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1524 results about "Ultra high performance" patented technology

Method for detecting unknown poison by establishing liquid chromatography-mass spectrometry database

The invention relates to a method for detecting unknown poison by establishing a liquid chromatography-mass spectrometry database, in particular to a method used for detecting unknown poison during food poisoning. According to the method, firstly, an ultra-high performance liquid chromatography-quadrupole-time-of-flight mass spectrometry method is used for establishing a liquid chromatography-mass spectrometry database of common poison; then, a sample is subjected to supersonic extraction with methyl alcohol or acetonitrile, liquid chromatography-mass spectrometry data of an extracting solution are measured similarly and searched and compared in the liquid chromatogram-mass spectrometry database of common poison according to the retention time of the sample and mass spectrometry fragments, and the variety of the unknown poison in the sample is judged; and the unknown poisoning sample is simply extracted and directly measured and compared, and a screening result can be acquired in one hour, so that the detecting and treating time of the sample is greatly shortened, the detecting efficiency is improved, and technical support is provided for related events such as food poisoning and the like caused by unknown reasons.
Owner:BEIJING CENT FOR DISEASE PREVENTION & CONTROL

Ultra-high performance wearable high-manganese steel and producing method thereof

ActiveCN101191180AReduced tendency to overcoolImprove toughnessRheniumManganese
The invention provides ultra-high-performance abrasion-resistant high manganese steel and the production method thereof. The chemical compositions of the steel are that: carbon of 1.00 to 1.50 percent; manganese of 10.5 to 20.0 percent; silicon of 0.30 to 0.80 percent; chromium of 1.3 to 2.8 percent; sulfur of less than or equal to 0.040 percent; phosphorus of less than or equal to 0.070 percent; titanium of 0.06 to 0.20 percent; vanadium of 0.10 to 0.40 percent; boron of 0.002 to 0.010 percent; magnesium of 0.06 to 0.3 percent; rhenium of 0.08 to 0.4 percent; nitrogen of 0.05 to 0.2 percent; the remainder is iron. The production method is that: when the molten steel temperature reaches between 1500 and 1550 DEG C, the nitrogen and the calcium are added within 5 minutes after the molten steel is reduced, the aluminum is inserted and the vanadium (2 to 5 kg / t) and the titanium (4 to 10 kg / t) are added within 10 minutes before steel tapping, the rare earth magnesium (2 to 6 kg / t) is added into a tank when one-third steel is tapped, the rare earth silicon (1 to 4 kg / t) is added into the tank when one-second steel is tapped, the boron (0.1 to 0.3 kg / t) is added into the tank when two-third steel is tapped, the casting temperature of the molten steel is controlled between 1430 and 1460 DEG C. The invention adopts new alloying process, improves the abrasion- resistant performance and the comprehensive mechanical performance of the high manganese steel.
Owner:ANSTEEL GRP MINING CO LTD

Ultra-high performance concrete with micro-expansion and compensation shrinkage and preparation method thereof

The invention belongs to the field of building materials, and especially relates to ultra-high performance concrete with micro-expansion and compensation shrinkage and a preparation method thereof. Raw materials include, by weight, the following components: 1 part of cement, 0.05-0.2 part of fly ash, 0.2-0.5 part of silica fume, 0.1-0.25 part of mineral powder, 0.05-0.2 part of quartz powder, 0.9-1.2 parts of quartz sand, 0.04-0.2 part of an expanding agent, 0.01-0.03 part of a water reducing agent, and 0.01-0.03 part of an expansion promotion reinforcing agent. A mixing amount of super absorbent resin is 0.4%-0.8% of a cementing material; a volume mixing amount of steel fiber is 1%-3% of a total volume of the concrete; the water-to-binder ratio is 0.16-0.22; and the compressive strength is 100-160 MPa. The ultra-high performance concrete with the micro-expansion and the compensation shrinkage has the characteristics of micro-expansion, high strength, high toughness, excellent workingperformance, and the like, and solves the problem that the expanding agent is difficult to produce effective expansion in the ultra-high performance concrete with a low water-to-binder ratio, and so,the risk of early shrinkage cracking of the ultra-high performance concrete is reduced, and the ultra-high performance concrete can maintain the micro-expansion for a long time.
Owner:HUNAN UNIV

Steel-super high performance concrete composite beam based on ribbed plate type bridge deck and construction method

