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846 results about "Amorphous phase" patented technology

Process and apparatus for producing metallic glass

A process and an apparatus for producing metallic glass which are capable of producing a bulk amorphous alloy of desired shape, in particular, a bulk amorphous alloy of desired final shape are provided. In the present invention, the molten metal at a temperature above the melting point is selectively cooled at a rate higher than the critical cooling rate, and the product comprises single amorphous phase which is free from the crystalline phase formed by the development of crystal nuclei through nonuniform nucleation. The present invention is capable of producing the bulk amorphous alloy which is free from casting defects such as cold shuts and which has excellent strength properties in a simple process at a high reproducibility. Accordingly, a bulk metallic glass of desired shape is produced by filling a metal material in a hearth; melting the metal material by using a high-energy heat source which is capable of melting the metal material; pressing the molten metal at a temperature above the melting point of the metal material to deform the molten metal into the desired shape by at least one of compressive stress and shear stress at a temperature above the melting point, while avoiding the surfaces of the molten metal cooled to a temperature below the melting point of the metal material from meeting with each other during the pressing; and cooling the molten metal at a cooling rate higher than the critical cooling rate of the metal material simultaneously with or after the deformation to produce the bulk metallic glass of desired form.
Owner:MAKABE GIKEN

High saturation magnetization intensity Fe-based nanocrystalline magnetically soft alloy material and preparation method thereof

The invention relates to a high saturation magnetization intensity Fe-based nanocrystalline magnetically soft alloy material and a preparation method thereof. The high saturation magnetization intensity Fe-based nanocrystalline magnetically soft alloy material is a FexSiyBzPaCub alloy comprising ferrum, silicon, boron, phosphorus and copper, wherein x, y, z, a and b in the formula respectively represent atom percentage content of each corresponding component, x=70-90%, y=1-15%, z=1-20 %, a=1-20% and b=0.1-1%, and x+y+z+a+b=100%; the microstructure of the Fe-based nanocrystalline magnetically soft alloy is as follows: a body-centered cubic Alpha-Fe(Si) nanocrystalline phase with the size of 1-35nm and an amorphous phase rich in phosphorus and boron coexist, and the amorphous phase is the basic phase. The preparation method comprises steps of: preparing proportioned raw materials into an alloy ingot, preparing into amorphous alloy and carrying out other procedures to obtain the high saturation magnetization intensity Fe-based nanocrystalline magnetically soft alloy. The invention can greatly enhance the saturation magnetization intensity of the nanocrystalline magnetically soft alloy, maintain lower coercivity and effectively reduce cost of raw materials simultaneously.
Owner:朗峰新材料启东有限公司

Device and method for continuous block metal glass shaping

InactiveCN101543885ASolve the vacuum problemIncrease cooling intensityMetallic materialsPressure difference
The invention relates to a device and method for continuous block metal glass shaping, belonging to the technical field of metal material preparation. A heat insulating ring is arranged between a graphite casting mould and a water cooling copper mould which are arranged in a first vacuum chamber, an air cooler is arranged in a second vacuum chamber, and a traction rod enters the graphite casting mould and horizontally moves by a traction device. The method uses the graphite casting mould and the water cooling copper mould for primary main cooling and the air cooling mode for secondary auxiliary cooling, and the two vacuum chambers have a certain air-pressure difference. The device and the method have a high cooling speed, satisfy the requirements of the amorphous phase change of the block metal glass material. The shaping pressure of a metal melting body can be easily controlled, and the good shaping performance of the metal melting body is ensured by adjusting the pressure in the vacuum chambers. The metal passes through the graphite casting mould in a liquid state and is solidified in the water cooling copper mould, and the casting graphite casting mould has long service. The composite casting mould and the traction device have exchangeability to be convenient for realizing the continuous shaping of rod wires, boards, pipes and abnormal-shaped materials of different section sizes.
Owner:江苏苏州洲盛非晶科技有限公司

