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516results about How to "Low oil absorption" patented technology

Surface treatment method for nanometer calcium carbonate applied to fill silicone sealant

A disclosed surface treatment method for nanometer calcium carbonate applied to fill a silicone sealant comprises the following steps: adding a nanometer calcium carbonate slurry into a reaction kettle, stirring and heating to 60-80 DEG C, so as to obtain a nanometer calcium carbonate suspending slurry; slowly adding a compound surfactant composed of saturated aliphatic acid and coconut oil into the nanometer calcium carbonate suspending slurry for first surface treatment; then slowly adding an alkylphenol polyoxyethylene ether dimeric surfactant for secondary surface treatment, so as to obtain a nanometer calcium carbonate modification solution; and performing dewatering, drying, crushing and sieving on the nanometer calcium carbonate modification solution, so as to obtain the nanometer calcium carbonate for filling the silicone sealant. The nanometer calcium carbonate obtained according to the surface treatment method possesses good dispersibility, hydrophobicity and relatively low oil absorption value, and is capable of improving the storage stability, mechanical properties, ageing resistance, photothermy resistance, oxidation resistance and other performances of the silicone sealant when being applied to fill the silicone sealant.
Owner:GUANGXI HUANA NEW MATERIALS TECH CO LTD

Preparation method for submicron active calcium carbonate special for PVC and with low oil absorption value

The invention discloses a preparation method for submicron active calcium carbonate special for PVC and with low oil absorption value. The preparation method comprises the main steps: preparing a solution of a refined calcium hydroxide slurry with a weight percentage of 5-7%, adding a crystal-form controlling agent cane sugar accounting for 0.4-0.8% by weight of calcium hydroxide, introducing kiln gas containing carbon dioxide with a concentration of 25% or more, controlling the temperature of the reaction slurry at 27-30 DEG C for carbonization, when the carbonization rate is 15-25%, stopping cooling water, continuing to introduce kiln gas for normal-temperature carbonization, wherein the carbonization terminal point is that the pH value of the slurry is less than 7; then heating the slurry to 80 DEG C, adding a saponification emulsion of stearic acid accounting for 2.5-4.5% by weight of calcium carbonate, and under the effect of high shearing force of an emulsification pump, synchronously finishing dispersing and surface cladding of the calcium carbonate slurry; and finally performing filtering, drying and depolymerizing on the slurry to obtain the PVC special-purpose low-oil-absorption-value submicron active calcium carbonate product with the particle size of 200-400 nm and the oil absorption value of 16-18.
Owner:WUHU ZHUOYUE NANO NEW MATERIALS

Single-component addition type high-temperature-resistant high-thermal-conductivity silica gel and preparation method thereof

The invention provides single-component addition type high-temperature-resistant high-thermal-conductivity silica gel and a preparation method thereof. The single-component addition type high-temperature-resistant high-thermal-conductivity silica gel is prepared from the following raw materials in parts by weight: 80 to 100 parts of vinyl silicone oil, 0.1 to 5 parts of cross-linking agent hydrogen-containing silicone oil, 500 to 2000 parts of a thermal-conductive filler, 1 to 20 parts of a treating agent, 1 to 4 parts of a catalyst and 1 to 8 parts of a pigment, and the hydrogen-containing silicone oil comprises at least one of terminated hydrogen-containing polysiloxane and side hydrogen-containing polysiloxane; and the hydrogen content of the end hydrogen-containing polysiloxane is 0.16 to 3.00 mmol/g, and the hydrogen content of the side hydrogen-containing polysiloxane is 0.9 to 9 mmol/g. Compared with silicone grease and silicon gaskets which are frequently used in the market at present, the single-component addition type high-temperature-resistant high-thermal-conductivity silica gel provided by the invention has the advantages of higher heat conductivity coefficient, higher bearing temperature, almost unchanged thermal resistance after long-time aging and the like, and further ensures that a heat-conducting interface material always keeps high heat-conducting efficiency in a long-term use process.
Owner:SHANGHAI HUITIAN NEW CHEMICAL MATERIALS CO LTD

Method for preparing silver powder for touch screen silver paste

The invention relates to a method for preparing silver powder for a touch screen silver paste and belongs to the technical field of preparation of conductive metal powder. The method comprises the following steps: using silver nitrate as a raw material and controlling the speed of liquid phase reduction reaction by regulating the process conditions of reaction temperature, charging manner and charging speed so as to prepare approximately spherical or spherical particle reduced silver powder with a particle size of 300 nm to 800 nm; sufficiently stirring and modifying the silver powder in absolute ethyl alcohol solution containing two modifiers of oleic acid, stearic acid, hexadecanol, a polyacrylate dispersing agent and a graft copolymer dispersing agent, carrying out batching on the obtained modified silver powder and phi3 stainless steel beads according to a mass ratio of 1:10 after drying at a temperature of 60 DEG C, and grinding for 10 to 24 hours; and after finishing grinding, carrying out bead and material separation, sieving the obtained silver powder by 300 meshes to obtain the high dispersion approximately spherical or spherical silver powder with D50 of 1.5 to 2.5mum and tap density of 4.0 to 6.0 g/cm<3>. The silver powder prepared by the method disclosed by the invention has high crystallinity, is suitable for an addition volume of silver of 70 to 85 percent and can be used for printing capacitive screen silver paste of a thin wire with a specification below 80 mum.
Owner:云南铜业科技发展股份有限公司

