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203 results about "Cyclopentene" patented technology

Cyclopentene is a chemical compound with the formula (CH₂)₃(CH)₂. It is a colorless liquid with a petrol-like odor. It is one of the cycloalkenes. Cyclopentene is produced industrially in large amounts by steam cracking of naphtha. It has however few applications, and thus is mainly used as a component of gasoline.

Process for recycling and regenerating waste lithium iron phosphate positive electrode material by using specific chelating agent

The invention relates to a process for recycling and regenerating a waste lithium iron phosphate positive electrode material by using a specific chelating agent. The method comprises the following steps: carrying out heat treatment on a waste lithium iron phosphate positive electrode material, putting separated waste lithium iron phosphate powder into a ball milling tank, adding organic acid and a chelating agent, and carrying out ball milling; after the ball milling is finished, adding hydrogen peroxide, uniformly stirring and mixing, adjusting the pH value to 2-3 by using nitric acid, and filtering to obtain a filter cake which is iron phosphate; adding saturated sodium carbonate into the filtrate, precipitating, and recovering lithium carbonate; putting the iron phosphate, the lithium carbonate, the iron source, the lithium source and the phosphorus source in the step S3 into a ball mill for ball milling, and performing high-temperature solid-phase sintering after ball milling to obtain a regenerated lithium iron phosphate material; the chelating agent disclosed by the invention is prepared from (9ci)-2-(2-propenyl)-1-cyclopentene-1-carboxylic acid, 2-mercaptobenzimidazole carboxylic acid, an ethylene boric anhydride pyridine complex and potassium persulfate. The regenerated lithium iron phosphate material prepared by the method has excellent electrochemical performance.
Owner:ZHEJIANG SHANGAO NEW ENERGY CO LTD

Preparation method of optical OCA (Optical Clear Adhesive) and application of optical OCA in folding screen of mobile phone

The invention discloses a preparation method of an optical OCA (Optical Clear Adhesive) and application of the optical OCA in a mobile phone folding screen, and relates to the technical field of optical cement, the optical OCA is prepared from the following raw materials in parts by weight: 50 parts of acrylate prepolymers, 2-4 parts of 3-allyl-2-mercapto-3H-quinazoline-4-ketone, 1-3 parts of diallyl disulfide, 1-3 parts of 3-[N, N-dimethyl formamide], 1-3 parts of 2, 3, 5-trimethyl-1, 3-pentanediol monoisobutyronitrile, 1-3 parts of 2, 3, 5-trimethyl-1, 3, 5-trimethyl-1, 3, 5-trimethyl-1, 3 The preparation method comprises the following steps: adding 3-5 parts of N, N-dimethyl-[2-(2-methylpropane-2-enoyloxy) ethyl] ammonium] propane-1-sulfonic acid inner salt, 1-3 parts of allyl succinimido carbonate, 2-4 parts of dicyclopentene methacrylate, 1-3 parts of 1, 3, 5-triacryloyl hexahydro-1, 3, 5-trimethyl-1, 3, 5-trimethyl-1, 3, 5-trimethyl-1, 3, 5-trimethyl-1, 3, 5-trimethyl-1, 3, 5-trimethyl-1, 3, 5-trimethyl-1, 3, 5- The invention relates to a graphene quantum dot photoinitiator which is prepared from the following components in parts by weight: 1-3 parts of 1, 3, 5-triazine, 0.8-1.2 parts of a photoinitiator, 1-3 parts of an aziridine cross-linking agent, 1-3 parts of graphene quantum dots, 0.8-1.2 parts of a coupling agent and 40-50 parts of a diluent. The optical OCA adhesive is high in light transmittance and bonding strength, good in weather resistance and excellent in folding resistance.
Owner:DONGGUAN HANGDA ELECTRONICS

