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49 results about "Treatment modification" patented technology

Improvement method for titanium alloy laser 3D printing

The invention discloses an improvement method for titanium alloy laser 3D printing and relates to an improvement method for laser 3D printing. The improvement method for titanium alloy laser 3D printing solves the problems that titanium alloy and components prepared through laser 3D printing at present are low in strength level and heat resistant temperature, the metallographic structure is thick and big and not even, the metallographic structure grows to be big in the subsequent heat treatment modification process, the technological parameter selectable range in subsequent heat treatment is narrow, the mechanical property improvement is limited, and the plasticity level of the alloy and the components is low. The improvement method includes the steps that firstly, titanium or titanium alloy powder is evenly mixed with improved raw material powder in a ball milling mode; secondly, laser 3D printing is conducted. The metallographic structure of a laser 3D titanium metal product prepared through the mode of execution is thin and small, a subsequent heat treatment window can be greatly expanded, a balanced structure formed by high-temperature annealing can be achieved, long-time solution strengthening processing or annealing processing can be conducted, the even metallographic structure is obtained, and the mechanical performance of the metallographic structure is greatly improved.
Owner:HARBIN INST OF TECH

Nano silver in-situ formation silver-plating method based on plasma modification and silver-plated fabric

The invention relates to a nano silver in-situ formation silver-plating method based on plasma modification and a silver plated fabric. In the provided method, a plasma surface treatment modification technology is adopted to crack and etch the surface of synthetic fibers so as to form micro pits and fine cracks on the surface of fibers, thus the surface area of the fibers is enlarged, and the wettability of the fiber surface is improved. At the same time, the surface of the fibers is etched, and the binding strength between the metal coating and the fibers is enhanced. After the fibers are subjected to an oxygen gas plasma technology, hydrophilic and polar groups (-COOH, =C=O) are grafted on the fiber surface, thus silver ions can be adhered on the fiber surface more easily; in the presence of polyvinylpyrrolidone (PVC), sodium borohydride (NaBH4) is taken as the reducing agent to directly reduce the silver ions into nano silver particles, and a compact silver coating is in-situ generated on the etched fiber surface. The provided method has the advantages of simple technology, environment-friendliness, energy saving, and reduced cost. The silver coating on the produced silver-plated fabric is uniform and compact, the binding force between the silver coating and the fabric is strong, and the method is worth to promote.
Owner:SHANHAI CHENLONG TEXTILE NEW MATERIAL CO LTD

ETS-10 titanium silicalite molecular sieve modification method

The invention relates to an ETS-10 titanium silicalite molecular sieve modification method. The ETS-10 titanium silicalite molecular sieve modification method provided by the invention comprises the following steps: alkali treatment modification: carrying out alkali treatment modification of EST-10 titanium silicalite molecular sieve raw powder through adopting an alkaline solution, filtering, washing, and drying to obtain alkali treatment modified ETS-10 titanium silicalite molecular sieve; and realuminated modification treatment: carrying out realuminated modification treatment of the alkali treatment modified ETS-10 titanium silicalite molecular sieve through adopting an aluminum salt solution or an aluminate solution, filtering, washing, drying, and roasting to obtain the alkali treatment modification and realuminated modification treated ETS-10 titanium silicalite molecular sieve. The modification method provided by the invention adopts the alkali treatment modification and the realuminated modification treatment of the EST-10 titanium silicalite molecular sieve raw powder to be carried out, so the surface phase of the EST-10 titanium silicalite molecular sieve is rich in titanium and aluminum, abundant meso-structures are introduced, and the skeletal acidity is improved.
Owner:PETROCHINA CO LTD +1

Point, line, surface three-dimensional carbon material composite heat-conduction silica gel and preparation method thereof