Method for modifying surface of nano calcium carbonate

The invention discloses a method for modifying the surface of nano calcium carbonate. The method comprises the steps that 1, lime milk is added to a bubbling carbonatation reaction kettle, mixed gas containing carbon dioxide is introduced to the reaction kettle for a carbonatation reaction, carbonatation is conducted till the pH is equal to 7.0, carbonatation is completed, and a nano calcium carbonate suspension solution is obtained; 2, a stabilizer is added to the nano calcium carbonate suspension solution, the temperature is controlled within 50-60 DEG C, and heat preservation is conducted for 20-30 min; 3, a fatty acid modifier is heated and melted in water, an emulsifier is added to the fatty acid modifier, stirring is conducted for 10-30 min, and a modifier emulsion is obtained; 4, the nano calcium carbonate suspension solution obtained in the second step is added to the modifier emulsion, stirring is conducted for 30-60 min, and then through filter-pressing dehydration, drying and smashing, a nano calcium carbonate product is obtained. The prepared nano calcium carbonate has the advantages of good dispersity and processability, low oil absorption value, high thixotropy and activation rate, good stability, pH value close to neutral and the like. The method is low in production cost and simple in technology, facilitates industrial production and has good economic, social and ecological benefits.
Owner:ANHUI PROVINCE XUNCHENG CITY HUANA NEW MATERIAL TECH CO LTD

Preparation method of low-specific-surface-area high-oil-absorption-value friction type silicon dioxide

The invention belongs to the technical field of silicon dioxide, and particularly relates to a preparation method of low-specific-surface-area high-oil-absorption-value friction type silicon dioxide.The preparation method comprises the steps that S1, 8-12 m<3> of ethanol aqueous solution is injected and heated to 60-70 DEG C, and stirring starts; S2, water glass and sulfuric acid are added dropwise to carry out a parallel flow reaction, the pH value in the reaction process is controlled to be 6.0-6.8, meanwhile, absolute ethyl alcohol is added every 5-10 minutes in the reaction process to keep the volume ratio of ethyl alcohol to water in a reaction system to be 1:(3-7), after the water glass is dropwise added, dropwise addition of sulfuric acid is stopped, and stirring continues; S3, stirring and heating are stopped, aging is conducted for one hour, and pressure filtration, washing, drying and crushing are conducted on the on formed silicon dioxide to prepare silicon dioxide. The silicon dioxide has the advantages of a low in specific surface area, a high oil absorption value, a high water absorption amount, the friction property and the like; toothpaste has good friction and cleaning performance after the silicon dioxide is used, and meanwhile, the problem of expansion of the viscosity of the toothpaste is well solved.
Owner:GUANGZHOU FEIXUE MATERIAL TECH

Oil-proof low-smoke halogen-free flame-retardant heat shrinkable label sleeve as well as preparation method and application thereof

The invention discloses an oil-proof low-smoke halogen-free flame-retardant heat shrinkable label sleeve and a preparation method thereof. The label sleeve consists of the following components in parts by weight: 60 to 80 parts of matrix resin, 15 to 25 parts of linear low-density polyethylene, 5 to 15 parts of polymer compatilizer, 32 to 70 parts of phosphorous nitrogen series expansible halogen-free flame retardant, 0 to 30 parts of inorganic flame retardant, 3 to 5 parts of titanium white powder, 1 to 3 parts of lubricant, 0.8 to 2 parts of antioxidant and 1 to 2 parts of sensitizer. The preparation method comprises the following steps of: mixing the raw materials uniformly, extruding with a double-screw extruder, drawing, air cooling and granulating; extruding into a pipe through a screw extruder with a neck mould and a core mould, radiating, expanding, stretching, cooling, sizing, printing the label by using a heat transfer printer to obtain the oil-proof low-smoke halogen-free flame-retardant heat shrinkable label sleeve. The preparation method is simple; and the product has excellent flame-retardant performance and good oil resistance, produces little smoke, permanently preserves the label, and keeps good mechanical property, electric insulating performance and heat resistance.
Owner:广州凯恒科塑有限公司

Hydrolysis method for producing electronic-grade special titanium white by sulfuric acid process

The invention belongs to the field of chemical industry and relates to a hydrolysis method for producing electronic-grade special titanium white by a sulfuric acid process. The technical problem to be solved is that the electronic-grade special titanium white with narrow particle size distribution and low impurity content is prepared by the sulfuric acid process. The method improves the hydrolysis method in the sulfuric acid process, and the improved hydrolysis method comprises the following steps of: A, adding titanium liquid with the concentration of 140 to 190g/L which is preheated to the temperature of between 75 and 95 DEG C into water which is preheated to the temperature of between 80 and 95 DEG C; B, heating the system to boil, and keeping the system boiling; C, when the hydrolysis system becomes steel grey, continuously keeping boiling for 5 to 25 minutes, stopping heating and stirring, and curing; and D, heating the system to boil with stirring, and keeping the system slightly boiling until the hydrolysis is finished. The obtained titanium white has the mean grain size of 800 to 1,200nm, the half-peak width of 70 to 98nm, narrow range of particle size distribution and low impurity content, and can be used as electronic-grade special titanium white.
Owner:PANGANG GROUP VANADIUM TITANIUM & RESOURCES +1
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