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807 results about "Tricresyl phosphate" patented technology

Tricresyl phosphate, abbreviated TCP, is an organophosphate compound that is used as a plasticizer and diverse other applications. It is a toxic substance that causes neuropathy through ingestion, and has been the cause of several mass poisonings in history. It is a colourless, viscous liquid, although commercial samples are typically yellow. It is virtually insoluble in water.

Ester type fire-resistant hydraulic fluid and preparation method thereof

InactiveCN103013635AInhibition of catalytic oxidationImprove stabilityLubricant compositionPhosphoric acidTriazole derivatives
The invention relates to an ester type fire-resistant hydraulic fluid. The hydraulic fluid comprises the following raw materials by weight percent: 95-99% of base oil, 1.0-5.0% of diphenol propane, 0.005% of dimethylsilicone fluid or dimethylsilicone grease, 0.05% of tricresyl phosphate, 0.1% of benzotriazole, 100 parts per million (PPM) demulsifying agent T1001 or LZ5957 and 0.2-0.3% of triazole derivative, thiadiazole derivative, N-salicylidene ethylamine, N, N'-bis(salicylidene)ethylenediamine, N, N'-bis(salicylidene)propylene diamine or ethylenediamine tetraacetic acid. A preparation method of the ester type fire-resistant hydraulic fluid comprises the following steps of sufficiently and evenly stirring various materials at room temperature according to a formula, and then filtering. The ester type fire-resistant hydraulic fluid has the beneficial effects that the high temperature use performance of the product is greatly improved, the service life of a hydraulic system and the oil changing period of oils are prolonged, and the ester type fire-resistant hydraulic fluid has a good flame-retardant effect and is safe to use. The preparation method has the advantages that operation is convenient, technology and equipment are simple, energy consumption is low, cost is low, and the like.
Owner:ANLU AOSEN PETROCHEM

High-expansion fireproof sealant and preparation thereof

The invention discloses high intumescent fire stopping mastic and a method for preparing the same. The mastic is prepared by taking acrylate emulsion (or elastic styrene-acrylate emulsion), polybutene (or polyisobutylene), glycol, emulsifying agent and tritolyl phosphate as base materials with addition of certain auxiliary materials. The preparation method is as follows: the base materials are added into a reaction kettle according to certain mass portion, stirred, slowly heated and insulated for a period of time, and transferred into a colloid stirrer; auxiliary materials such as ammonium polyphosphates, flame-retarding aluminum hydroxide, flame-retarding zinc borates, calcium carbonates, expandable graphite, iron oxide red and glass fibers are gradually added into the mixture under the condition of stirring; and the process of stirring is continued until a colloid is uniform. The fire stopping mastic prepared by adoption of the method can be quickly carbonized and expanded to 5 to 8 times of the prior volume in case of fire, and can not fall off; the strength and the heat insulation after solidification are good, and the fire resistance is very good; and the adhesion is strong and the elasticity is good. The high intumescent fire stopping mastic and the method are particularly suitable for fire compartmentation of various penetrating penetration assemblies such as cables, cable bridges, pipes and so on.
Owner:NUCLEAR POWER INSTITUTE OF CHINA

Polypropylene hollow fiber ultrafiltration membrane coated with polymer composite coating

The invention relates to a polypropylene hollow fiber ultrafiltration membrane coated with a polymer composite coating. The polypropylene hollow fiber ultrafiltration membrane comprises a water inlet surface and a water outlet surface which are respectively coated with a coating; the coating on the water inlet surface comprises the following raw materials: tricresyl phosphate, dioctyl phthalate, a modified polysiloxane polymer, polyether-ether-ketone (PEEK), methenamine and the like; and the coating on the water outlet surface comprises the following raw materials: allyl polyoxy alkyl epoxy ether, pentaerythritol, polyethylene glycol lauric acid diester, polyoxyethylene alkylamine, nano silver and the like. The polypropylene hollow fiber ultrafiltration membrane is capable of increasing the retention rate for macromolecular organic matter and emulsified oil, so that the COD removal rate of sewage is greatly increased, the electrostatic effect on the surface of the membrane is changed, the adsorption for contaminants of the surface of the membrane is prevented, the membrane can be continuously used for a long time under the condition of high membrane flux, and the service life of the membrane is prolonged. The addition of the nano silver effectively improves the antibacterial mildew properties of the membrane.
Owner:广州市纳清环保科技有限公司

PET (polyethylene glycol terephthalate) fiber/polyacrylonitrile fiber composite sound absorbing cotton and preparation method of PET fiber/polyacrylonitrile fiber composite sound absorbing cotton

