Patents
Literature
Patsnap Eureka AI that helps you search prior art, draft patents, and assess FTO risks, powered by patent and scientific literature data.

63 results about "Grain orientation" patented technology

The grain orientation of every piece of wood that goes into a real wooden vessel is specifically chosen for the purpose the piece will serve. Wood is stronger in its vertical grain direction than the horizontal or face grain direction, as anybody who's ever played baseball knows.

Dynamic stress regulation and control method of crusher in bio-fertilizer production process

The invention relates to the technical field of bio-fertilizer crushing, and discloses a dynamic stress regulation and control method of a crusher in a bio-fertilizer production process, which comprises the following steps: arranging a non-uniform gradient microgroove array arranged according to a Fibonacci sequence on a working surface of a cutter, filling a beta-glucan-based viscoelastic composite material in the microgrooves, the grain orientation of a tool matrix is regulated and controlled through an electromagnetic field-assisted directional solidification process, and a dynamic stress wave self-interference regulation and control system is constructed. Through the synergistic effect of geometric arrangement of the microgroove array and the nonlinear damping characteristic of the viscous-elastic material, the destructive interference effect of stress waves is spontaneously formed in the crushing process, and space equalization and peak suppression of dynamic stress of the working face of the cutter are achieved; the problems of stress concentration and tool fatigue of a traditional crusher in high-fiber and high-viscosity bio-fertilizer raw material processing are fundamentally solved, the crushing efficiency is remarkably improved, and the service life of equipment is remarkably prolonged.
Owner:CHANGSHA XINYUAN AMINO ACID BIOLOGICAL FERTILIZERCO

Multi-scale simulation method for thermal compression deformation behavior of TC4 titanium alloy

The invention discloses a multi-scale simulation method for a thermal compression deformation behavior of TC4 titanium alloy, and belongs to the field of metal material processing simulation. Comprising the following steps: 1, carrying out thermal compression experiments at different temperatures to obtain a deformed sample; 2, analyzing the grain orientation, orientation difference angle and texture evolution of the sample by using an electron back scattering diffraction technology; 3, constructing a crystal plasticity finite element model, and simulating a polycrystalline deformation process; 4, constructing a molecular dynamics model, and simulating phase change and dislocation evolution in thermal compression and cooling processes; and 5, based on a multi-scale simulation result, hot working parameters are optimized, dynamic recrystallization and a beta-to-alpha phase change path are regulated and controlled, and grain refinement and performance homogenization are achieved. The invention discloses a correlation mechanism of the microstructure and the mechanical property in TC4 titanium alloy thermal compression deformation, and provides a theoretical basis for optimization of a thermal processing technology of a high-performance titanium alloy component in the aerospace field.
Owner:TIANJIN UNIVERSITY OF TECHNOLOGY

Welded joint fatigue weak area evaluation method based on crystal plasticity

The invention discloses a method for evaluating a fatigue weak area of a welded joint based on crystal plasticity, which aims at the problem of fatigue failure of the welded joint caused by complex microstructures such as grain orientation difference and uneven grain size distribution, establishes a quantitative correlation model of grain orientation and size evolution through CPFEM, and combines a macro-micro cross-scale analysis method to evaluate the fatigue weak area of the welded joint. And precise prediction of local stress concentration and crack initiation behaviors of the welding joint under a real fatigue load working condition is realized, so that scientific evaluation of a fatigue weak region is completed. According to the method, an innovative framework of fatigue weak area evaluation is constructed through load working condition reduction and grain characteristic multi-scale coupling, so that excessive simplification of a traditional method on real load conditions is made up, the limitation that a traditional model is difficult to couple a microstructure and a real load is overcome, and the fatigue weakening quantization precision is remarkably improved; and a high-precision analysis technology is provided for anti-fatigue design, process optimization and service life evaluation of the engineering welding structure.
Owner:EAST CHINA UNIV OF SCI & TECH

Hard alloy cutter life prediction and material selection method and system based on working condition parameters

