grain boundary comprises adding picric acid 5g into distilled water100ml and mixing continuously, then adding sodium dodecyl benzene sulfonate 5ml 50% and mixing, finally adding ferric chloride 2g, and using after placing for 24 hours. A sample is grinded roughly, grinded finely, polished, cleared, dried, immersed into caustic erodent for 2-5 minutes according to normal method under a quenching tempering condition until etched surface is changed into silver grey, cleaned up through flowing water, cleaned with alcohol 95%, and dried. If the sample is over-corroded, polishing paste W0.5-1.0 or metallographic polishing egent0.5-1.0 is added on silk polishing cloth, the sample is polished slightly with hands, then cleaned with alcohol 95%, and dried. According to practical condition, grain granularity measurement can adopt methods of picture contrast, grid, intercept, quantitative metallography, and the like, to assess according to relevant standards.

The present invention provides an austenitic stainless steel tube with a uniform fine grained structure of regular grains, which is not changed to a coarse structure and the steam oxidation resistance is maintained even if the tube is subjected to a high temperature reheating during welding and high temperature bending working. The austenitic stainless steel tube consists of, by mass %, C: 0.03-0.12%, Si: 0.1-0.9%, Mn: 0.1-2%, Cr: 15-22%, Ni: 8-15%, Ti: 0.002-0.05%, Nb: 0.3-1.5%, sol. Al: 0.0005-0.03%, N: 0.005-0.2% and O (oxygen): 0.001-0.008%, and the balance Fe and impurities, the austenitic stainless steel tube having austenitic grain size number of 7 or more and a mixed grain ratio of preferably 10% or less. The present invention also provide a method of manufacturing the austenitic stainless steel tube comprising the following steps: (a) heating an austenitic steel tube at 1100-1350° C. and maintaining the temperature, and cooling at a cooling ratio of 0.25° C./sec; (b) working by cross-sectional reduction ratio of 10% or more at a temperature range of 500° C. or less; and (c) heating at a temperature range of 1050-1300° C. and at a temperature of lower by 10° C. or more than the heating temperature in the step(a).

Process for hot rolling of high-strength low-alloy steel cast in Compact Strip Production as a thin slab. The strain and temperature at initial roll stands where deformation occurs allows full recrystallization, and at latest roll stands where deformation occurs there is no recrystallization. Deformation is absent at strains and temperatures where partial recrystallization would occur, allowing increased recrystallization over conventional CSP rolling. The result may be beneficial for microalloyed high-strength low-alloy steel in permitting accurate ultrasonic testing of welds. The time allowed between deformation at passes through roll stands may be increased by eliminating deformation at one or more central roll stands. Combined with increased strain at the initial roll stands where the temperature of the steel is in the full recrystallization region, the process may result in a relatively fine and uniform austenite grain size.

The invention relates to a manufacture method for manufacturing a steel plate with high strength and high toughness by using a hot-rolling coiled plate. The method comprises the following steps that: firstly, after a hot-rolling coiled plate is leveled on a leveling machine set, refining heat treatment is carried out on the hot-rolling coiled plate, i.e. the hot-rolling coiled plate is heated in induction heating equipment, the heating time is within 60-140s, and the hot-rolling coiled plate is heated to 910DEG C to 960DEG C and austenized; then, the hot-rolling coiled plate enters a water-cooling or steam-cooling quenching machine set to carry out quenching, the quenching and cooling speed of the hot-rolling coiled plate is greater than or equal to 5DEG C/s, and a quenched martensite organization is obtained after quenching; tempering is carried out after quenching, induction heating is carried out by adopting the induction heating equipment in the tempering, the heating temperature of the quenched martensite organization is 220DEG C to 440DEG C, the tempering time is 80 to 180s, and a tempered martensite organization is obtained; and finally, straightening, flaw detection, surface inspection and sampling inspection are carried out to finally obtain the steel plate with excellent performance, high strength and high toughness. The invention has the advantages that as refining treatment adopts an induction heating method, the heating time is short, austenite crystal grains are fine, the mechanical property is superior to that of a similar product produced by the traditional technology, the plate type of the steel plate is good, and the invention has high production efficiency, low equipment investment, little maintenance cost of the equipment, small occupation area and little environmental pollution.

