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133 results about "Scratch test" patented technology

Micron-nano scale in-situ nano indentation and scratching test system

The invention relates to a micron-nano scale in-situ nano indentation and scratching test system which integrates driving, precise loading and signal detection, micron-nano scale mechanics performance testing, ultraprecise scratching processing and high resolution in-situ observing as one. The system is mainly composed of a precise positioning platform at X-axis and Y-axis directions, a precise linear positioning platform at Z-axis direction, a precise indentation driving unit, a load signal and displacement signal detection unit and a high resolution digital microscopic imaging system for observing and storing material deformation and damage conditions in the test process. The precise positioning platform at the X-axis and Y-axis directions is assembled on a base, the precise linear positioning platform at the Z-axis direction is assembled on a side plate, the precise indentation driving unit, a precise mechanical sensor for detecting the indentation material pressure of a diamond tool head and a precise displacement sensor for detecting the indentation depth of the diamond tool head to along the Z-axis direction are assembled on the precise linear positioning platform at the Z-axis direction, and the high resolution digital microscopic imaging system is assembled on a beam.
Owner:赵宏伟

Preparation method for silver nano wire transparent conductive film capable of preventing corrosion of hydrogen sulfide gas

The invention discloses a preparation method for a silver nano wire transparent conductive film capable of preventing corrosion of a hydrogen sulfide gas. The method comprises: scratching or sparying a silver nano wire colloid on an appropriate substrate to obtain a low-conductivity silver nano wire transparent conductive film; then carrying out post treatment of high temperature, high voltage and the like to obtain a high-transparency high-conductivity silver nano wire transparent conductive substrate; and then preparing a protective agent solution, diluting the protective agent solution in a large proportion, according to the type and size of the substrate selected for the silver nano wire film, selecting an appropriate spraying instrument or a spin coating instrument, preparing a protective layer of a thin layer on the surface of the substrate film, and finally, solidifying the protective layer through natural drying, heating by use of a heating plate or blow-drying by use of a blower. The silver nano wire transparent conductive film prepared by use of the method provided by the invention can prevent corrosion of gases such as the hydrogen sulfide gas and the like, can prevent scratches and has good conductivity and transmittance through a 3M adhesive tape and a pencil scratch test. The operation is simple, the cost is low, and large scale production can be carried out.
Owner:HEFEI INSTITUTES OF PHYSICAL SCIENCE - CHINESE ACAD OF SCI

Rock brittleness evaluation method based on stress strain curve and scratch test

The invention provides a rock brittleness evaluation method based on a stress strain curve and a scratch test. The method comprises the following steps that: evaluating rock from a crustal stress environment where the rock is positioned, and pore pressure, and obtaining the stratum condition of the rock; selecting a rock mechanical experiment of the environment where a rock sample to be tested ispositioned, wherein the experiment includes a conventional triaxial compression test or a triaxial compression test which considers pore pressure, and a scratch test; obtaining a pre-peak strain energy density value, a crack initiation stress value, a peak value stress value, a residual stress value as well as corresponding strain size and crack linear density; and determining the value range of an effective stress coefficient [Alpha] from the pore pressure of a tested rock sample, and substituting the pre-peak strain energy density value, the crack initiation stress value, the peak value stress value, the residual stress value as well as the corresponding strain size and crack linear density into a brittleness index calculation formula to obtain the brittleness index of the rock to be tested. By use of the brittleness evaluation method, the accuracy and the applicability of the rock brittleness evaluation can be improved.
Owner:CHINA UNIV OF PETROLEUM (BEIJING)

Device for testing nano scratch and friction stick-slip properties of film surfaces

The invention discloses a device for testing the nano scratch and friction stick-slip properties of film surfaces. The device comprises a base, wherein the base is provided with a piezoelectric motion platform for holding test samples and a displacement platform capable of moving vertically and horizontally, the displacement platform is provided with a sensor holder, the front end of the sensor holder is fixedly provided with a nano scratch and stick-slip testing sensor, the scratching head of the nano scratch and stick-slip testing sensor is located right above the piezoelectric motion platform, and the base is also provided with an optical imaging system. According to the device disclosed by the invention, the motion platform and the sensor are organically combined, through different motion control modes, on the one hand, a nano scratch test on films can be completed, and therefore the defects that an AFM (Atomic Force Microscope) nano scratch device is limited in a loading range and difficult to control, and has high requirements on the surface roughness of samples are overcome; and on the other hand, the online test on the friction stick-slip properties of film surfaces can also be completed, therefore, the defect that a high-stiffness friction tester can not reflect the friction stick-slip properties of surfaces is overcome.
Owner:XI AN JIAOTONG UNIV

Test method for evaluating initial wear resistance of austenite high manganese steel under high impact load