The invention discloses PET (polyethylene glycol terephthalate) fiber/polyacrylonitrile fiber composite sound absorbing cotton, which is prepared from the following ingredients in parts by weight: 70 to 80 parts of PET fibers, 40 to 50 parts of polyacrylonitrile fibers, 10 to 15 parts of emulsifying agents OP-20, 5 to 10 parts of peregal O-15, 80 to 100 parts of PP (propene polymer), 30 to 40 parts of SEBS (styrene ethylene butylene styrene), 15 to 20 parts of calcined clay, 10 to 15 parts of modified kieselguhr, 2 to 3 parts of stearic acid, 5 to 8 parts of diisooctyl phthalate, 4 to 6 parts of tricresyl phosphate, 2 to 3 parts of polyethylene wax, 1 to 2 parts of vinyl (beta-methoxyethoxy) trisilane, 2 to 3 parts of calcium stearate, 1 to 2 parts of dimethyl dimercapto isooctyl acetate tin, 0.5 to 1.5 parts of anti-aging agents ODA (octyl decyl adipate) and 1 to 2 parts of antioxidants 1035. The sound absorbing cotton prepared by the invention has the advantages that the appearance evenness is good, the thickness is uniform, the hand feeling is soft, the product bonding degree is good, the tensile performance is high, the sound absorbing performance is excellent, the flame retardant effect is good, and the like.
Owner:芜湖跃飞新型吸音材料股份有限公司

Ash-free anti-wear hydraulic lubricating oil composition and preparation method thereof

The invention discloses an ash-free anti-wear hydraulic lubricating oil composition and a preparation method thereof. The ash-free anti-wear hydraulic lubricating oil composition consists of the following components in percentage by weight: 0.1-5.0% of an extreme pressure anti-wear reagent, 0.05-2.00% of an antioxidant, 0.01-0.5% of a metal deactivating agent, 0.05-0.1% of an anti-rusting agent, 0.03-0.06% of an emulsification resistant agent, 0.001-0.01% of an anti-foam agent, 0.2-6.5% of a viscosity index improver and 92.0-98.6% of basic oil, wherein the extreme pressure anti-wear reagent issulfurized isobutylene, di-n-butyl phosphate, tricresyl phosphate, phosphorothioate and amino salt derivatives thereof, phosphate and amino salt derivatives thereof, or a mixture of any combination of the components. The preparation method comprises the following steps: putting the antioxidant, the extreme pressure anti-wear reagent, the anti-rusting agent, the metal deactivating agent, the anti-foam agent, the emulsification resistant agent and the viscosity index improver respectively into the basic oil, or mixing additives to prepare a concentrated substance, heating and mixing the concentrated substance with the basic oil at a mixing temperature between 40-90 DEG C for 1-6 hours, and filtering. The ash-free anti-wear hydraulic lubricating oil composition disclosed by the invention isexcellent in high-temperature oxidation resistance, high-pressure wearing resistance and extreme pressure resistance, and specification indexes of GB11118.1 and ISO11158-2009 can be met.
Owner:NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI +1

Formula of environment-friendly flame-retardant chloroprene rubber

ActiveCN101812193APrevent thermal decompositionInhibition of spreadQuinoxalineZinc borate
The invention relates to the formula of environment-friendly flame-retardant chloroprene rubber. The flame-retardant chloroprene rubber, according to the formula thereof, comprises the following components by weight part: 100 parts of chloroprene rubber, 1 to 4 parts of hexamethyl-quinoxaline-2,3-dithioformate, 1 to 2 parts of DM as accelerator, 3 to 10 parts of zinc oxide, 3 to 10 parts of magnesium oxide, 1 to 2 parts of 4010NA as anti-ager, 0.5 to 2 parts of paraffin, 20 to 40 parts of FEF (fast-extruding furnace) carbon black (N550), 30 to 40 parts of kaolin, 30 to 50 parts of aluminum hydroxide, 5 to 15 parts of zinc borate, 10 to 20 parts of FR-808A and 5 to 15 parts of tricresyl phosphate. According to the comparative analysis on the performance of the chloroprene formula using halogen-containing flame retardant and the chloroprene rubber formula using halogen-free flame retardant, the performance of the formula using the halogen-free flame retardant in the invention can fully satisfy the requirements of standards, thus substituting for the chloroprene formula using the halogen-containing flame retardant; and based on the chloroprene rubber formula, the invention can meet the requirements of the flame-retardant application, and the materials of the formula are environment friendly and safe for human bodies.
Owner:TIANJIN PENGYI GRP CO LTD

Determination method for content of tricresyl phosphate flame retardants in rubber parts of electronic and electrical products

The invention discloses a method for detecting the content of a triocresyl phosphate fire retardant of a rubber part of an electrical or electronic product. The method comprises the following steps of: (1) sample preparation; (2) extraction of the triocresyl phosphate fire retardant: adding heavy metal powder into the sample, uniformly mixing and performing accelerated solvent extraction so as to obtain extract; (3) extract purification: uniformly mixing the extract and an interior label, transferring to a small solid phase extraction column, eluting by using a mixed solvent, collecting and concentrating eluent so as to obtain the purified extract; and (4) measurment of the triocresyl phosphate fire retardant: measuring the purified extract and the triocresyl phosphate mixed standard solution containing the interior label by using a gas chromatography-mass spectrometer, and performing data processing and quantitative analysis to obtain the content of the triocresyl phosphate fire retardant. By the method, interference impurities in the rubber can be eliminated effectively, triocresyl phosphate can be extracted fully, the purification degree is high, the detection sensitivity is high and the sample measurement cost is low.
Owner:广东德威检验认证有限公司

