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2523 results about "Dodecylsulfonic acid" patented technology

Compound plant-derived pesticide and preparation method thereof

The invention relates to a compound plant-derived pesticide, which is prepared by mixing the following components in percentage by weight: 2-5% of nicotine, 2-5% of wild mugwort oil, 3-8% of cinnamon leaf oil, 5-10% of litsea cubeba oil, 30-40% of flavescent sophora root mixed ethanol extract, 10-15% of Rangoon creeper fruit mixed water extract, 15-20% of emulsifying agent, 1-2% of sodium dodecylsulfate and the balance of water, wherein the flavescent sophora root mixed ethanol extract is obtained by extracting 3 parts by weight of flavescent sophora root, 1 part by weight of triperygium wilfordii, 2 parts by weight of toosendan fruit, 2 parts by weight of hellebore, 2 parts by weight of szechuan aconite, 1 part by weight of cnidium fruit and 1 part by weight of camphor tree seed with 70wt% ethanol solution, and has the relative density of 1.02-1.10; and the Rangoon creeper fruit mixed water extract is obtained by extracting 1 parts by weight of groundsel and 2 parts by weight of Rangoon creeper fruit with water solution, and has the relative density of 1.02-1.10. The compound plant-derived pesticide overcomes the limitations that the most plant derived pesticides are single in pest-killing components and simple in action mechanism, improves the comprehensive prevention and control effect, is quick in acting and long in duration, and avoids the generation of pest pesticide resistance.
Owner:HUBEI CHINA TOBACCO IND +1

Method for recycling carbon and electrolytes from waste cathode carbon block of aluminum electrolytic cell

InactiveCN105821445AReduce dosageReduced dosage of chemicals (reduced amount of collectorElectrolysis componentsCalcium/strontium/barium fluoridesKeroseneFuel oil
The invention discloses a method for recycling carbon and electrolytes from a waste cathode carbon block of an aluminum electrolytic cell. The method comprises the following steps that 1, the cathode carbon block is crushed and grinded; 2, cathode carbon powder obtained from the cathode carbon block subjected to crushing and grinding in the step 1 is stirred and leached in alkali liquor and then filtered, so that a filter cake A1 and filtrate B1 are obtained; and a precipitating agent is added into the filtrate B1, so that a filter cake A2 and filtrate B2 are obtained after filtering is conducted; and 3, the filter cake A1, the filter cake A2, a flotation medium and flotation reagents are subjected to mixing and pulp conditioning, and thus the carbon and electrolytes are obtained through flotation and separation; the flotation reagents comprises the collecting agents, the foaming agents and the conditioning agents; the collecting agents are composed of the collecting agent C1 and the collecting agent C2 at the mass ratio of 0.65-0.75:0.25-0.35; the collecting agent C1 is selected from at least one of coal tar, heavy oil, kerosene and diesel oil; and the collecting agent C2 is selected from at least one of dodecylamine, sodium dodecyl benzene sulfonate, sodium oleate and sodium dodecyl sulfate. According to the method for recycling the carbon and the electrolytes from the waste cathode carbon block of the aluminum electrolytic cell, the carbon powder and the electrolytes are effectively separated and recycled from the waste cathode carbon block.
Owner:CENT SOUTH UNIV

Preparing method of nano-magnetic polymer composite microsphere

The invention relates to a preparing method ofa nano-magnetic polymer composite microsphere, which comprises the following steps: preparing a hydrophilic Fe3O4 magnetic liquid particle by using a chemical co-precipitation method; dissolving initiating agents and emulsifying agents by weight part into ionized water to prepare water phase, adding the hydrophilic Fe3O4 magnetic liquid particle and adding a monomer to obtain nano-magnetic seed emulsion through polymerization; dissolving initiating agents by weight part into ionized water, adding the nano-magnetic seed emulsion and then adding a monomer to obtain nano-magnetic polymer composite microsphere emulsion through polymerization; the emulsifying agents are sodium lauryl sulfate, sodium dodecyl sulfate or sodium dodecyl benzene sulfonate; the initiating agents are potassium peroxydisulfate, ammonium persulphate or sodium peroxydisulfate; the initiating agents are potassium peroxydisulfate, ammonium persulphate or sodium peroxydisulfate; the hydrophobic monomer is styrene or methyl methacrylate or a mixture of the styrene and the methyl methacrylate; the nano-magnetic polymer composite microspheres prepared by adopting a seed emulsion polymerization method have the superparamagnetism, have stronger magnetic responsiveness, have no uncoated magnetic particle and contain magnetic polymer microspheres and are narrow to distribute.
Owner:PETROCHINA CO LTD

Method for preparing MWNT (Multi-Walled Carbon Nanotube) modified paper-based friction material