The invention relates to a test method for evaluating the initial wear resistance of austenite high manganese steel under a high impact load. The test method comprises the following steps of: (1) performing a simple pendulum impact scratch test by using a simple pendulum scratch testing machine; (2) calculating energy E consumed in a scratch forming process; (3) calculating the volume V of a sample surface scratch; and (4) calculating specific dissipating energy e according to a formula e=E/V and judging the level of the initial wear resistance of the austenite high manganese steel under the high impact load according to the magnitude of the specific dissipating energy e under the same test parameter condition. The simple pendulum impact scratch test has a function of simulating the micro-plowing and micro-cutting of abrasive wear, and has the impact energy loading characteristic when a single abrasive particle scratches a material surface with a certain impact force and the working condition is similar to that of the austenite high manganese steel under the high impact load, so the specific dissipating energy e obtained under the simple pendulum impact scratch test can represent the initial wear resistance of the material under the high impact load.
Owner:DALIAN JIAOTONG UNIVERSITY

Coating service life prediction method based on stress and bonding strength evolvement mechanism

The invention provides a coating service life prediction method based on a stress and bonding strength evolvement mechanism and relates to a coating service life prediction method. The coating service life prediction method aims at solving the problem a comprehensive and objective coating service life prediction method is not disclosed at present. The coating service life prediction method comprises the steps that firstly, residual stress-time change relation and oxidation layer stress-time change relation are established, and a coating stress evolutionary physical model is established; secondly, a thermal-cycle sample aging acceleration test is performed, and the acceleration times of artificially accelerating sample aging are obtained according to the coating stress evolutionary physical model and sample stress value-time relation; thirdly, a scratch test instrument is adopted to test the bonding strength of the sample artificially accelerated in aging, the bonding strength-ageing time relation is fit and is drawn into a changing curve, the time corresponding to the intersection point of the changing curve and a timeline serves as the service life 1 of the sample artificially accelerated in aging, and L is equal to sample service life 1* final acceleration times k and serves as the predicted service life. The coating service life prediction method is applicable to the field of coating service life prediction.
Owner:HARBIN INST OF TECH

Palladium-free activation process for plastic substrate surface of nickel adsorbed sodium carboxymethylcellulose by chelating function

The invention provides a method for non-precious metal Pd-free plastic matrix surface activation using sodium carboxymethyl cellulose to chelae and absorb nickel, which comprises the processing steps of pretreatment of the surface of the plastic matrix to be plated, preparation of an activating and film forming liquid, treatment of activation and film forming, treatment of reduction, and chemical nickel plating; and a metal organic complex solution consisting of divalent ion water soluble salt containing nickel uses a strong reducing agent to directly reduce the active metal-nickel and deposit on the matrix, then the chemical nickel plating is carried out. The result of the configuration of a nickel plating layer by a scanning electron microscope and a metaloscope shows that the plating layer is combined compactly, and particles are evenly distributed; and scratch tests show that the bonding force of the plating layer is good. The method has simple process, convenient operation, wide sources and low price of sodium carboxymethyl cellulose used, low cost and reduced precious metal pollution due to replacement of expensive Pd by nickel, can be suitable for most of plastics due to low activation temperature, and has high practical value and application prospect.
Owner:PLA SECOND ARTILLERY ENGINEERING UNIVERSITY

Method for controlling growth of graphene nanocrystalline carbon film by adjusting irradiation density of ECR ions

The invention provides a method for controlling the growth of graphene nanocrystalline carbon film by adjusting the irradiation density of ECR ions. According to the method, an ECR plasma sputtering system is utilized, the current of a third magnetic coil is adjusted to be changed within the range of 0-48A, argon ions are restrained by adopting a transition magnetic field mode, and a certain working pressure and microwave power are combined, so that the ion irradiation density in the preparation process of the carbon film is further changed. Nano-indentation and nano-scratching tests are carried out on the carbon films prepared under different ion irradiation densities, and when the current of the third magnetic coil varied from 0 A to 48 A, the ion irradiation density can vary from 1.88 mA/cm<2> to 26.89 mA/cm<2>, therefore, the graphene nanocystalline carbon film influenced by the ion irradiation densities within the range has the average size of the graphene nanocystalline from 0.66nm to 1.19 nm, the hardness from 6.45 GPa to 14.53 GPa, the elastic modulus from 116.30 GPa to 179.28 GPa, the friction coefficient from 0.07 to 0.38, and the scratch depth from 2.78 nm to 6.36 nm, and and has better mechanical and tribological properties.
Owner:SHENZHEN UNIV

Method and device of full-domain cutting force modeling in rotary ultrasonic vibration milling