Disclosed are a high-heat-input welding thick steel plate and a manufacturing method thereof. The manufacturing method includes following steps: a) smelting, refining and continuous casting; b) rolling; and c) cooling. Steel consists of components including, by weight percentage, from 0.05 to 0.09% of C, from 0.10 to 0.30% of Si, from 1.3 to 1.7% of Mn, from 0.005 to 0.03% of Ti, from 0.003 to 0.025% of Nb, from 0.001 to 0.01% of S, smaller than or equal to 0.015% of P, smaller than or equal to 0.006% of N, from 0.0005 to 0.01% of Mg, smaller than or equal to 0.01% of Al, smaller than or equal to 0.003% of Ca, more than one of smaller than or equal to 0.3% of Cu, smaller than or equal to 0.4% of Ni and smaller than or equal to 0.002% of B, and the balance Fe; and Ti/Nb is larger than or equal to 1.2, deoxidant Mn, Si, Al, Ti, Ca and Mg are successively added in a steel liquid deoxidizing process, wherein (Mg+Ca)/Mn is larger than or equal to 0.3 for micrometer impurities with the grain size larger than or equal to 1.0 micrometer in the steel, (Mg+Ca)/Mn is larger than or equal to 0.1 for sub-micron impurities with the grain size ranging from 0.1 micrometer to 1.0 micrometer in the steel, and Ti/Mn is larger than or equal to 0.07. A large quantity of impurities which are distributed in a dispersion manner are formed, growth of austenite grains in a welding heat affected zone can be restrained, growth of intra-granular ferrite is promoted, and the high-heat-input welding performance of the thick plate is greatly improved.

A rolling bearing (10) having an outer ring (1), an inner ring (2), and a plurality of rolling elements, wherein at least one of the members, the outer ring (1), inner ring (2) and rolling elements (3), has a nitrogen rich layer and the grain size number of austenite crystal grains is in the range exceeding the number 10.

The invention relates to a metallographic corrosion method for clearly displaying the original austenite grain boundary of a NiCrMoV type rotor steel, and belongs to the field of metallographic sample preparation. The method comprises the steps of: coarse grinding, fine grinding, polishing and corroding; putting a polished sample into a corrosive liquid of 75 DEG C, wherein the formula of the corrosive liquid comprises 200ml of distilled water, 5g of picric acid, 2ml of 5% diluted hydrochloric acid and 4g of sodium dodecyl benzene sulfonate; etching for 2minutes, taking the sample out, cleaning the sample with flowing water, cleaning the sample with alcohol and drying; and observing the clear original austenite grain boundary through an optical microscope. The method has the advantages that a difficult displaying problem of the original austenite grains of the NiCrMoV type rotor steel is solved, the original austenite grain boundary can be very clearly displayed, and the method is simple and practicable.

The invention relates to a method of preparing dead mild steel ultra-low-carbon steel golden phase sample and indicating structure, it belongs to preparation technology field of golden phase sample. The invention includes the following steps: thick grinding, thin grinding-polishing, eroding, arranging corrosion fluid. Its advantages are that: solves the difficult display problems of dead mild steel ultra-low-carbon steel austenite grain, obtains the clear photograph of austenite grain, The implementation of this invention is simple, it can easily prepare dead mild steel ultra-low-carbon steel golden phase sample.

The invention discloses a metallographic-phase aggressive agent of an austenitic stainless steel, a preparation method thereof and application thereof. The metallographic-phase aggressive agent comprises the mixed solution of hydrofluoric acid and nitric acid, calculated by volume ratio, the proportion of each component of the agent is that hydrofluoric acid : nitric acid : water is equal to 2 : 1 : 7. The preparation method thereof is carried out according to the following steps of: taking 70ml of water first, then taking 10ml of analytically pure nitric acid and finally taking 20ml of analytically pure hydrofluoric acid, which are then evenly mixed. The application method thereof comprises the following steps of: putting a simple of the austenitic stainless steel in the metallographic-phase aggressive agent of the austenitic stainless steel and observing the color change of the surface of the sample by time, taking out the sample of the austenitic stainless steel when metallographic-phase surface of the sample is corroded to darker silver gray, washing the sample with water which is then neutralized with alkaline solution and finally washing with water and absolute ethyl alcohol. The technical effects thereof are represented by good corrosion effect, clear austenite grain boundary, slow corrosion speed, easy control, no pollution and other aspects.