The invention discloses a hard alloy cutter life prediction and material selection method and system based on working condition parameters, and relates to the technical field of hard alloy cutter manufacturing, and the method comprises the steps: collecting cutting force distribution and temperature gradient data through a cutter tip area stress sensing array and a temperature sensing array, and constructing stress-temperature-wear synergistic effect data; calculating a fatigue damage characteristic value based on the synergistic effect data to obtain a wear prediction correction coefficient; compensating the tool nose stress field by using the correction coefficient, and outputting life prediction data; and designing a carbide phase gradient distribution structure according to the synergistic effect data and the fatigue damage characteristic value, adjusting a carbide grain orientation angle in combination with the wear prediction correction coefficient and the life prediction data, outputting optimal material structure parameters, and realizing optimal selection of the hard alloy cutter material. According to the method, the cutter service life prediction precision is improved, and the dynamic optimization of the material structure is realized.
Owner:HUNAN CLOUD BUSINESS MANAGEMENT CO LTD

A method for simulating and controlling recrystallization defects of a second generation nickel-based single crystal superalloy and a second generation nickel-based single crystal superalloy

The application discloses a kind of second generation nickel-based single crystal superalloy recrystallization defect simulation and control method.The method steps are: according to sample preparation wax mold, after sand blasting, dry baking, manufacture ceramic shell;Through directional solidification preparation second generation nickel-based single crystal superalloy sample, control pulling speed, holding temperature and temperature gradient and other parameters;According to service condition preparation sample, simulate stress loading, in combination with heat treatment simulate actual service environment;Using electron backscattering diffraction and X-CT imaging, characterize recrystallization grain orientation distribution, three-dimensional morphology, content and thickness.Process parameter-defect characteristic mapping relationship is established, the stress distribution characteristics during preparation are clarified, the ceramic shell and preparation process are feedback controlled, and the control of recrystallization defects is realized.The application simulates the actual service environment of high-temperature alloy blade, and restores the performance of recrystallization defect sample in actual service environment.The application provides an experimental reproduction method and effective process control strategy for recrystallization defect research.
Owner:SHANGHAI UNIV +1

Electrolytic copper foil with preferred orientation of (200) crystal face as well as manufacturing method and application of electrolytic copper foil

The present invention relates to an electrolytic copper foil having a preferred orientation of a (200) crystal plane, a method for manufacturing the same, and an application thereof, in which the electrolytic copper foil before heat treatment has a crystal grain orientation ratio of 20% or less in the (200) crystal plane as measured by XRD analysis, and a crystal grain orientation ratio of less than 20% in a {001} crystal plane family as measured by EBSD analysis; the electrolytic copper foil after heat treatment has a crystal grain orientation ratio in the (200) crystal plane of 50% or more as measured by XRD analysis and a crystal grain orientation ratio in the {001} family of crystal planes of 20% or more as measured by EBSD analysis. And the heat treatment is heating at 200 DEG C for two hours. The electrolytic copper foil subjected to heat treatment has a microstructure similar to that of a rolled and annealed copper foil and shows excellent mechanical properties.
Owner:DUPONT ELECTRONICS INC

Grain-oriented electromagnetic steel sheet and method for producing same

The grain-oriented electrical steel sheet includes a base steel sheet having a predetermined chemical composition, a glass coating provided on a surface of the base steel sheet, and a tension-applying insulation coating provided on a surface of the glass coating. The base steel sheet has a texture oriented in the Goss orientation. In the base steel sheet, when an average dispersion angle from an ideal Goss orientation with a rolled surface normal direction ND as the rotation axis is defined as α (°), an average dispersion angle from the ideal Goss orientation with an orthogonal-to-rolling direction TD as the rotation axis is defined as β (°), and an average dispersion angle from the ideal Goss orientation with a rolling direction RD as the rotation axis is defined as γ (°), α, β, and γ satisfy the following formula (1). 0.0≤β<2.5<α<4.0≤γ≤10.0
Owner:NIPPON STEEL CORPORATION

Preparation method for regulating ferroelectric texture ceramic grain size by phase field method