The invention provides a method and a device of full-domain cutting force model in rotary ultrasonic vibration milling. By carrying out the kinematics analysis between a tool abrasive grain and a workpiece material interaction in the machining process, a technology parameter matching relation meeting the vibration separation of a cutting area is obtained, and a condition equation of an intermittent cutting characteristic is established; and according to an ultrasonic vibration auxiliary scratch test, critical press-in depth of ductility or brittleness removal mode changing of a material is obtained, the abrasive particle press-in depth distribution relation of the cutting area is established, the abrasive grain loads of different positions of the cutting area are accumulated, and ductilityor brittleness cutting force model is obtained correspondingly, the models are fused according to the critical press-in depth and the maximum cutting thickness, and the rotary ultrasonic vibration machining whole-domain cutting force model is obtained. According to the device, the rotary ultrasonic vibration machining characteristic and a removing mechanism can be more comprehensively reflected,so that the cutting force prediction and the technology optimization of the actual machining can be effectively guided.
Owner:BEIHANG UNIV

Abrasive particle shear fatigue test equipment

The invention discloses abrasive particle shear fatigue test equipment. The abrasive particle impact fatigue test equipment comprises abrasive particles fixedly connected with a tool head, a scratched test piece, a base system, an ultrasonic vibration system, a force measuring system and an acoustic emission system, wherein the ultrasonic vibration system is mounted on and connected with the base system; the tool head is fixedly connected with the ultrasonic vibration system; the acoustic emission system is mounted on and connected with the tool head; the force measuring system is mounted on and connected with the base system; the scratched test piece is fixedly connected with the force measuring system; the relative position between the scratched test piece and the abrasive particles is adjusted through the base system; the shear sliding between the abrasive particles and the scratched test piece is realized by the ultrasonic vibration system; the force measuring system is used for detecting dynamic force change between the abrasive particles and the scratched test piece; the acoustic emission system is used for carrying out acoustic emission of signals when the abrasive particles reach the fatigue rupture condition during the shear sliding process between the abrasive materials and the scratched test piece. The abrasive particle impact fatigue test equipment disclosed by the invention can quantize and compare the shear resistance of different abrasive particle materials, and meanwhile, provides the shear resistance time data, so as to achieve the theoretical guiding significance in the aspects of abrasive material manufacture, abrasive tool design and the like.
Owner:HUAQIAO UNIVERSITY

Suspended rotary rapid positioning in-situ indentation/deepened arc indentation testing device

The invention relates to a suspended rotary rapid positioning in-situ indentation/deepened arc indentation testing device and belongs to the field of mechanical and electronic integrated precise instruments. The device comprises a suspended rotary rapid positioning module, a deepened arc indentation testing module, a micro-nano indentation module and an in-situ observation module, wherein the micro-nano indentation module and the in-situ observation module are integrated on the suspended rotary rapid positioning module; the deepened arc indentation testing module is composed of an indentation tester and a test piece supporting platform together; and the test piece supporting platform is composed of two parts, namely a shear-type electric lifting table and an electric rotating platform. The device disclosed by the invention has the advantages that the device is novel in structure, has motor-driven rapid feed ability and micro-nano-level piezoelectric micro actuating ability, and can be used for accurately testing the hardness, elasticity modulus, scratching resistance and other mechanical property performances of the test materials. The loading displacement resolution reaches a micro-nano level, and the loading force resolution reaches a micro-Newton level. The effective test means is provided for mechanical behaviors and service behaviors of the materials.
Owner:JILIN UNIV

Full-strain measurement type in-situ nanometer impress/scratch testing device

The invention relates to a full-strain measurement type in-situ nanometer impress / scratch testing device, belonging to the field of an electric integrated precise scientific instrument. The full-strain measurement type in-situ nanometer impress / scratch testing device comprises a macro-adjustment mechanism, a precise pressing unit, a load and displacement signal detecting unit, and a scratch driving unit; the macro-adjustment mechanism is mounted on a base; the precise pressing unit is connected with an x direction sliding table of the macro-adjustment mechanism through a transition connection board; the load and displacement signal detecting unit comprises two groups of eight strain sheets; the strain sheets are respectively mounted on a flexible hinge and an x direction flexible hinge for detecting a load of the precise pressing unit in an embedded manner; and the scratch driving unit is connected with the base through a screw. Signal detection is carried out by using the internal strain sheets, so that the entire testing device has the advantages of compact structure and small size; and the entire testing device is conveniently mounted on carrier tables, such as a scanning electron microscope (SEM) or an X-ray diffraction meter, so that the in-situ impress and scratch test of the material can be realized. Therefore, the full-strain measurement type in-situ nanometer impress / scratch testing device provides technical support for researching a damage mechanism of the material.
Owner:中机试验装备股份有限公司
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