Process for preparing glutaraldehyde through cyclopentene oxidation

A technology for preparing glutaraldehyde through cyclopentene oxidation belongs to the technical field of organic synthesis, glutaraldehyde is prepared through cyclopentene oxidation by adopting a photocatalysis-electrocatalysis synergistic catalyst g-C3N4 / TiO2 (at) Au-Co / N-G. The catalyst is of a unique core-shell structure, is stable in property, promotes an oxygen reduction reaction in a catalysis technology, and has good catalytic activity. The conversion rate of cyclopentene and the selectivity of glutaraldehyde are remarkably improved, and the effect is remarkable.
Owner:PUYANG LIANZHONGXINGYE CHEM IND CO LTD

Tobacco flavor base module, flavor and heated cigarette for improving puff-by-puff consistency

The present invention relates to a tobacco flavor base module, flavor and heated cigarette that improve the consistency of puff by puff, and belongs to the field of tobacco flavors and fragrances. The tobacco flavor base module is composed of the following components: 3,4-dimethyl-1,2-cyclopentanedione slow-release flavor, 3,5-dimethyl-1,2-cyclopentanedione slow-release flavor, methylcyclopentenolone slow-release flavor, ethylcyclopentenolone slow-release flavor, furfural slow-release flavor, 5-methylfurfural slow-release flavor, furfuryl alcohol slow-release flavor, 2-methyltetrahydrofuran-3-one slow-release flavor, 4-hydroxy-2,5-dimethyl-3(2H)furanone slow-release flavor, 3-pentene-2-one slow-release flavor, ethyl maltol slow-release flavor, maltol slow-release flavor, 5-methyl-2-furanmethanol slow-release flavor. The present invention prepares the slow-release flavor by making each component into a slow-release flavor and then mixes it as a tobacco flavor base module, which not only improves the consistency of puff by puff during puffing, but also significantly improves the burnt sweet fragrance characteristics of heated cigarettes.
Owner:ZHENGZHOU TOBACCO RES INST OF CNTC

Catalytic synthesis method of octafluorocyclopentene

The invention belongs to the technical field of octafluorocyclopentene gas preparation, and particularly relates to a catalytic synthesis method of octafluorocyclopentene. The method specifically comprises the following step: under the action of a fluorine-chlorine catalyst, carrying out gas-phase catalytic fluorination reaction on 1-chloroheptafluorocyclopentene and anhydrous hydrogen fluoride at 80-120 DEG C to obtain octafluorocyclopentene. The preparation method of the fluorine-chlorine catalyst comprises the following steps: dissolving metal chloride in water, adding a precipitant, and fully stirring for reaction to obtain slurry; filtering the slurry to remove filtrate to obtain a solid, and washing the solid with deionized water until the solid is neutral; adding aluminum nitrate into the washed solid, fully stirring and drying to obtain a precursor of the catalyst; and performing compression molding on the precursor of the catalyst, roasting, and activating to obtain the fluorine-chlorine catalyst. The method is mild in reaction condition and high in catalytic efficiency.
Owner:PERIC SPECIAL GASES CO LTD

Hollow mesoporous silica supported phosphotungstic acid catalyst and preparation method and application thereof

The invention belongs to the technical field of novel material catalysis, and particularly relates to a hollow mesoporous silica supported phosphotungstic acid catalyst and a preparation method and application thereof. According to the invention, the advantages of high specific surface area and regional effect performance of hollow mesoporous silica and the characteristic of adjustable acidity of vacancy heteropolyacid quaternary ammonium salt are innovatively combined, and the cationic surfactant is loaded on the surface of the hollow mesoporous silica, so that the contact surface of raw materials is effectively increased, efficient conversion of reactants is assisted, and the reaction efficiency is improved. The supported catalyst with efficient catalysis and stable performance is obtained. The catalyst can be used for a reaction for preparing glutaraldehyde through heterogeneous catalysis of cyclopentene oxidation, and the reaction condition is mild. Experiments show that under the catalytic system, the cyclopentene conversion rate can reach 90% or above, the glutaraldehyde selectivity is improved to 75% or above, double improvement of the cyclopentene conversion rate and the glutaraldehyde selectivity is successfully achieved, meanwhile, the advantage that the catalyst is easy to separate is achieved, and an efficient solution is provided for industrial application of synthesis of glutaraldehyde through cyclopentene oxidation.
Owner:GUANGDONG NEWHUAYUE PETROCHEMICAL GROUP STOCK COMPANY

