Preparation method for silver nano wire transparent conductive film capable of preventing corrosion of hydrogen sulfide gas

A transparent conductive film, silver nanowire technology, applied in cable/conductor manufacturing, circuits, electrical components, etc., can solve the problems that affect the continued use of conductive films, decrease in light transmittance and conductivity, and have not yet been provided, and achieve low cost. , Good conductivity and transmittance, anti-scratch effect

Inactive Publication Date: 2014-10-22
HEFEI INSTITUTES OF PHYSICAL SCIENCE - CHINESE ACAD OF SCI
View PDF5 Cites 19 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in practical applications, the silver nanowire transparent conductive film is easily corroded by corrosive gases (especially hydrogen sulfide gas) in the air and turns yellow and black, which leads to a decrease in its light transmittance and conductivity, and affects the continuation of the conductive film. use
At present, there is no report on a simple method for preparing a silver nanowire transparent conductive film that is resistant to hydrogen sulfide gas corrosion.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Preparation method for silver nano wire transparent conductive film capable of preventing corrosion of hydrogen sulfide gas
  • Preparation method for silver nano wire transparent conductive film capable of preventing corrosion of hydrogen sulfide gas
  • Preparation method for silver nano wire transparent conductive film capable of preventing corrosion of hydrogen sulfide gas

Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0023] (1) Preparation of transparent conductive film substrate: Ultrasound the glass substrate or PET substrate in ethanol, acetone, and deionized water for 20 minutes respectively, after drying, clean it with a plasma cleaner for 15 minutes to make the surface hydrophilic;

[0024] (2) Preparation of silver nanowire transparent conductive film: use 3M adhesive tape (12.7mm wide x 33m long) to fix the substrate on the horizontal platform, take the silver nanowire colloid, scrape it on the fixed substrate with a glass rod, and blow it with a hair dryer Dry;

[0025] (3) Post-treatment of silver nanowire transparent conductive film. If it is a glass substrate, heat it on a heating plate at 200C for 20 minutes and then cool down naturally; if it is a PET substrate, process it with a press at 30MPa;

[0026] (4) Preparing a protective agent, taking PVA as an example: 5g of PVA can be dissolved in 95g of deionized water, heated and stirred at 90°C for 6h, and a 5% PVA aqueous sol...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention discloses a preparation method for a silver nano wire transparent conductive film capable of preventing corrosion of a hydrogen sulfide gas. The method comprises: scratching or sparying a silver nano wire colloid on an appropriate substrate to obtain a low-conductivity silver nano wire transparent conductive film; then carrying out post treatment of high temperature, high voltage and the like to obtain a high-transparency high-conductivity silver nano wire transparent conductive substrate; and then preparing a protective agent solution, diluting the protective agent solution in a large proportion, according to the type and size of the substrate selected for the silver nano wire film, selecting an appropriate spraying instrument or a spin coating instrument, preparing a protective layer of a thin layer on the surface of the substrate film, and finally, solidifying the protective layer through natural drying, heating by use of a heating plate or blow-drying by use of a blower. The silver nano wire transparent conductive film prepared by use of the method provided by the invention can prevent corrosion of gases such as the hydrogen sulfide gas and the like, can prevent scratches and has good conductivity and transmittance through a 3M adhesive tape and a pencil scratch test. The operation is simple, the cost is low, and large scale production can be carried out.

Description

technical field [0001] The invention relates to a preparation method of a silver nanowire transparent conductive film, in particular to a preparation method of a silver nanowire transparent conductive film resistant to hydrogen sulfide gas corrosion. Background technique [0002] In recent years, due to its better characteristics than ITO, silver nanowires have shown good prospects in the practical application of transparent electrodes, touch screens, solar cells and other small devices. In the future, the silver nanowire transparent conductive film will also be used for large devices such as game consoles and touch screens above 46 inches. [0003] There are various preparation methods for the silver nanowire transparent conductive film, such as scraping method, spraying method and so on. However, in practical applications, the silver nanowire transparent conductive film is easily corroded by corrosive gases (especially hydrogen sulfide gas) in the air and turns yellow and...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): H01B13/00
Inventor 王可何微微冉云霞季书林叶长辉
Owner HEFEI INSTITUTES OF PHYSICAL SCIENCE - CHINESE ACAD OF SCI
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products