The invention discloses a steel-super high performance concrete composite beam based on a ribbed plate type bridge deck and a construction method. The construction method includes the following steps that step1, steel beams are machined, manufactured and installed; step2, shearing force connecting parts are welded; step3, the super high performance concrete bridge deck is constructed; step4, a guardrail or an anti-collision wall is constructed; step5, bridge deck pavement is constructed, wherein the super high performance concrete bridge deck and the steel beams are fixed through the shearing force connecting parts, the cross section or/and the longitudinal section of the super high performance concrete bridge deck is/are of a ribbed plate structure, and pre-stressed reinforcements can be arranged on a longitudinal rib region or/and a transverse rib region. The composite beam is reasonable in stress, high in strength and capable of substantially reducing the structure dead weight, effectively avoiding defects at a hogging moment region of a composite continuous beam and bringing tensile strength, compressive strength and high durability of super high performance concrete into full play; the composite beam has the advantages of being small in building height, high in rigidity, small in dead weight, good in durability, crack resistance and fatigue resistance and the like, and has great practical value and good economic benefits.
Owner:FUZHOU UNIV

Ultra-high performance hybrid fiber concrete shield segment and preparation method thereof

The invention discloses an ultra-high performance hybrid fiber concrete shield segment and a preparation method thereof. The ultra-high performance hybrid fiber concrete shield segment is of a reinforced concrete structure which consists of a steel skeleton and concrete, wherein the reinforcement ratio of used main reinforcements is 0.5%-1.0%, the distances of the main reinforcements are 150-300mm, the grades of steel reinforcements are not less than three, the smallest steel reinforcement distance of distributed reinforcements is 400mm, the biggest steel reinforcement distance of used distributed reinforcements is 2000mm, and the grades of the steel reinforcements are not less than two. The ultra-high performance hybrid fiber concrete shield segment is made from ultra-high performance hybrid fiber concrete, and comprises cementitious materials, sands, crushed stones, steel fibers, synthetic fibers, water reducer, defoamer and water. The ultra-high performance hybrid fiber concrete shield segment is less in dosage of the steel reinforcements and concrete and high in early strength, can prevent steam preservation, reduces energy consumption, and is green, energy-saving and environmentally friendly. The ultra-high performance hybrid fiber concrete shield segment is strong in anti-burst performance when having a fire, excellent in toughness and crack resistance and excellent in durability, enables edge joints not to easily break, and overcomes the defects of traditional segments.
Owner:CHINA STATE CONSTRUCTION ENGINEERING CORPORATION +2

Method for analyzing and detecting a plurality of endocrine disruptors in food

The invention belongs to the field of food inspection, relates to an assay determination method for endocrine disruptors in food, and particularly relates to a method for analyzing and determining a plurality of endocrine disruptors in milk powder and liquid milk. The method comprises the steps of dissolving a sample with water, adding an organic solvent mixable with water, extracting a to-be-detected material by ultrasonic, adding a sodium salt to make the organic solvent separated from a water phase to realize liquid-liquid extraction, taking an organic solvent containing quantitative to-be-detected material, purifying by extraction with a solid phase filled with C 18 materials, deriving by dansyl chloride, and analyzing and detecting four types of 26 endocrine disruptors in the food by using ultra-high performance liquid chromatography-quadrupole-time of flight-mass spectrometry at the same time. The method can overcome the disadvantages that a conventional technology cannot realize simultaneous analysis of the plurality of the endocrine disruptors in the food by once chromatographic sample injection, can increase sensitivity of the quadrupole-time of the flight-mass spectrometry, and realize accurate analysis of the endocrine disruptors in the food by using the quadrupole-time of the flight-mass spectrometry.
Owner:FUDAN UNIV

Method for simultaneously detecting a plurality of mycotoxins in sesame paste

The invention relates to a method for detecting a plurality of mycotoxins in a sesame paste, and particularly relates to a method which carries out pre-treatment by an optimized dispersive solid-phase extraction method (QuEChERS), and simultaneously detects 26 mycotoxins in sesame paste by ultra-high performance liquid chromatography-tandem mass spectrometry (UHPLC-MS / MS). The method particularly comprises: extracting a sample twice with acid-containing acetonitrile-aqueous solutions with different concentrations, adding magnesium sulfate and sodium chloride into the sample extract for salting out, performing centrifugation, adding n-hexane into the obtained supernatant, performing vortex oscillation and degreasing, purifying the product with C18 and magnesium sulfate, performing vacuum concentration, dissolving the residues again with methanol and water in order to obtain a sample analytic solution, and detecting the solution by a multi-reaction monitoring mode of ultra-high performance liquid chromatography-tandem mass spectrometry. The method improves the detection efficiency, saves detection cost, is high in sensitivity, high in repeatability, and high in adding standard recovery rate, and can be extended to detection of other samples with a high grease content.
Owner:PEOPLES REPUBLIC OF CHINA BEIJING ENTRY EXIT INSPECTION & QUARANTINE BUREAU