Preparation method and application of catalyst with high-valence tungsten coordination structure

The invention discloses a preparation method and application of a catalyst with a high-valence tungsten coordination structure, and the preparation method of the catalyst comprises the following steps: enabling tungstic acid and hydrogen peroxide with specific concentration and proportion to react at a certain temperature to prepare a peroxy tungstic acid solution; dissolving a polydentate organic ligand capable of forming a stable chelation structure with a tungsten center in an organic solvent, mixing the obtained ligand solution with a peroxytungstic acid solution according to a specific ratio, and carrying out a coordination reaction at a certain temperature until the ligand is completely reacted; and finally, carrying out solid-liquid separation, washing and drying to obtain the high-valence tungsten coordination structure catalyst. The catalyst can be used for a reaction for synthesizing glutaraldehyde through cyclopentene oxidation, under the mild condition, hydrogen peroxide serves as a green oxidizing agent, the conversion rate of cyclopentene reaches 90% or above, the selectivity of glutaraldehyde exceeds 60%, the catalyst is stable in structure and can be recycled for 10 times or above, and the problems that in the prior art, a catalyst is difficult to separate, low in activity, poor in stability and the like are solved; the method has a remarkable industrial application value.
Owner:GUANGDONG NEWHUAYUE PETROCHEMICAL GROUP STOCK COMPANY

Preparation method of alkyl naphthalene and used modified ionic liquid catalyst

The invention relates to a preparation method of alkyl naphthalene and a modified ionic liquid catalyst used in the preparation method. The modified ionic liquid catalyst is obtained by modifying ionic liquid Et3NHCl-AlCl3, Et3NHCl-FeCl3 or Et3NHCl-ZnCl2 with carbon disulfide. The preparation method of the alkyl naphthalene comprises the following steps: enabling naphthalene, cyclopentene and alpha-olefin to react under the action of the modified ionic liquid catalyst in the claim 1, and then performing post-treatment to obtain an alkyl naphthalene product. The carbon disulfide is used for modifying the ionic liquid Et3NHCl-AlCl3, Et3NHCl-FeCl3 or Et3NHCl-ZnCl2, the Lewis acidity of the modified ionic liquid is reduced, and when the modified ionic liquid is used for alkylation reaction of naphthalene, cyclopentene and alpha-olefin, side reactions such as disproportionation can be reduced, and the conversion rate of naphthalene is increased. In addition, the modified ionic liquid catalyst is easier to separate from a reaction mixture, and purification of a target product is facilitated.
Owner:PETROCHINA CO LTD

7-acylhydrazone-cyclopentene pyridine compound, preparation method and application thereof, pharmaceutical composition and application thereof

The invention provides a 7-acylhydrazone-cyclopentene pyridine compound, a preparation method and application thereof, a pharmaceutical composition and application thereof, and relates to the technical field of medicines. According to the invention, an acylhydrazone group with pesticide activity is connected to the 7th site of cyclopentene pyridine to obtain the cyclopentene pyridine compound containing an acylhydrazone active fragment. The 7-acylhydrazone-cyclopentene pyridine compound provided by the invention contains a special Schiff base structure of a-CONHN = C-substructure, and an acylhydrazone group contains oxygen atoms and nitrogen atoms at the same time, can participate in formation of hydrogen bonds in organisms, has certain flexibility, is firmer in combination with receptors, has wide biological activity, and can be used for preparing a novel compound for preparing the 7-acylhydrazone-cyclopentene pyridine compound. And the compound has good application prospects in preparation of insecticides, bactericides, herbicides, anti-HIV drugs, anti-virus drugs or anti-cancer drugs, especially in plant protection, for example, the compound has good application prospects in preparation of insecticides, bactericides, herbicides, anti-virus drugs, anti-HIV drugs or anti-cancer drugs.
Owner:INSTITUTE OF APPLIED CHEMISTRY JIANGXI ACADEMY OF SCIENCES