The present invention provides a point, line, surface three-dimensional carbon material composite heat-conduction silica gel and a preparation method thereof. The composite heat-conduction silica gel comprises, by weight, 0.1-30% of surface-modified graphene, 0.1-30% of surface-modified carbon nano-tubes, 0.1-30% of surface-modified carbon nano-spheres, and the balance of silica gel, wherein the sum of the mass fractions of the surface-modified graphene, the surface-modified carbon nano-tubes and the surface-modified carbon nano-spheres is more than or equal to 10%, a mass ratio of the surface-modified graphene to the surface-modified carbon nano-tubes to the surface-modified carbon nano-spheres is 1:0.5-2:0.5-4, and the surface-modified graphene, the surface-modified carbon nano-tubes and the surface-modified carbon nano-spheres are prepared through treatment modification with strong acids. According to the present invention, the solubilities and the dispersions of the graphene, the carbon nano-tubes and the carbon nano-spheres in the silica gel are effectively improved, and the three modified carbon materials form the stable and continuous three-dimensional heat-conduction network in the silica gel so as to substantially improve the thermal conductivity of the heat-conduction silica gel.
Owner:江苏华永烯科技有限公司

Sludge continuous-heat-treatment modification device and technology of deep dehydrating, drying and incineration

The invention relates to a sludge continuous-heat-treatment modification device and a technology of deep dehydrating, drying and incineration. The sludge continuous-heat-treatment modification device comprises sludge conveying tubes and heat medium spacing casing tubes, wherein the sludge conveying tubes comprises a preheating section, a reacting section and a cooling section, and the sludge conveying tubes of all the preheating section, the reacting section and the cooling section are sleeved by the heat medium spacing casing tubes; the heat medium spacing casing tube of the reacting section communicates with a heat medium heating converter to form a first heat medium circulating loop; the heat medium spacing casing tube of the preheating section communicates with the heat medium spacing casing tube of the cooling section to form a second heat medium circulating loop; and a heat medium heat recovery circulating pump is arranged in the second heat medium circulating loop. The sludge continuous-heat-treatment modification device uses a heat medium to perform indirect heat treatment on sludge and improves the dehydrating property of the sludge, therefore the sludge continuous heat treatment is realized and the recycling use of the heat medium saves more energy and is more friendly to environment at the same time.
Owner:浙江绿治环保技术有限公司 +1

Method for preparing polyurethane-nanosilver long-acting antibacterial film by post-heat treatment modification method

The invention relates to a method for preparing a polyurethane-nanosilver long-acting antibacterial film by a post-heat treatment modification method, which includes the following steps: (1) diisocyanate and polytetrahydrofuran are mixed to react; a cross-linking agent and an acetone solution of a chain extender are added, dimethylolpropionic acid and a catalyst are added, reaction takes place, and thereby PU (polyurethane) is obtained; a dimethylformamide solution of silver nitrate is added into a polyurethane solution, a film is formed after uniform stirring, heat treatment is carried out, and thereby a polyurethane-nanosilver film is obtained; (2) 4,4'-dihydroxybenzophenone reacts with long-chain alkyl halide, so that 4,4'-bis-long-chain alkoxy benzophenone is obtained; the 4,4'-bis-long-chain alkoxy benzophenone reacts with hydrazine hydrate, so that 4,4'-bis-long-chain alkoxy benzophenone hydrazone is obtained; and the 4,4'-bis-long-chain alkoxy benzophenone hydrazone undergoes oxidation reaction, so that long-chain alkyl diazomethane is obtained; (3) the long-chain alkyl diazomethane is dissolved into a solvent, and is uniformly applied onto the surface of the polyurethane-nanosilver film, and after heat treatment, the polyurethane-nanosilver long-acting antibacterial film is obtained. The method can be used for realizing long-acting bacteria resistance.
Owner:QILU UNIV OF TECH

Surface heat treatment modification method of fluorescent powder and COB light source made of fluorescent powder