Heat-resistant and oil-resistant rubber hose

The invention provides a heat-resistant and oil-resistant rubber hose. The heat-resistant and oil-resistant rubber hose comprises an outer rubber layer, an inner rubber layer and a framework layer located between the outer rubber layer and the inner rubber layer. The inner rubber layer is composed of, by mass, 100 parts of hydrogenated acrylonitrile butadiene rubber, 30-40 parts of semi-reinforcing carbon black, 20-30 parts of fast extruding furnace black, 15 parts of white carbon black, 5-10 parts of tricresyl phosphate, 0.5-1.5 parts of stearic acid, 1-3 parts of 2,2'-diurethane dimethacrylate-(4-methyl-6-tert-butylphenol), 1-2 parts of polyethylene glycol 4000, 4-6 parts of activated zinc oxide, 0.5-2 parts of accelerant DM, 0.8 part of vulcanizing agent dicumyl peroxide, 1 part of sulphur, 2-3 parts of assistant crosslinker triallylisocyanurate. The heat-resistant and oil-resistant rubber hose further comprises a middle rubber layer. The middle rubber layer is composed of, by mass, 90-110 parts of rubber, 0.5-1.5 parts of active agent, 10-12 parts of vulcanizing agent, 1-2 parts of accelerant, 32-48 parts of reinforcing agent, 16-24 parts of plasticizer, 2-3 parts of anti-aging agent and 20-30 parts of binding agent. By the adoption of the optimum rubber material formula, the heat-resistant and oil-resistant rubber hose has the excellent advantage of being resistant to high temperature, oil, pressure and deflection.
Owner:青岛橡六胶管有限公司

Energy-saving engineering machinery hydraulic oil with high viscosity index and ultralow temperature

The invention discloses energy-saving engineering machinery hydraulic oil with a high viscosity index and an ultralow temperature. The energy-saving engineering machinery hydraulic oil is composed of, by weight, 0.1-1 part of tricresyl phosphate, 0.5-1.5 parts of an antiwear agent, 3-7 parts of benzene triazole fatty amine, 1-5 parts of ethylene glycol oleate, 70-90 parts of viscosity index improvers, 1-3 parts of purification dispersant, 1-3 parts of antioxygen, 2-4 parts of 4, 4'-di-iso-octyldiphenylamine, 3-9 parts of pour point depressant, 0.01-0.05 part of an anti-foaming agent and 800-1000 parts of base oil. According to the energy-saving engineering machinery hydraulic oil, an ash-free extreme pressure antiwear additive agent is adopted for complex formulation, applicability is wider, abrasion resistance is better, efficiency is higher, and lubrication of a plunger pump of a hydraulic transmission system with high power and high pressure can be effectively met; preferably, compatibility between an oiliness agent and the antiwear agent with the base oil is good, and lubrication guarantee can be provided in time in different work stages; equipment can operate steadily, pressure transfer is even, frication is lowered, abrasion is reduced, temperature rise is low, heat dissipation is high in speed, the power loss is lowered, energy consumption is saved, and the oil exchange cycle is prolonged.
Owner:北京雅士科莱恩石油化工有限公司

Preparation and application of isobutylcyanoacrylate medical adhesive

The present invention provides a medical adhesive which has the advantages of short adhesion time, good flexibility of adhesive layer, sufficient hemostasis, high adhesion strength and short break-off time. The invention is characterized in that the medical adhesive is manufactured by the following inventive formula and technique, wherein the inventive formula is as follows: 30-75 parts of alpha-isobutyl cyanoacetate by weight, 3.5-23.5 parts of formaldehyde by weight, 0.15-1.55 parts of polymerization inhibitor by weight, 0.1-15.5 parts of pH adjusting agent by weight, and 0.5-19.3 parts of stabilizing agent. The inventive technique comprises the following steps: executing polycondensation reaction with alpha-isobutyl cyanoacetate, formaldehyde and hexa-hydrogen pyridine as pH adjusting agent, executing suction-filtering to the product after water cleaning, and vacuum drying; adding the material which is executed with vacuum drying in a fractionating flask, then adding phosphoric acid as pH adjusting agent, tricresyl phosphate as stabilizing agent and hydrochinone as polymerization inhibitor, mixing to uniform, installing a capillary tube of SO2 protective gas, starting depolymerization, distilling, collecting the component with constant boiling point, and packaging or pouring-in. The medical adhesive can be applied to the aspects of medicine, health-care, beauty treatment, daily life, etc.
Owner:孙丽华
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