Hydrofluorocarbon compounds and their use integrated circuit manufacturing processes

Mixtures configured to etch a thin film of an integrated circuit material are disclosed. The mixtures may include a first compound comprising one or more of: A, B, and C; and a second compound comprising one or more of: oxygen, argon, helium, nitrogen, octafluorocyclobutane (C4F8), hexafluorobutadiene (C4F6), carbonyl fluoride (COF2), difluoromethane (CH2F2), trifluoromethane (CHF3), carbon tetrafluoride (CF4), methyl fluoride (CH3F), octafluorocyclopentene (C5F8), 2,3,3,3-tetrafluoropro-l-ene (C3H2F4), 2,3,3,3-tetrafluoropro-l-ene (C3H2F4), hexafluoropropene (C3F6), hexafluorocyclopropane (C3F6), or 1,1,3,3,3-pentafhioropropene (C3HF5).
Owner:VERSUM MATERIALS US LLC

Organic compound and application thereof

The invention discloses an organic compound and application thereof. The organic compound has a structure as shown in a formula I. In the formula I, R1 and R2 represent C1-C15 straight-chain, branched-chain alkyl or alkoxy in a same or different manner at each occurrence, and R1 and R2 represent C1-C15 straight-chain, branched-chain alkyl or alkoxy at each occurrence. Wherein any one or more disconnected-CH2-can be replaced by cyclopropylidene, cyclobutyl, cyclopentadiene or cyclopentadiene,-CH = CH-,-N (Re)-,-O-,-S-,-CO-,-CO-O-and-O-CO-in a form that O-or S-is not connected with each other, and at least one-CH2-in R1 and R2 is replaced by cyclopropylidene, cyclobutyl, cyclopentadiene or cyclopentadiene. The organic compound structure has the characteristics of low melting point, good low-temperature solubility and small normal temperature-high temperature contrast change rate. The liquid crystal material can be uniformly mixed with mixed crystals and completely dissolved at a relatively low processing temperature, and the risk of thermal decomposition or phase change of the liquid crystal material can be reduced. # imgabs0 #
Owner:SHIJIAZHUANG CHENGZHI YONGHUA DISPLAY MATERIALS CO LTD

A detection method for electronic grade octafluorocyclopentene

The invention discloses a detection method for electronic grade octafluorocyclopentene. The pre-cutting (removal) column is about 1m long and is a Hastelloy C-grade column with an inner diameter of about 2mm. Silica Gel with a particle size of 0.18mm-0.25mm is filled therein, or other equivalent chromatographic columns are used. The pre-cutting (removal) sampling method specified in GB / T 28726 is used to determine the contents of hydrogen, oxygen+argon, nitrogen, carbon monoxide, methane and other fluorocarbon compounds in the octafluorocyclopentene. The provisions of GB / T 5832.2 are used to determine the water content in the octafluorocyclopentene. An inductively coupled plasma mass spectrometry method is used to determine the contents of metal elements such as sodium, zinc, chromium, copper, nickel and iron in the octafluorocyclopentene. Finally, the purity of the octafluorocyclopentene is accurately determined by a difference subtraction method.
Owner:ZHEJIANG BRITECH CO LTD

Benzocyclo[1,2]oxaborol-1(3H)-ol derivatives as SHP2 inhibitors, compositions and methods thereof

PendingCN122295347ADiseaseCyclopentene
This invention provides a novel phosphine oxide compound that inhibits SHP2, a composition thereof, a method for preparing the compound, and a method for treating SHP2-related diseases (such as cancer).
Owner:CANWELL BIOTECH LTD

Preparation methods of α-corpse alcohol-based compounds and γ-corpse alcohol-based compounds