ActiveCN102943410AOvercoming the problem of unstable friction performanceIncrease frictionOther chemical processesPaper/cardboardFiberCarbon fibers
The invention relates to a method for preparing an MWNT (Multi-Walled Carbon Nanotube) modified paper-based friction material, which comprises the following steps of: dissolving cashew nut shell modified phenolic resin into absolute ethyl alcohol to obtain solution A; dispersing MWNTs into aqueous solution of sodium dodecyl sulfate to obtain suspension B; dispersing chopped carbon fibers, bamboo fibers and kieselguhr into water and then adding the suspension B to obtain solution C; after pouring the solution C into a fluffer to disperse, carrying out sheet making on a sheet making machine and drying to obtain a sample wafer D; and after impregnating the sample wafer D in the solution A, taking out the sample wafer D, naturally air-drying the sample wafer D and carrying out hot-press forming on a vulcanizing machine so as to obtain the MWNT modified paper-based friction material with a stable friction performance. According to the invention, the carbon nanotubes are used as the raw materials to be added into a carbon fiber reinforced reins-based wet friction material so as to prepare the single-layer paper-based friction material. The problems of delamination and unstable friction performance in the long-term application process, which are caused by the case that the carbon nanotubes are used as an enhancement layer to be added into the friction material in a conventional process, are solved; the friction performance of the paper-based friction material is greatly improved; and the wear rate is effectively reduced.
Owner:杨洁如

Direct flotation collector of collophanite at room temperature and preparation method thereof

InactiveCN103056036ARealization of normal temperature positive flotationImprove solubilityFlotationActive agentProcess engineering
The invention belongs to collophanite flotation technology, and relates to a direct flotation collector of collophanite at room temperature and a preparation method thereof. The collector comprises ingredients with the following weight ratio: fatty acids 95-100 parts, sodium hydroxide 10-15 parts, sodium dodecyl sulfate 3-8 parts, polyoxyethylene5-10 parts and pine oil 1-3 parts. The preparation method includes: according to a certain weight ratio, heating and stirring the mixture of sodium dodecyl sulfate, polyoxyethylene pine oil, and water to obtain a novel surfactant; subjecting the fatty acid to saponification; finally, compounding the saponificated fatty acid and the novel surfactant by a certain percentage, stirring uniformly so as to obtain the collector. The direct flotation collector is not only good in solubility, but adaptable to low and medium grade collophanite and different temperature. In addition, the direct flotation collector has the advantages of good stability and simple pharmaceutical preparation process, Information about residual glue in the glue container is determined according to forming of vacuum when the vacuum generating system extracts air in the detection tube and accordingly can be widely used in the beneficiation of collophanite.
Owner:INST OF MULTIPURPOSE UTILIZATION OF MINERAL RESOURCES CHINESE ACAD OF GEOLOGICAL SCI

Berberine electrostatic composite and preparation method of berberine electrostatic composite

The invention discloses a berberine electrostatic composite and a preparation method of the berberine electrostatic composite, which are applied to medical and health industries. The berberine electrostatic composite is prepared from anionic surfactant and berberine or berberine salt by compositing; the molar ratio of the anionic surfactant to the berberine or berberine salt is 1 to 0.5-10; the molar ratio of anion to the berberine salt is 1 to 1; the anionic surfactant is one or more of alkyl sulfate or alkyl sulfonate or fatty acid salt; the alkyl sulfate is one or more of sodium cholesteryl sulfate, lauryl sodium sulfate and deoxysodium cholate; the alkyl sulfonate is one or more of sodium heptanesulfonate and sodium dodecyl sulfate; the fatty acid salt is one or more of sodium caprate and sodium enanthate, and the berberine and berberine salt are obtained by chemical synthesis or by extracting traditional Chinese medicine. The berberine is prepared into the berberine electrostatic composite to increase the biological membrane penetrating ability of the berberine and improve the oral bioavailability of the berberine, and the berberine electrostatic composite plays a significant treatment role on important chronic metabolic disorder diseases such as diabetes mellitus, complication of the diabetes mellitus, hyperlipidemia and the like.
Owner:NORTHEAST PHARMA GRP