The invention relates to a surface heat treatment modification method of fluorescent powder and a COB light source made of the fluorescent powder, belonging to the field of LED inorganic luminescent materials. According to the method, heating treatment is carried out on a (Ca, Q)1-y(Al, Si)2(N, T)3: Ay fluorescent powder material in an oxidative atmosphere to ensure that a compact oxide layer is formed on the surface of the fluorescent powder material; and the surface of the fluorescent powder material is modified to effectively isolate the fluorescent powder material from the external environment, so that the stability of the fluorescent powder is improved and the service life of the fluorescent powder is prolonged. According to the method, the stability of single-phase nitrides can be improved to ensure that the nitrides are beneficial for the absorption and emission of light, thereby improving the performance and stability of nitride red powder after LED packaging. When the nitride red powder prepared through the method is matched with an ultraviolet, near-ultraviolet or blue LED and other light emitting materials such as yttrium aluminum garnet and the like, the COB light source with high power and high coloration can be prepared; and after the COB light source is continuously lightened for 1000 hours, the lumen depreciation is zero.
Owner:BEIJING YUJI SCI & TECH +2

Preparation method of black titanium dioxide nano thin film

The invention belongs to the technical field of preparation of nano thin films and relates to a preparation method of a black titanium dioxide nano thin film. A technological process comprises three steps including preparation of nanoparticles, preparation of the nano thin film and thickness control of the nano thin film; black titanium dioxide nanoparticles are prepared from titanium tetraisopropoxide and nickel nitrate; the black titanium dioxide nanoparticles are deposited on a stainless steel substrate by adopting an electrophoretic deposition method so as to prepare the black titanium dioxide nano thin film; nickel ion doping is coupled with hydrogen atmosphere heat treatment modification, and effective active sites can be formed on the surface of titanium dioxide by doping nickel ions, and separation of photo-induced electrons and holes is accelerated; the catalytic activity of the titanium dioxide is improved and hydrogen atmosphere heat treatment can expand a photo-response region of the titanium dioxide; white titanium dioxide is turned into black titanium dioxide; the technological process is simple, low in production cost, rapid in deposition speed and high in film-forming quality; an application environment is environmentally friendly and commercialized requirements are met.
Owner:青岛西交蓝海科技有限公司

High-pressure low-sulfur-tolerant shift catalyst and preparation method thereof

The invention belongs to the technical field of sulfur-tolerant shift in coal chemical industry, and particularly relates to a high-pressure low-sulfur-tolerant shift catalyst and a preparation methodthereof, wherein the catalyst comprises a carrier and an active component, the active component is selected from a binary component of cobalt oxide and molybdenum oxide, the raw materials of the carrier are selected from a magnesium-containing compound, an aluminum-containing compound, a titanium-containing compound and a heat-treated modified montmorillonite. According to the present invention,montmorillonite with characteristics of wide source and low cost is subjected to heat treatment modification to be used as the carrier component so as to reduce the catalyst preparation cost; the montmorillonite is subjected to heat treatment so as to avoid the treatment of the waste acid solution; the product is prepared by the mixing kneading method, such that the active components are uniformlydispersed in the carrier and are not easily lost so as to increase the activity stability of the catalyst; and compared with the impregnation method in the prior art, the method of the present invention has the following advantages that the water consumption is saved, the preparation process and the operation process are simplified, the cost advantage is remarkable, and the prepared catalyst hasgood shift activity and good activity stability under low sulfur condition, and further has good economic benefits and popularization and application prospects.
Owner:CHINA PETROLEUM & CHEM CORP

High-pressure-resistant insulation electric pump and surface heat-treatment modification process thereof