The present invention provides a method for preparing an α-cadaverine-based compound of the following general formula (3): wherein R 2 represents a monovalent hydrocarbon group having 1 to 9 carbon atoms, the method comprising: making a 3,5,5-trimethyl-3-cyclopentene compound of the following general formula (1): wherein R 2 As defined above, and X represents a leaving group, and the methylating agent of the following general formula (2): wherein M represents Li, Mg, Z 1 、ZnZ 1 、Cu、CuZ 1 or CuLiZ 1 , and Z 1 represents a halogen atom or a methyl group, undergoing a nucleophilic substitution reaction to form an α-cadaverine-based compound (3). The present invention also provides a method for preparing a γ-cadaverine-based compound of the following general formula (4): wherein R 2 represents a monovalent hydrocarbon group having 1 to 9 carbon atoms, and the method comprises: subjecting the thus obtained α-cadaverine-based compound (3) to positional isomerization reaction at the double bond to form a γ-cadaverine-based compound (4). #imgabs0#
Owner:SHIN ETSU CHEMICAL CO LTD

Preparation method of dichlorohexafluorocyclopentene

The invention provides a preparation method of dichlorohexafluorocyclopentene. Perhalogenated cyclopentene or / and perhalogenated cyclopentadiene is used as a raw material and reacts with HF and Cl2 in a tubular reactor filled with a catalyst to generate dichlorohexafluorocyclopentene, the catalyst needs to be used after being activated for 2-12 h in a mixed gas of HF and F2 at the temperature of 200-600 DEG C, and the catalyst is one or more of molybdenum fluoride, nickel fluoride, cobalt fluoride or molybdenum fluoride; the reaction conditions are as follows: the molar ratio of HF to Cl2 to octachlorocyclopentene or hexachlorocyclopentadiene is (4-10): (1-5): 1, the reaction temperature is 200-500 DEG C, the reaction pressure is 0-2.0 MPa, and the catalyst contact time is 5-90 seconds. According to the method, the reaction process is simple, the needed target object is prepared through one-step gas-phase catalytic fluorination, the method is suitable for large-scale production of dichlorohexafluorocyclopentene, the requirement for equipment is low, and the catalyst activity and stability are high.
Owner:PERIC SPECIAL GASES CO LTD

Slow reaction recyclable epoxy resin system and process for recycling composite materials

PendingCN122037139ACyclopentenePolymer science
A slow-reaction recyclable epoxy resin system for structural composites and a process of recycling the composites made therefrom are disclosed. The system includes an epoxy resin component including: a high purity epoxy resin selected from a high purity bisphenol A epoxy resin, a high purity bisphenol F epoxy resin, and combinations thereof, where the high purity epoxy resin is in a range of from 20 wt% to 95 wt% of the total weight of the cyclopentene resin component; a standard epoxy resin selected from a standard bisphenol A epoxy resin, a standard bisphenol F epoxy resin, and combinations thereof, where the standard epoxy resin is in the range of from 1 wt% to 50 wt% of the total weight of the epoxy resin component; and a curing agent component including a curing agent having at least one cleavage bond selected from a group including an acetal bond, a ketal bond, a formal bond, an orthoester bond, or a siloxy bond. The pot life of the slow-reaction recyclable epoxy resin system is greater than 540 minutes at 25 DEG C.
Owner:ADITYA BIRLA CHEM (THAILAND) LTD

A process for the synthesis of cyclopentanol

The application belongs to the technical field of fine chemical industry, and discloses a method for synthesizing cyclopentanol, which comprises the following steps: (1) taking cyclopentene and water as raw materials, adding a solubilizer, and mixing to obtain a reaction liquid; (2) continuously hydrating the reaction liquid in a fixed bed reactor filled with a cation exchange resin to obtain a reaction product; and (3) distilling and separating the reaction product to obtain cyclopentanol. The synthesis method has the advantages of simple process flow, environmental protection, low energy consumption, excellent product indexes, and long operation cycle of the catalyst. Polyethylene glycol-400 or polypropylene glycol-400 is used as a single solubilizer, and a specific macroporous strong acid cation exchange resin catalyst is used to realize the efficient and high-selectivity hydration reaction of cyclopentene.
Owner:DAN DONG MING ZHU TE ZHONG SHU ZHI YOU XIAN GONG SI