Synthesis method of hydroxyoximate

The invention relates to a synthesis method of hydroxamate. The hydroxamate is synthesized from fatty acid, short chain alcohol, dodecyl sulfonic acid, hydroxylamine hydrochloride and caustic alkali by two steps; and the synthesis method comprises the following steps of adding fatty acid, short chain alcohol and dodecyl sulfonic acid into a reactor, stirring and reacting at a constant temperature of 75 DEG C-100 DEG C; carrying out reduced pressure distillation on the reactants to obtain fatty acid ester; adding hydroxylamine hydrochloride into another reactor, adding caustic alkali in batches while stirring, and mixing; adding fatty acid ester and reacting for 3-5 hours at 40 DEG C-60 DEG C to obtain a hydroxamate solution; and rapidly cooling the hydroxamate solution to obtain the solid hydroxamate. By the synthesis method, the conversion between acid-alkali environment for the esterification and hydroximation two-step reaction is avoided, the synthesized product needs not to be subjected to processing steps such as acidification, impurity removal and purification and the obtained product can be organically combined with flotation industry. The synthesis method has the advantages that the operation is simple, the yield of the product is high, the generation of a large amount of acidic wastewater is avoided and the cost of chemical agents is effectively decreased.
Owner:BLUESTAR LEHIGH ENG INST CO LTD

Heavy metal cadmium, lead and arsenic compound contaminated soil restorative agent and preparation method thereof

The invention provides a heavy metal cadmium, lead and arsenic compound contaminated soil restorative agent. The heavy metal cadmium, lead and arsenic compound contaminated soil restorative agent is prepared from the following components in percentage by weight: 30-50 percent of biomass charcoal, 5-10 percent of diatomite, 5-10 percent of sodium bentonite, 5-10 percent of activated aluminum oxide, 10-20 percent of dithiocar-bamate, 5-10 percent of ethylenediaminetetraacetic acid, 5-10 percent of tartaric acid, 5-10 percent of polyacrylamide and 5-10 percent of sodium dodecyl sulfate. A preparation method for the heavy metal cadmium, lead and arsenic compound contaminated soil restorative agent comprises the following steps: mixing the biomass charcoal, diatomite, sodium bentonite, activated aluminum oxide, ethylenediaminetetraacetic acid, tartaric acid, polyacrylamide and sodium dodecyl sulfate in mass proportion to obtain a mixture; and adding the dithiocar-bamate into the mixture in corresponding mass proportion to sufficiently mix uniformly, thereby obtaining the prepared soil restorative agent. The prepared soil restorative agent has good effect in restoring the cadmium, lead and arsenic compound contaminated soil.
Owner:CHANGSHA HUIJU ENVIRONMENTAL TECH CO LTD

Nanometer carboxylated polystyrene microsphere with spacer arm and preparation method thereof

The invention relates to a nanometer carboxylated polystyrene microsphere with a spacer arm and a preparation method thereof. A nanometer carboxylated polystyrene microsphere A is prepared by taking styrene and acrylic acid as a mixed monomer, taking water as a reaction medium, taking potassium persulfate as an initiator and taking sodium dodecyl sulfate as an emulsifier with an emulsion polymerization method. In the presence of EDC (Ethylidene Dichloride) serving as a coupling agent and Sulfo NHS, 4-aminobutyric acid, 6-amidocaproic acid or 8-aminocaprylic acid is connected to the surface of the microsphere, so that the nanometer carboxylated polystyrene microsphere with the spacer arm is prepared. The spacer arm is introduced into the surface of the nanometer microsphere, so that the steric hindrance of a coupling macromolecule is lowered, the activity and utilization ratio of the macromolecule are increased, and a nonspecific interaction between the macromolecule and the polystyrene microsphere is reduced. Meanwhile, the grain diameter of the microsphere can be adjusted by adjusting the using amount of the emulsifier, the length of the space arm and surface density, so that the nanometer microsphere has a wide application prospect in the fields of immune diagnosis, solid phase extraction and the like when serving as a carrier as well as a template.
Owner:TIANJIN MEDICAL UNIV

Preparation method of coal-based magnetic activated carbon and coal-based magnetic activated carbon

The invention relates to a preparation method of coal-based magnetic activated carbon and the coal-based magnetic activated carbon. The preparation method of the coal-based magnetic activated carbon comprises the following steps of: placing deashing coal dust and dodecyl sodium sulfate into a ferric chloride solution, sufficiently mixing, and then standing for adsorption; then adding ammonia water and a sodium hydroxide solution or a potassium hydroxide solution, sufficiently stirring, and then standing for transforming ferric chloride into ferric hydroxide; filtering and drying solid-phase materials to obtain a mixture of deashing coal and the ferric hydroxide, i.e. a precursor of the coal-based magnetic activated carbon; sufficiently mixing the precursor with activating agents, i.e. potassium hydroxide or sodium hydroxide, adding distilled water to stir into paste, and warming for carbonization under the protection of nitrogen; and heating and activating under the protection of the nitrogen. The obtained coal-based magnetic activated carbon has difficult blockage of pores because a magnet exists in a state of Fe3C, thereby having higher saturation and magnetization intensity and larger specific surface area. The invention has the advantages of extensive source of coal raw materials, low cost, simple preparation process and easy separation and recovery of the coal-based magnetic activated carbon.
Owner:CHONGQING UNIV
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