The invention discloses a high-pressure-resistant insulation electric pump. A high-pressure-resistant insulation layer is covered on an outer shell of the electric pump, and comprises a high-pressure-resistant layer and an insulation layer; the high-pressure-resistant layer and the insulation layer are compounded according to the proportion of the high-pressure-resistant layer to the insulation layer being equal to 3:2; the high-pressure-resistant layer is prepared from the components in parts by mass: 3 to 9 parts of water-based resin emulsion, 13 to 19 parts of silicon carbide micro powder,29 to 32 parts of polypropylene carbonate, 10 to 14 parts of 1-butanol, 10 to 15 parts of polypropylene carbonate, 13 to 18 parts of barium sulfate, 22 to 29 parts of lime powder, 3 to 11 parts of calcium-zinc compound stabilizer, 29 to 32 parts of defoaming agent, 11 to 19 parts of coupling agent, and 22 to 28 parts of fire retardant; the insulation layer is prepared from the components in partsby mass: 9 to 15 parts of nanosilicon dioxide, 2 to 9 parts of butyl acrylate, 10 to 15 parts of silane coupling agent, 22 to 29 parts of wood fiber powder, 15 to 19 parts of carbon fiber powder, 11 to 15 parts of vapor phase inhibitor, 18 to 21 parts of coalescing agent, 20 to 24 parts of thickening agent, 9 to 13 parts of defoaming agent, and 20 to 28 parts of curing agent.
Owner:博维恩冷冻科技(苏州)有限公司

Strong-acid-resistant high-strength metal valve and surface heat treatment modification process thereof

The invention discloses a strong-acid-resistant high-strength metal valve. The outer surface of the metal valve is coated by a strong-acid-resistant high-strength layer, the strong-acid-resistant high-strength layer is formed by compounding of an A component and a B component, wherein the A component comprises the following materials: 9-13 parts of epoxy resin, 6-13 parts of polyurethane, 8-15 parts of titanium dioxide, 3-7 parts of graphite fluoride, 19-24 parts of barium sulfate, 8-13 parts of a thixotropic auxiliary agent, 14-19 parts of a base-material emulsion, 3-9 parts of an antifreezing agent, 20-25 parts a filler, and 33-39 parts of an auxiliary material; and the B component comprises the following materials: 13-19 parts of nano silicon dioxide, 11-19 parts of butyl acrylate, 1-7parts of a silane coupling agent, 14-19 parts of xylem fiber powder, 20-25 parts of carbon fiber powder, 8-14 parts of a vapor phase corrosion inhibitor, 10-14 parts of antimony trioxide, 19-22 partsof a film forming auxiliary agent, 15-19 parts of a thickener, 4-9 parts of a defoaming agent, and 10-15 parts of a curing agent. The metal valve provided by the invention improves working efficiency,reduces pollution to the environment, and reduces production costs, and the process has simple steps, and is convenient for operation.
Owner:张剑

Wear-resistant and rust-proof valve handle and vacuum heat treatment modification process thereof

The invention discloses a wear-resistant and rust-proof valve handle. The surface of a metal valve is coated with a wear-resistant and rust-proof layer, and specific operation of coating the wear-resistant and rust-proof layer comprises steps as follows: (1) cleaning the valve handle with purified water at a temperature of 95-100 DEG C, performing blow drying at a temperature of 80-90 DEG C, cooling the valve handle naturally to the room temperature, cleaning the rubber surface 5-6 times with an aliphatic hydrocarbon solvent with respect to the dried valve handle surface, washing the surface with purified water at the temperature of 45 DEG C, and finally drying the surface by a fan for standby application; (2) preparing a wear-resistant and rust-proof layer coating which is prepared from the following components in parts by mass as shown in the description; (3) sending the valve handle treated in the step (1) to a heating furnace for preheating to 300-350 DEG C, and then sending the preheated valve handle into a spraying device, evenly spraying fine sand to the valve surface for thickness of 0.01-0.03 mm by using a spraying gun, then performing heating curing rapidly, repeating thespraying process until the film thickness is 0.06-0.08 mm; (4) cooling the valve handle coated with the wear-resistant and rust-proof layer, cooling the valve handle to room temperature, and inspecting and warehousing the valve handle.
Owner:朱建海
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