Production method of high-purity cyclopentene

The invention provides a production method of high-purity cyclopentene, and belongs to the technical field of olefin production. According to the method, a crude cyclopentene raw material rich in cyclopentene, cyclopentane and 1, 2-pentadiene is mixed with hydrogen, the mixture is introduced into an adiabatic bubbling bed reactor for a selective hydrogenation reaction, and a catalyst is modified Pd / Al2O3. After hydrogenation reaction liquid is subjected to light component removal and refining, a high-purity cyclopentene product with the content of 99.9% or above and the content of 1, 2-pentadiene being 10 ppm or below is obtained, and the monomer requirement for producing cyclopentene rubber is met.
Owner:TONGLING BEISIMEI TECH CO LTD

A 5-aryl-cyclopentenopyridine compound, a preparation method and application thereof, and a plant protection agent

The application provides a 5-aryl-cyclopentenopyridine compound and a preparation method and application thereof and a plant protection agent, and relates to the technical field of plant protection. The 5-aryl-cyclopentenopyridine compound provided by the application introduces an aromatic group Ar, which can not only increase the stability of the compound molecule, but also interact with amino acids in a receptor protein, thereby improving the biological activity of the compound. The 5-aryl-cyclopentenopyridine compound provided by the application has good antiviral, antibacterial and insecticidal effects, and has a good application prospect in plant protection.
Owner:INSTITUTE OF APPLIED CHEMISTRY JIANGXI ACADEMY OF SCIENCES +1

Composite sweet and fragrant flavor composition and application thereof

The invention provides a compound type sweet and fragrant flavor composition and an application thereof, and the compound type sweet and fragrant flavor composition comprises maltol, ethyl maltol, methyl cyclopentenolone, ethyl cyclopentenolone, 3, 4-dimethyl-1, 2-cyclopentanedione, 4-hydroxy-2, 5-dimethyl-3 (2H) furanone and 3, 5-dimethyl-1, 2-cyclopentanedione, and the compound type sweet and fragrant flavor composition comprises maltol, ethyl maltol, methyl cyclopentenolone, ethyl cyclopentenolone, 3, 4-dimethyl-1, 2-cyclopentanedione, 4-hydroxy-2, 5-dimethyl-3 (2H) furanone and 3, 5-dimethyl-1, 2-cyclopentanedione. The composition disclosed by the invention has obvious sweet aroma style characteristics and aroma intensity, can effectively increase the sweet aroma flavor and sensory style characteristics of cigarettes, makes up for the defects of light cigarette aroma, insufficient smoke concentration and the like of low-coke cigarettes, can restore the natural feeling of the cigarette aroma, ensures good harmony, and has good application prospects. The method has a wide application prospect in the field of tobacco flavor blending, especially in the aspect of low-coke cigarette flavor enhancement compensation.
Owner:CHINA TOBACCO JIANGSU INDAL

Photostimulation responsive rare earth functionalized HOFs material, and preparation method and application thereof

PendingCN120289818AInksBenzoic acidCyclopentene
The invention relates to a photostimulation responsive rare earth functionalized HOFs material as well as a preparation method and application thereof. The material comprises a hydrogen bond organic framework and a luminescent rare earth complex, the mass ratio of the luminous rare earth complex to the hydrogen bond organic framework is 0.1-0.2; the method comprises the following steps: constructing HOFs by using 4, 4 '-((perfluorocyclopent-1-ene-1, 2-diyl) bis (5-methylthiophene-4, 2-diyl)) dibenzoic acid (DAE) as a skeleton trunk and 4, 4', 4 '', 4'' '-methane tetrabenzamidine (TAM); according to the obtained material, DAE is subjected to a ring opening / closing isomerization reaction under ultraviolet / visible light illumination, meanwhile, topological configuration conversion of HOFs is carried out, fluorescence on / off reversible light regulation and control of the rare earth functionalized HOFs are achieved by coating a rare earth complex through the porosity of the HOFs, and the material is further used for multiple times of reciprocating light-operated encryption and decryption of information.
Owner:HEBEI UNIV OF TECH

