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100results about How to "High tensile shear strength" patented technology

High-temperature resistant copper foil glue and preparation and application thereof

The invention relates to high-temperature resistant copper foil glue containing the following components: 5-15wt percent of trifluoromethyl-contained maleimide resin, 10-30wt percent of polyfunctional ethoxyline resin, 10-40wt percent of bisphenol A epoxy resin, 5-15wt percent of ethylene-contained polyetherimide, 5-10wt percent of curing agent and 25-45wt percent of organic solvent; the preparation comprises the following steps of: adding the trifluoromethyl-contained maleimide resin and the ethylene-contained polyetherimide to the mixture of the polyfunctional ethoxyline resin and the bisphenol A epoxy resin, stirring while heating for reacting, and then cooling to 30-50 DEG C; adding the organic solvent and the curing agent; evenly stirring to obtain the high-temperature resistant copper foil glue the homogeneous phase of which is transparent and clear. The high-temperature resistant copper foil glue has Tonset temperature reaching up to 415 DEG C and excellent comprehensive performance, can be applied to the high-tech fields of electronics and microelectronics, automobiles, electrical machines, aerospace and the like; moreover, the invention has simple preparation process, low cost, convenient operation and available reaction raw materials, thereby being beneficial to realizing industrial production.
Owner:DONGHUA UNIV

Light-cured adhesive as well as preparation method and application thereof

The invention provides a light-cured adhesive and a preparation method and application thereof.The light-cured adhesive is prepared from sulfydryl-terminated hyperbranched polyester, urethane acrylate, epoxy resin, a reactive diluent, a silane coupling agent and a photobase generator. Compared with the prior art, sulfydryl-terminated hyperbranched polyester is adopted as a preparation raw material, and an active diluent is supplemented, so that the viscosity of the adhesive system can be further reduced, the uniform dispersion and migration of active components generated after illumination inthe system are facilitated, the concentration of active components at the bottom layer can be improved, and deep curing can be quickly realized after heating and drying. Sulfydryl-terminated hyperbranched polyester, urethane acrylate and epoxy resin are used as reaction monomers, and under the action of alkaline light initiation of a photobase generator, sulfydryl double bonds / epoxy can be subjected to a rapid click chemistry type deep photocuring reaction. The polyurethane acrylate and the silane coupling agent are introduced, so that the toughness, the adhesive force and the waterproof performance of the adhesive can be effectively improved.
Owner:GUANGDONG PUSTAR SEALED RAYON CO LTD

High-temperature-resistant benzoxazine resin adhesive and preparation method thereof

The invention discloses a high-temperature-resistant benzoxazine resin adhesive and a preparation method thereof, relates to a benzoxazine resin adhesive and a preparation method thereof, and aims to solve the problems of poor resistance of an existing benzoxazine resin adhesive to high temperature and weak tensile shear strength at high temperature. The adhesive comprises acetylene-terminated benzoxazine resin, a toughening agent, an organic solvent, a coupling agent and an inorganic filler. The method comprises the following steps: 1, placing dihydric phenol, aminophenylacetylene and paraformaldehyde in a four-neck flask, performing heating reaction and cooling, adding trichloromethane for dissolution, performing extraction, performing washing to neutral with de-ionized water, and performing drying to obtain the acetylene-terminated benzoxazine resin; 2, uniformly mixing the acetylene-terminated benzoxazine resin, the toughening agent and the organic solvent to obtain a base adhesive; 3, sequentially adding the coupling agent and the inorganic filler into the base adhesive, and performing uniform mixing to obtain the high-temperature-resistant benzoxazine resin adhesive. The adhesive is resistant to high temperature, has strong tensile shear strength at high temperature, and is used in the field of adhesives.
Owner:INST OF PETROCHEM HEILONGJIANG ACADEMY OF SCI

Organic grouting material for road and preparation method of organic grouting material for road

The invention discloses an organic grouting material for a road and a preparation method of the organic grouting material for the road. The organic grouting material for the road is prepared by foaming black and white polyurethane materials, wherein an epoxy resin-diethanolamine affixture (EP-DEA affixture) is also added into the white polyurethane material, and the addition of the EP-DEA affixture accounts for 5-20wt% of the total mass of the black and white polyurethane materials. The EP-DEA affixture is prepared by using a method comprising the following steps of mixing EP and DEA, and uniformly dispersing in a reaction vessel by taking butanone as a solvent; heating to 70 DEG C, maintaining the temperature and reacting for 4h; and removing the superfluous solvent through reduced-pressure distillation to obtain a slightly-yellow oily liquid, namely the EP-DEA affixture. When the organic grouting material for the road, disclosed by the invention, is used for filling a gap of the road by grouting and solidifying, the adhesive property of solidification filler is better and the compression strength is more approximate to the use requirement on the premise that the grouting performance is not influenced, and therefore, the organic grouting material is an excellent improved product of a pure black / white polyurethane product, which is maximally used at present.
Owner:GUANGDONG PROVINCIAL CHANGDA HIGHWAY ENG +1

Organic silicon electronic pouring sealant for flame retardant heat conduction PCB (printed circuit board)

The invention discloses an organic silicon electronic pouring sealant for a flame retardant heat conduction PCB (printed circuit board). The organic silicon electronic pouring sealant is prepared from the following raw materials in parts by weight: 40 to 50 parts of vinyl-terminated silicone oil-1, 50 to 60 parts of vinyl-terminated silicone oil-2, 0.38 to 0.5 part of 12-percent platinum catalysts, 0.02 to 0.04 part of ethynyl cyclohexanol, 25 to 30 parts of vinyl silicone resin, 14.8 to 16.8 parts of 1-allyloxy-2,3-epoxy propane, 23 to 25 parts of 1,3,5,7-tetramethyl cyclotetrasiloxane, 2.7 to 3.6 parts of silane coupling agents A171, a proper amount of hydrogen-containing silicone oil, 4 to 5 parts of quartz powder, 2 to 3 parts of aluminum hydroxide, 0.3 to 0.5 part of titanate coupling agents TC114 and 0.3 to 0.4 part of silane coupling agents KH560. The prepared pouring sealant has the advantages that the curing time is short; the viscosity is stable; the intensity is high; the anti-corrosion performance and the flame retardant performance are good; the production process is stable; the operability is high; the pouring sealant is suitable for large-scale production.
Owner:铜陵安博电路板有限公司
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