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Certain polyester compositions which comprise cyclohexanedimethanol, moderate cyclobutanediol, cyclohexanedimethanol, and high trans cyclohexanedicarboxylic acid

Described as one aspect of the invention are polyester compositions A polyester composition comprising at least one polyester which comprises:
    • (A) a dicarboxylic acid component comprising:
      • i) 70 to 100 mole % of cyclohexanedicarboxylic acid residues or an ester thereof comprising:
        • (a) 80 to 99 mole % trans-cyclohexanedicarboxylic acid residues or an ester thereof; and
        • (b) 1 to 20 mole % cis-cyclohexanedicarboxylic acid residues or an ester thereof;
      • ii) 0 to 30 mole % of aliphatic dicarboxylic acid residues, other than cyclohexanedicarboxylic acid residues, having up to 16 carbon atoms or esters thereof, other than cyclohexanedicarboxylic acid residues; and
      • iii) 0 to 10 mole % of aromatic dicarboxylic acid residues having up to 20 carbon atoms; and
    • (B) a glycol component comprising:
      • i) 5 to 35 mole % of 2,2,4,4-tetramethyl-1,3-cyclobutanediol residues; and
      • ii) 65 to 95 mole % of 1,4-cyclohexanedimethanol residues, 1,3-cyclohexanedimethanol residues, 1,2-cyclohexanedimethanol residues or esters thereof or mixtures thereof,
wherein the total mole % of said dicarboxylic acid component is equal to 100 mole %;
the total mole % of said glycol component is equal to 100 mole %;
wherein the inherent viscosity of said polyester is from 0.35 to 1.2 dL/g as determined in 60/40 (wt/wt) phenol/tetrachloroethane at a concentration of 0.5 g/100 ml at 25° C.; and wherein said polyester has a Tg of from 66 to 120° C. The polyesters may be manufactured into articles.

Composite phase-change energy storage material for microcapsule and preparation method thereof

InactiveCN101824307ANo leaksPlay the role of self-control temperature controlHeat-exchange elementsMicroballoon preparationCrack resistanceSolvent
The invention discloses a composite phase-change energy storage material for microcapsules and a preparation method thereof. The coating of the microcapsule is made of silicon dioxide, and the core of the microcapsule is made of a phase-change energy storage material, wherein the phase-change energy storage material is a paraffin organic solid-liquid phase-change energy storage material. 0.2 to 0.5 wt.% of dispersed emulsifier, 52.5 to 62.5 wt.% of solvent water, 18.75 to 31.5 wt.% of phase-change energy storage material and 15.5 to 18.75 wt.% of inorganic silica source are matched and put into a reactor for stirring for 5 to 8 hours; the mixture is uniformly dispersed and emulsified at the temperature 3 to 8 DEG C higher than that for solid-liquid phase change; hydrochloric acid aqueous solution catalyst with the pH value of 0.93 to 4.07 or sodium hydroxide aqueous solution catalyst with the pH value of 8.0 to 12.0 is added into the emulsion; the reacting solution is naturally cooled to room temperature and precipitation solution is obtained; the precipitate is washed with the combination of water and petroleum ether, wherein the mass percent of the petroleum ether is 30 wt.%; then the precipitate is washed with deionized water and is filtered, and the product is naturally aired. The invention improves the technology of phase-change energy storage and conservation, and has the function of automatic temperature regulation, favorable physical and chemical stability, crack resistance, flame retardancy, wear resistance and high thermal conductivity.

Environment-friendly type water-based intaglio ink used for package printing and preparation method thereof

The invention relates to a water-based ink and a preparation method thereof, especially to an environment-friendly type water-based intaglio ink used for package printing and a preparation method thereof. The ink is prepared by mixing epoxy acrylate composite emulsion, pigments, deionized water, ethanol, triethylamine, wax powder, a wetting dispersant, an anti-foaming agent, a levelling agent, a thickening agent and a film forming auxiliary agent according to a certain mass ratio, wherein, the epoxy acrylate composite emulsion is prepared by modifying acrylate emulsion with an epoxy resin and allowing the epoxy resin and acrylate to organically bind together, has the advantages of good adhesion, thermostability, good chemically-resistant properties and the like and has a certain application value when used as a binder for a water-based ink. The water-based intaglio ink in the invention is applicable to package printing in the field of flexible package which mainly relates to packaging of tobacco, liquor, foodstuffs, beverage, medicines, daily chemical articles and the like; the ink is nontoxic, non-combustible and non-explosible, has no pungent smell, accords with environmental protection requirements, and has a very promising prospect.
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