The invention relates to the technical field of
ceramic capacitors, in particular to a lead-free high-
voltage pulse-resistant
energy storage multilayer
ceramic capacitor and a preparation method thereof. The method comprises the steps that
ceramic powder, a
solvent, a dispersing agent, a
plasticizer and a
silicon-based defoaming agent are subjected to ball milling to obtain
slurry, and the lead-free high-
voltage-pulse-resistant
energy storage multilayer
ceramic capacitor is obtained through the processes of
tape casting,
screen printing, lamination, lamination,
cutting, glue discharging,
sintering, chamfering, end sealing, end burning and
electroplating in sequence. The thickness of the film is 25-40 [mu] m; 70 Ag-30 Pd, 60 Ag-40 Pd or 90 Ag-10 Pd
electrode slurry is used as an inner
electrode material, and
drying is carried out at the temperature of 65-75 DEG C after printing; the soft pressing temperature is 60-80 DEG C, the soft pressing pressure is 12-15 MPa, and the pressure
holding time is 15-18 s; the lamination pressure is 40 MPa to 55 MPa, and the pressure maintaining time is 10 min to 30 min; the glue discharging temperature is 265-325 DEG C, and the temperature is kept for 7-11 hours; the
sintering temperature is 1050-1200 DEG C, and the
sintering time is 2-4 hours; in the
electroplating process, the
nickel plating current ranges from 19 A to 21 A, and the time ranges from 90 min to 120 min; the
tin plating current is 13A-15A, and the time is 90 minutes to 120 minutes.