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1704results about "Ether separation/purification" patented technology

Energy-saving and emission-reducing technique for producing propane epoxide by using hydrogen peroxide epoxidation propylene

The invention relates to an energy-saving and emission-reducing technique for producing propane epoxide by using hydrogen peroxide epoxidation propylene, belonging to the field of petrochemical technology. The technique comprises a reaction part, a separation part and a tail gas treatment part, and is characterized in that propylene and hydrogen peroxide have an epoxidation reaction through a Ti-Si molecular sieve at medium pressure and low temperature; the propylene and solvent have higher recovery rate, the propane epoxide meeting the requirement of commercial-grade purity can be obtained by extractive distillation, and the joint product of propylene glycol monomethyl ether can be prepared by azeotropic distillation and purification; after part of tail gas is condensed and absorbed and the propylene is recovered, the tail gas reaches the standard and is discharged; extracting agent, absorbing agent and entrainer which are needed by the technique are in closed cycle in the process flow; and medium-pressure operation is adopted by a propylene tower to ensure water-cooling on the top of the tower, and thermal energy can be recovered by multiple-effect rectification and matching of streams. The technique has the effect and the advantage that the new energy-saving and environment-friendly technique for producing the propane epoxide can generate remarkable economic and social benefits.
Owner:DALIAN UNIV OF TECH

System for recovering glycol from glycol/brine streams

A system for recovering glycol from glycol and brine mixtures produced from oil or natural gas wells that combines energy efficiency with a capability for handling salt and other solids contained in the mixture. The system comprises three effect evaporator systems in series. Each effect evaporator system comprises an evaporator, a separator vessel, product pumps, and a solids removal system.The process utilizes the system to remove salt and other solids as well as excess water leaving a glycol stream that can be reused as a hydrate inhibitor. The process begins by preheating a glycol / brine stream comprising approximately fifty percent (50%) glycol. The stream is then subjected to three evaporation cycles. The first evaporation cycle comprises introducing the preheated stream into a suppressed boiling point evaporator where the stream is heated under a constant pressure. The stream pressure is then dropped to cause a portion of the water contained in the stream to vaporize or flash. The flashing stream is then introduced into a separator vessel where the water vapor is separated from the remaining liquid stream. The water vapor is removed from the separator and condensed. The remaining liquid glycol / brine stream is then pumped from the separator vessel through a solids removal system where precipitated salts and solids are removed. These steps are repeated two additional times. Each time the remaining liquid stream becomes more concentrated with glycol until the finished product is approximately ninety percent (90%) glycol.
Owner:TRANSOCEAN SEDCO FOREX VENTURES LTD

Process and system for recovering glycol from glycol/brine streams

A process and a system is disclosed for recovering glycol from glycol and brine mixtures produced from oil or natural gas wells that combines energy efficiency with a capability for handling salt and other solids contained in the mixture. The system comprises three effect evaporator systems in series. Each effect evaporator system comprises an evaporator, a separator vessel, product pumps, and a solids removal system. The process utilizes the system to remove salt and other solids as well as excess water leaving a glycol stream that can be reused as a hydrate inhibitor. The process begins by preheating a glycol/brine stream comprising approximately fifty percent (50%) glycol. The stream is then subjected to three evaporation cycles. The first evaporation cycle comprises introducing the preheated stream into a suppressed boiling point evaporator where the stream is heated under a constant pressure. The stream pressure is then dropped to cause a portion of the water contained in the stream to vaporize or flash. The flashing stream is then introduced into a separator vessel where the water vapor is separated from the remaining liquid stream. The water vapor is removed from the separator and condensed. The remaining liquid glycol/brine stream is then pumped from the separator vessel through a solids removal system where precipitated salts and solids are removed. These steps are repeated two additional times. Each time the remaining liquid stream becomes more concentrated with glycol until the finished product is approximately ninety percent (90%) glycol.
Owner:TRANSOCEAN SEDCO FOREX VENTURES LTD

Method and device for removing organic sulfur in methyl tertiary butyl ether (MTBE)

