The invention belongs to the technical field of magnetic materials, in particular relates to a preparation method of MnZn ferrite in a magnetic field. The method comprises the following steps: by using a phase conversion method, placing a certain amount of mixed solution of Fe, Mn and Zn metal ions in a 0-6T magnetic field; under the stirring of nitrogen at the speed of 160-260ml/min, controlling the pH value to 9-10, heating to 95 DEG C, and insulating for 3-5 hours; then filtering, washing, and drying at the temperature of 70-90 DGE C, so as to obtain nano crystal MnZn ferrite powder, wherein the obtained powder is a single-phase MnZn ferrite particle and is of a typical spinel structure, the grain size is about 7-11 nanometers, and super paramagnetism is shown within a 40-300K temperature range. The obtained MnZn ferrite material has the advantages that magnetic conductivity is large, frequency characteristic is good, saturation induction density is greatly improved on the original basis, and obstruction temperature is greatly reduced.