The invention relates to the technical field of
metal material preparation, and particularly discloses a method for preparing an ODS
alloy based on a 3D printing and ply rolling process, and the method comprises the following steps: S1, uniformly mixing
alloy powder with reaction element
powder; s2, preparing the uniformly mixed
powder into a block material; s3, stacking the blocks to form a sheathed steel material A, and carrying out
hot isostatic pressing treatment; s4, hot rolling treatment is carried out, a sheath is removed, and a
hot rolled plate is formed;
cutting and
processing the hot-rolled plate into thin plates with the same size; s5, repeating the steps S3 to S4 until the reaction elements are uniformly distributed to obtain a thin plate; s6, performing high-temperature
oxygen permeation treatment; s7, the thin plates are stacked to form sheathed steel B, and
hot isostatic pressing treatment is carried out; and S8, the sheathed steel B is subjected to hot
forging, a sheath is removed, and the ODS
alloy is obtained. The prepared ODS alloy has the advantages of high purity, high-uniformity oxidation phase, controllable
crystal grains, stable quality and
isotropy.