The invention relates to a method and a device for removing organic sulfur in methyl tertiary butyl ether (MTBE). The method and the device are utilized for high-sulfur content MTBE refinement. The method and the device realize normal-pressure low-temperature extraction rectification desulphurization of a high-sulfur content MTBE product. A technical scheme of the invention comprises the following steps that 1, a sulfur-containing MTBE product is heated by a heat exchanger and then is fed into a rectifying tower from a lower part of the rectifying tower; 2, an extractant is fed into the heat exchanger, is heated and then is fed into the rectifying tower from an upper part of the rectifying tower, wherein a rectifying tower temperature is in a range of 70 to 80 DEG C and the heated sulfur-containing MTBE product and the heated extractant countercurrently contact with each other so that countercurrent contact extraction desulphurization is realized; 3, the desulfurated MTBE product is output from the top of the rectifying tower, is subjected to cooling condensation to form liquid in the heat exchanger and then is output; and 4, the sulfur-containing extractant obtained by the step 2is output from the bottom of the rectifying tower, is heated by the heat exchanger, is fed into a flash tank, is distilled at a temperature of 80 to 85 DEG C so that the residual desulfurated MTBE product is distilled off, then is fed into an actifier column, and countercurrently contacts with dry air in the actifier column so that countercurrent contact gas stripping regeneration is realized. Through the method and the device, good desulphurization effects are realized; a high product yield is obtained; and an extractant can be regenerated for recycle. The method is convenient for operation,has low costs and low energy consumption, and can be utilized for high-sulfur content MTBE product refinement.
Owner:SOUTHWEST PETROLEUM UNIV

Method of stabilizing reduced coenzyme q10

The present invention provides a stabilization method, a preservation method and the like method of reduced coenzyme Q10, which is useful as functional nutritive foods, specific health foods and the like. Furthermore, the present invention provides a method for efficiently obtaining reduced coenzyme Q10 of high quality and by a method suitable for a commercial production.
It is possible to handle and stably preserve reduced coenzyme Q10 under a condition that oxidation by a molecular oxygen is inhibited by contacting reduced coenzyme Q10 with an ascorbic acid and citric acid or a related compound thereof, and thus a stabilized composition is obtained. Moreover, reduced coenzyme Q10 is converted into a crystalline state in such a condition that the formation of oxidized coenzyme Q10 as a byproduct is minimized by crystallizing reduced coenzyme Q10 in the presence of ascorbic acid or a related compound thereof, etc., and thus a reduced coenzyme Q10 crystal of high quality is produced. Furthermore, by successively crystallizing the generated reduced coenzyme Q10 in the presence of ascorbic acid or a related compound thereof after reducing oxidized coenzyme Q10 to reduced coenzyme Q10 using ascorbic acid or a related compound thereof, operations are simplified and minimized, and thus reduced coenzyme Q10 of high quality is produced.
Owner:KANEKA CORP

Method and device for recovering polyethylene glycol raffinate byproduct from ethylene glycol process

The invention relates to a method and a device for recovering a polyethylene glycol raffinate byproduct form an ethylene glycol process. The method comprises the following steps of: (1) adding phosphoric acid into the polyethylene glycol raffinate, controlling the pH value to be between 7 and 9, conveying the mixture to a preheater (1), and preheating; (2) allowing a preheated material to enter a scraper falling-film evaporator (2), discharging a material at the bottom of the evaporator into an intermediate tank (3), and allowing the material to enter the preheater (1) through a centrifugal separator (8); (3) conveying the mixture of water and alcohol on the top of the falling-film evaporator to a dehydration rectifying tower (3); (4) conveying a mixed alcohol material at the bottom of the tower to an ethylene glycol separating tower (4); (5) conveying the material at the bottom of the tower to a diethylene glycol separating tower (5); and (6) conveying the material at the bottom to a triethylene glycol separating tower (6), and collecting products on the top and bottom of the tower respectively. The method is simple, efficient and low in energy consumption, and is suitable for industrial application; and by the method, the utilization rate of the raffinate produced by ethylene glycol is improved.
Owner:NINGBO POLYTECHNIC +1

Novel technique for preparing schizandrol A and schizandrol B

The invention belongs to the field of medical technology and discloses a new preparation technique of schizandrol B and schizandrol A in schisandra chinensis baill leaves. The technique comprises the steps: schisandra chinensis baill leaves are taken as raw material, ground and then processed by one or more technique(s) in solvent extraction method, organic solvent extraction method, resin adsorption method, normal phase column chromatography, reversed-phase column chromatography and the like, namely, the schisandra chinensis baill leaves are taken as raw material, extracting solution containing the schizandrol A and the schizandrol B is extracted by organic solvent; after extract is processed by repeated column chromatographic separation, the flowing parts containing the schizandrol A and the schizandrol B are collected, and the schizandrol A and the schizandrol B are obtained after repeated recrystallization of the condensate; the purities of the schizandrol A and the schizandrol B can be more than 98% by HPLC detection. The preparation method has simple technique, stable purity and good reproduction quality, can be used for replacing shizandra fruit to extract and prepare standard product, fully utilizes the resource of shizandra and relieve the situation that the supply of the shizandra fruit is not adequate to the demand.
Owner:SHENYANG PHARMA UNIVERSITY
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