A steel-made rolling-contact shaft with a joint claw improved in both the rolling contact fatigue life at the raceway and the static fracture strength (torsional strength) at the claw includes a joint claw at one end, and has a portion of the outer cylindrical surface functioning as a raceway of a needle roller qualified as a rolling element of a needle bearing. The joint claw is subjected to tempering by induction heating. A nitrogen-enriched layer is formed at the surface layer of the rolling-contact shaft with a joint claw. The grain size number of austenite grains in the nitrogen-enriched layer exceeds number 10. The hydrogen content of the rolling-contact shaft with ajoint claw is not more than 0.5 ppm.

The invention discloses a corrosive agent for displaying 9% Cr steel original austenite grain boundary and an application thereof. The corrosive agent is prepared by fully mixing the following components of: 60-80ml of H2O, 4-8ml of 36 wt% HCl, 2-4g of FeCl3, 0.2-0.5g of picric acid, and 1.0-2.0g of sodium dodecanesulphonate. The corrosive agent provided by the invention can be used as a reagent for 9% Cr steel grain boundary to clearly display the original austenite grain boundary of large crystal grain, large and small mixed crystal grain and small crystal grain of a sample. Under 100 times, it is easy to carry out grain size rating and the effect is good.

The invention relates to a method for producing an annealing-free hot rolling S50C plate and strip, belonging to the technical field of hot rolled plates and strips. The invention adopts the technical scheme that austenite rolling is adopted in rough rolling, a deformation-induced ferrite rolling and warm rolling combined process is adopted in finish rolling, temperature in a rough rolling region is controlled to be 960-1150 DEG C, accumulated screwdown rate is more than 50%, an intermediate blank obtained by the rough rolling is cooled by water and then enters into a finish rolling mill group, opening rolling temperature of a finish rolling mill is 760-850 DEG C, finished rolling temperature of the finish rolling mill is 650-750 DEG C, the accumulated screwdown rate is more than 50%, cooling rate after rolling is controlled to be 0.1-25 DEG C/s, and coiling temperature is controlled to be 550-700 DEG C. The austenite rolling during rough rolling is carried out, thus austenite crystals are refined; the deformation-induced ferrite rolling and warm rolling during finish rolling are carried out, thus ferrite is excessively separated out, carbide is modified in a deformation process, plasticity and toughness of steel are improved, the aim of direct moulding while annealing is eliminated is achieved, and a spheroidizing process before cold forming is eliminated.

The invention relates to a secondary cooling method for effectively controlling the surface-layer solidification structure of a continuous cast slab. After the continuous cast slab is discharged out of a crystallizer, the casting machine vertical section is cooled at the cooling speed of 3-10 DEG C/s for 50-160 s, the secondary cooling water quantity in the cooling section corresponding to the time period is increased to 2-5 times larger than the original water quantity, i.e. the broadside water quantity is 260-600 L/min, and the narrow side water quantity is 50-125 L/min. After the intensive cooling of the casting machine vertical section is finished, the subsequent cooling sections adopt the secondary cooling mode with the specific water flow of 0.55-0.8 L/kg. Shown by practices, the surface-layer structure of the cast slab poured in the secondary cooling mode is compact, the grain size is 10-100 mum, precipitates at grain boundary are few and uniform, and the original austenite grain boundary at high temperature is not obvious. High-temperature plasticity tests on steel show that the plasticity of the steel is obviously improved, which is beneficial to elimination of crack defects of the cast slab.

The invention belongs to a producing and cooling technique of rolled steel, relating to a cooling method of a heavy and medium plate controlled rolling intermediate blank, which can be realized by both a single-stand heavy and medium plate roll and a double-stand heavy and medium plate roll. The cooling method comprises the following steps of: transmitting a roughly rolled intermediate blank with the thickness range of 30-110 mm in an austenite recrystallization zone into an intermediate controlled cooling zone from a transmission roller way for rapidly cooling to 800-950 DEG C, and then transmitting the intermediate blank into the roll for rolling in a non- recrystallization zone after short-time air cooling and temperature evening. In the intermediate cooling process, an upper collecting pipe and a lower collecting pipe with high density or ultra-high density are adopted to impact, jet and cool the intermediate blank, and specific technological parameters are accurately controlled by a computer. Water is cooling water for the roll with the pressure of 0.3-1.0 MPa in a common water circulating system for workshops. The intermediate cooling holding time is 30-70% shorter than that of the conventional process so that the production efficiency is improved, and due to austenite grain refinement after intermediate controlled cooling, the mechanical properties of a steel plate can be improved.