The invention relates to a preparation method of
mullite whisker precursor pressureless forming one-time
sintering light heat insulation
ceramic, which comprises the following steps: mixing nano aluminum
sol,
nano silicon sol and water according to a certain proportion, adding
ammonium molybdate tetrahydrate, and uniformly stirring to prepare a
whisker growth precursor; and
drying in a
drying oven,
grinding into a
solid powdery product in a
mortar, filling an aluminum
oxide mold with the
solid powdery product, carrying out non-pressure compaction, carrying out high-temperature
calcination in a furnace, cooling, taking out, and demolding to obtain the lightweight porous
ceramic block prepared by in-situ growth of the
mullite whiskers. The preparation method has the advantages that the preparation process is easy to operate, green and free of
pollution,
renewable materials are used as raw materials, and the requirements for
environmental protection and
sustainable development are met; the morphology and components of the porous light heat-insulating block can be accurately controlled, and the porous light heat-insulating block has better stability under a high-temperature condition; the prepared porous light heat-insulating
ceramic block has high
compressive strength which is concentrated at 4.15-4.57 MPa, and is light, the density is concentrated at 0.65-0.75 g / cm < 3 >, the
porosity can reach 76.3-79.4%, and the load of the whole structure can be reduced. After the ceramic block is exposed for 1800-2000 seconds at 1250-1350 DEG C, the back temperature of the ceramic block is 290-300 DEG C, and the ceramic block has excellent heat insulation performance.