Process and apparatus for producing metallic glass

A process and an apparatus for producing metallic glass which are capable of producing a bulk amorphous alloy of desired shape, in particular, a bulk amorphous alloy of desired final shape are provided. In the present invention, the molten metal at a temperature above the melting point is selectively cooled at a rate higher than the critical cooling rate, and the product comprises single amorphous phase which is free from the crystalline phase formed by the development of crystal nuclei through nonuniform nucleation. The present invention is capable of producing the bulk amorphous alloy which is free from casting defects such as cold shuts and which has excellent strength properties in a simple process at a high reproducibility. Accordingly, a bulk metallic glass of desired shape is produced by filling a metal material in a hearth; melting the metal material by using a high-energy heat source which is capable of melting the metal material; pressing the molten metal at a temperature above the melting point of the metal material to deform the molten metal into the desired shape by at least one of compressive stress and shear stress at a temperature above the melting point, while avoiding the surfaces of the molten metal cooled to a temperature below the melting point of the metal material from meeting with each other during the pressing; and cooling the molten metal at a cooling rate higher than the critical cooling rate of the metal material simultaneously with or after the deformation to produce the bulk metallic glass of desired form.
Owner:MAKABE GIKEN

Ternary and multi-nary iron-based bulk glassy alloys and nanocrystalline alloys

InactiveUS20050263216A1High glass forming abilityIncreased electrical resistivityMagnetic materialsAmorphous phaseAtomic radius
Disclosed in this invention is a family of ternary and multi-nary iron-based new compositions of bulk metallic glasses which possess promising soft magnetic properties, and the composition selection rules that lead to the design of such new compositions. The embodiment alloys are represented by the formula MaXbZc, where M represents at least one of ferromagnetic elements such as iron and may partly be replaced by some other substitute elements; X is an element or combinations of elements selected from those with atomic radius at least 130% that of iron and in the mean time is able to form an M-rich eutectic; and Z is an element or combinations of elements selected from semi-metallic or non-metallic elements with atomic radius smaller than 86% that of iron and in the meantime is able to form an M-Z eutectic; a, b, c are the atomic percentage of M, X, Z, respectively, and a+b+c=100%. When 1%<b<15% and 10%<c<39%, the alloys show a bulk glass forming ability to cast amorphous ribbons/sheets at least 0.1 mm in thickness. When 3%<b<10% and 18%<c<30%, the alloys show a bulk glass forming ability to cast amorphous rods at least 1 mm in diameter. The amorphous phase of these as-cast sheets/rods is at least 95% by volume. This invention also discloses the existence of nano-crystalline phase outside of the outer regime of the bulk glass forming region mentioned above.
Owner:NATIONAL TSING HUA UNIVERSITY

Active belite-sulphate aluminum cement clinker and preparation method for active belite-sulphate aluminum cement clinker

The invention discloses active belite-sulphate aluminum cement clinker, which comprises the following mineral compositions in weight percentage: 25-30 percent of beta-type C2S, 25-30 percent of a-type C2S, 28-40 percent of C4A3S`, 4-12 percent of C4AF and 4-8 percent of amorphous-phase substance. The control of different forms and the change of number of the C2S in the clinker are controlled mainly through special setting on clinker ingredient rate values. The invention also discloses a preparation method for the active belite-sulphate aluminum cement clinker. Compared with traditional common silicate cement clinker, the active belite-sulphate aluminum cement clinker has the advantages that more industrial solid waste residues are used in raw materials by the active belite-sulphate aluminum cement clinker, and thereby, the production cost is reduced, the use proportion of limestone is greatly reduced, and the carbon dioxide emission in clinker production is obviously reduced. Under the condition that the water demand and the setting time of the obtained clinker are basically the same as that of the common silicate cement clinker, the strength of the obtained clinker is superior to that of the common silicate cement clinker.
Owner:TIANJIN CEMENT IND DESIGN & RES INST +1
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