Method for preparing 4-cyclopentene-1, 3-diketone by one-pot method

The invention provides a method for preparing 4-cyclopentene-1, 3-diketone through a one-pot method, and relates to the technical field of organic synthesis. According to the method for preparing the 4-cyclopentene-1, 3-diketone, provided by the invention, the 4-cyclopentene-1, 3-diketone is obtained by sequentially carrying out dehydration reaction and oxidation reaction on the hexanose in the water, the reaction can be carried out in the same reaction kettle, the production efficiency is high, the method is green and environment-friendly, and the cost is low.
Owner:PUTIAN DAKAI NEW MATERIALS CO LTD

Method for separating cyclopentyl methyl ether, cyclopentene and methanol through three-tower extractive distillation

The invention relates to a method for separating cyclopentyl hexyl methyl ether, cyclopentene and methanol through three-tower extractive distillation. According to the method, an extractive distillation process is adopted, and two extractive distillation towers and a solvent recovery tower are adopted. An organic solvent is used as an extraction agent, cyclopentyl hexyl methyl ether, cyclopentene and methanol firstly enter an extractive distillation tower (EDC1) for extraction separation, high-purity cyclopentene is obtained at the top of the extractive distillation tower (EDC1), materials at the bottom of the extractive distillation tower (EDC1) enter an extractive distillation tower (EDC2) for separation, and high-purity methanol is obtained at the top of the extractive distillation tower (EDC1). Materials at the tower bottom of the extractive distillation tower (EDC2) enter a solvent recovery tower (SRC), high-purity cyclopentyl hexyl methyl ether is obtained at the top of the solvent recovery tower (SRC), and an organic solvent extraction agent is obtained at the bottom of the solvent recovery tower (SRC). The method has the advantages of low energy consumption, simple process, greenness, energy conservation, high product purity after separation and the like, and the adopted organic solvent extraction agent is good in stability, non-toxic and environment-friendly.
Owner:QINGDAO UNIV OF SCI & TECH

Preparation method of odorant 3-(3-isopropyl phenyl) butyraldehyde

The invention belongs to the technical field of preparation methods of fine compounds, and particularly relates to a preparation method of 3-(3-isopropyl phenyl) butyraldehyde. The method comprises the following steps: by taking a mixed material of m-isopropenyl cumene and phenylcyclopentene as a raw material, carrying out carbonylation reaction under the action of a catalyst; the catalyst is a noble metal carbonyl catalyst; after the reaction is finished, a reaction product is rectified, and isopropenyl isopropyl benzene is obtained; and carrying out formylation reaction on the product, and separating to obtain the 3-(3-isopropyl phenyl) butyraldehyde. The method has the advantages that raw material sources are simplified, physical and chemical properties of products obtained after different components react are changed through different reaction conditions of the different components in the reaction process, the purposes of separation, removal and purification are easily achieved, then the target product is obtained through the hydroformylation reaction, high purity is kept, and the method is suitable for industrial production. And moreover, the conversion rate is more thorough, and the cost can be greatly reduced compared with the existing production technology economically.
Owner:HANGZHOU COLORIFIC CHEMICALS CO LTD

Catalyst for synthesizing glutaraldehyde from cyclopentene and synthesis method thereof

The invention relates to the technical field of catalyst synthesis, in particular to a catalyst for synthesizing glutaraldehyde from cyclopentene and a synthesis method thereof.The catalyst for synthesizing glutaraldehyde from cyclopentene comprises a molecular sieve and an active center loaded on the molecular sieve, and is characterized in that the molecular sieve is an HMS molecular sieve, the specific surface area is 500-700 m < 2 > / g, the average pore size is 2-10 nm, and the molecular sieve is an HMS molecular sieve. The active center is WO3, and the molar ratio of Si in the molecular sieve to W in the active center is (20-30): 1. The catalyst prepared by the preparation method of the catalyst for synthesizing glutaraldehyde from cyclopentene can load more catalytic active centers, the loading capacity is higher than that of the existing catalyst with the Si / W molar ratio of about 35: 1, but the catalyst is dispersed more uniformly and is not easy to agglomerate, so that higher conversion rate and selectivity are obtained.
Owner:PUYANG LIANZHONGXINGYE CHEM IND CO LTD

