The invention discloses a method for preparing a
porous carbon material by recycling
coal gasification
slag and semi-
coke wastewater, which comprises the following steps: by taking
coal gasification fine
slag as a carrier and semi-
coke wastewater as a
phenol source, carrying out flotation-acid leaching modification on the fine
slag to purify a carbon-rich component and optimize the surface adsorption activity of the carbon-rich component; then fully adsorbing phenolic substances in the
wastewater by utilizing the modified slag body; introducing a composite
aldehyde cross-linking agent, and initiating an in-situ
phenolic aldehyde polymerization reaction to generate a composite precursor; the precursor is subjected to high-temperature
carbonization and alkali activation pore forming, and finally the
porous carbon material with the characteristics of high specific surface area, rich graded pores and low ash content is prepared. According to the process, full-amount collaborative recycling of the two wastes is achieved, and the process is green and free of secondary
pollution. The obtained material is high in carbon content and rich in defect structure and surface functional groups, shows excellent adsorption capacity and catalytic carrier performance, can be widely applied to the fields of deep purification of
water pollutants, adsorption of volatile organic compounds, energy
catalysis and the like, and has remarkable
environmental protection benefits and resource economic values.