The application discloses a preparation method of a
metal catalyst material and application of the
metal catalyst material in controllable degradation of polysaccharides, and the preparation comprises the following steps: mixing and reacting a ligand material with a
metal ion solution,
solid-liquid separation, washing, and
drying;
grinding the dried
solid into
powder, and then high-temperature calcining to obtain a metal monatomic catalyst, namely the
metal catalyst material; or uniformly mixing and
grinding the obtained metal monatomic catalyst with a
metal organic framework material, and then high-temperature calcining to obtain a composite
metal catalyst material. The
metal catalyst material prepared by the application can make up for the limitations of
Fenton oxidation principle in degrading polysaccharides, such as large iron consumption, strong
pollution, and difficult control, and can avoid the adverse effects caused by the corrosiveness of
hydrogen peroxide in actual production and operation. Different molecular weight polysaccharides can be obtained by adjusting the proportion and dosage of the metal catalyst material, the method can prepare polysaccharides with different molecular weights, and the prepared polysaccharides have good uniformity.