Polyfunctional vinyl resin and method for producing same, polyfunctional vinyl resin composition, cured article, prepreg, resin sheet, and laminated plate

Provided is a resin material showing a high thermal conductivity and having high heat resistance while having a low dielectric constant and a low dielectric loss tangent. The material is a polyfunctional vinyl resin, which is represented by the following general formula (1):where R1s each independently represent a hydrocarbon group having 1 to 8 carbon atoms, R2s each independently represent a hydrogen atom or a dicyclopentenyl group, and at least one thereof represents a dicyclopentenyl group, Xs each independently represent a hydrogen atom or a vinyl group-containing aromatic group represented by the formula (1a), and at least one thereof represents a vinyl group-containing aromatic group, “n” represents a number of repetitions, and the average thereof is a number of from 1 to 5, and Ar represents an aromatic ring.
Owner:NIPPON STEEL CHEM & MATERIAL CO LTD +1

Stabilized cyanoacrylate compositions

This invention relates to cyanoacrylate-containing compositions that include, in addition to the cyanoacrylate component, a benzodioxol free radical stabilizer. The inventive cyanoacrylate compositions demonstrate improved shelf life stability while maintaining the level of adhesive performance.
Owner:HENKEL KGAA

Crosslinked fluororesin, preparation method and application

PendingCN120504770AVinyl etherCyclopentene
The invention discloses cross-linked fluororesin, a preparation method and application, and belongs to the technical field of fluorine-containing polymers. The cross-linked fluororesin is composed of a fluorine-containing copolymer A and a cross-linking agent B. The tensile strength of the cross-linked fluororesin is larger than or equal to 30 MPa, the elongation at break is larger than or equal to 150%, and the transparency is larger than or equal to 85% when the thickness is 0.1 mm. The fluorine-containing copolymer A is a copolymer formed by copolymerization of perfluoro-2, 2-dimethyl-1, 3-dioxole PDD, hexafluoropropylene and perfluoroalkyl vinyl ether containing two double bonds, and the fluorine-containing copolymer A is a copolymer formed by copolymerization of perfluoro-2, 2-dimethyl-1, 3-dioxole PDD, hexafluoropropylene and perfluoroalkyl vinyl ether containing two double bonds. The cross-linked fluororesin prepared by the invention has the advantages of high strength, high toughness, high transparency and the like, and the performance boundary and the application field of the fluororesin are expanded.
Owner:JIANGNAN UNIV

Alkali-soluble resin containing polymerizable unsaturated groups, method for producing the same, photosensitive resin composition, and cured product thereof

The present invention provides a photosensitive resin composition, an alkali-soluble resin containing a polymerizable unsaturated group used therein, and a method for producing the alkali-soluble resin containing a polymerizable unsaturated group. The photosensitive resin composition can achieve patterning with excellent resolution by alkali development, and can provide a cured product that can be applied to an insulating film or the like having excellent chemical resistance and excellent reliability such as fold resistance. A method for producing an alkali-soluble resin containing a polymerizable unsaturated group, characterized in that an epoxy (meth)acrylate resin represented by the following general formula (1) is reacted with a dicarboxylic acid, a tricarboxylic acid, or an acid anhydride thereof, and a tetracarboxylic acid or its acid dianhydride. Here, R 1 represents an alkyl group having 1 to 8 carbon atoms, a phenyl group, or an allyl group, R 2 represents a hydrogen atom or a dicyclopentene group, R 3 represents a hydrogen atom or a methyl group.
Owner:NIPPON STEEL CHEM & MATERIAL CO LTD +1