4D printing method and application of titanium-nickel shape memory alloy

The invention belongs to the technical field of preparation of shape memory alloys, and discloses a 4D printing method and application of a titanium-nickel shape memory alloy. Pure titanium and pure nickel are matched and smelted, and titanium-nickel alloy bars are obtained; then alloy powder is prepared through a rotating electrode atomization method, the powder is screened, and titanium-nickel alloy powder with the grain size of 15 micrometers to 53 micrometers is obtained; and the obtained titanium-nickel alloy powder is placed in a discharge plasma assisted ball mill to be subjected to discharge treatment, the powder is subjected to surface modification, and finally the titanium-nickel shape memory alloy is formed by means of SLM forming. The phase composition of the obtained titanium-nickel shape memory alloy is composed of a B2 austenite phase of a CsC1 type structure, a B19' Martensite phase of a monocline structure and a Ti2Ni precipitated phase. The microstructure comprises nano-sized afterbirth-like crystals and micro dendrite, and the afterbirth-like crystals and the dendrite are alternately distributed in a layered manner. The advantages of being unique in organizationstructure, nearly fully dense and ultrahigh in performance are achieved.
Owner:SOUTH CHINA UNIV OF TECH

Method for detecting blood sugar-lowering and blood pressure-lowering drugs in blood by ultra high performance liquid-mass spectrometry

ActiveCN104133006AMeet the requirements of actual testingThe test result is accurateComponent separationRetention timeBlood sugar
The invention provides a method for detecting 31 common blood pressure-lowering and blood sugar-lowering drugs in blood by an ultra high performance liquid-mass spectrometry, and is characterized in that the method comprises the following steps: (1) confirmation of detected target compounds; (2) sample processing: processing a sample by an organic solvent protein-deposition method; (3) primary screening detection: carrying out primary screening detection by a multiple reaction monitoring (MRM) mode of the ultra high performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS) in different periods of time; (4) reexamining of the sample which is positive by the primary screening detection in the step (3): after treating and concentrating the sample which is positive by the screening detection, carrying out UPLC-MS/MS detection; and optionally, (5) reexamining of the sample which is positive by the reexamining detection in the step (4): reexamining by a high performance liquid chromatography-high resolution time-of-flight tandem mass spectrometry (HPLC-QTOF). According to a fact that the drugs have different retention time in the set detection conditions, a method for sectional detection is creatively completed. The required time for totally completing the detection of 31 drugs can be within 11 minutes.
Owner:中国民用航空局民用航空医学中心

UPLC-MS/MS method for analyzing four categories and 29 types of restricted veterinary drug residues in animal foodstuff

The invention provides an UPLC-MS/MS method for analyzing four categories and 29 types of restricted veterinary drug residues in animal foodstuff. The method is characterized in that an advanced QuEChERS method is adopted for conducting sample preprocessing, a sample is subjected to McIlvaine buffering liquid-acetonitrile extraction, an extracting solution is subjected to acidification and salting out, a small amount of acetonitrile phase is taken, a C18 and NH2 adsorbing agent is utilized for conducting dispersive solid-phase extraction and purification, after purification liquid is subjected to concentration and volume setting, an ultra-high performance liquid chromatography-tandem mass spectrometer (UPLC-MS/MS) is adopted to conduct detection. The problem that it is difficult for tetracycline class veterinary drug to be extracted and purified along with other types of veterinary drugs is solved, meanwhile the sample processing steps are simplified, the UPLC-MS/MS method has the advantages of being efficient, rapid, low in cost, simple and convenient to operate, good in purification effect and high in sensitivity, and the accuracy and precision both meet the requirement of a multi-residue analysis method.
Owner:TIANJIN INSTITUE OF QUALITY STANDARD & TESTING OF AGRICULTUAL PRODS
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