The application discloses a preparation method for regulating and controlling ferroelectric texture ceramic grain size by using a phase field method simulation technology, and comprises the following steps: preparing a series of microcrystalline powders with different size distributions; setting an initial phase field structure meeting the particle size distribution; establishing a phase field model for grain orientation growth; simulating and analoging the grain orientation growth process; preparing a film; preparing a green body with microcrystalline parallel distribution; and preparing ferroelectric texture ceramics with target grain size distribution. The application fully utilizes the computer simulation intelligent prediction guidance technology, does not need repeated trial and error experiments, saves time and effort, has good product reproducibility and stability, easily realizes accurate control of the ferroelectric texture ceramic grain size distribution, and is easy to be industrialized; the application effectively controls the occurrence of grain abnormal growth, maintains high grain orientation, and promotes the densification of the ceramic; and the application can not only prepare high-texture-density ferroelectric ceramics, but also regulate and control the grain size.
Owner:SHANXI AGRI UNIV

Method for producing a sheet core, clamping system for a sheet stack and device for producing a sheet core

Method for producing a stacked grain-oriented sheet core (O) for a transformer from a sheet stack (W), clamping system (9) and apparatus (1); the method provides for preparing a sheet stack (W) comprising one or more sheets (P) made of grain-oriented electrical steel; said sheet stack (W) is grabbed by a clamping system (9); the sheet stack (W) is placed on an assembly table (7; 7I; 7II; 7III; 7IV); during the placing step, the sheet stack (W) falls in free fall along a path (tx1).
Owner:L A E LUGHESE ATTREZZATURE PER LELETTROMECCANICA SRL

Method and device for determining grain orientation

A method for determining grain orientation is used for identifying grain orientation in an image of a metallographic sample, the metallographic sample is a non-deformable alloy and is provided with a matrix and a second phase, and the second phase is provided with a habitual plane in the plane direction of the matrix {111} and is of a strip-shaped or disc-shaped structure. The method comprises the following steps: measuring an included angle between second phases in the same crystal grain on the surface of a metallographic sample, establishing a virtual regular tetrahedron of a matrix {111} plane, and calculating an angle relation between the surface of the metallographic sample and the matrix {111} plane according to the included angle between the second phases so as to determine the crystal grain orientation. According to the method, the grain orientation is calculated by utilizing the geometrical characteristics of the alloy structure, the method is simple, the requirement on the surface state of the sample is low, the characterization efficiency is effectively improved, and the test cost is reduced. The invention further provides a device for determining the grain orientation.
Owner:AECC COMML AIRCRAFT ENGINE CO LTD

Method for producing grain-oriented electromagnetic steel sheet

To provide a method for stably producing a grain-oriented electromagnetic steel sheet having low iron loss.SOLUTION: A method for producing a grain-oriented electromagnetic steel sheet comprises: hot rolling a steel slab to produce a hot-rolled sheet; after performing a first cold rolling and a first intermediate annealing without subjecting the hot-rolled sheet to hot band annealing, further performing cold rolling, as performed between the first cold rolling and the first intermediate annealing, twice or more to produce a cold-rolled sheet of final thickness; applying decarburization annealing that also serves as a primary recrystallization annealing to the cold-rolled sheet; and after that, performing a finish annealing to induce a secondary recrystallization. In the method, the rolling reduction ratio of the first cold rolling shall be 20% or more and less than 60%, and thereby, the area ratio of the crystal grains with a GAM value of 0.5 or less, observed by EBSD on a cross section perpendicular to the rolling direction of the steel sheet after the first intermediate annealing, shall be 80% or more. In addition, the ODF intensity of the {100}<011> orientation at the center of the sheet thickness of the steel sheet after decarburization annealing shall be more than 0.50 and not more than 1.5.SELECTED DRAWING: None
Owner:JFE STEEL CORP

High-strength weak-texture Cu-Ni-Si alloy and preparation method thereof

PendingCN121555925AHigh densityAlloy
The invention provides a high-strength weak-texture Cu-Ni-Si alloy and a preparation method thereof.The preparation method comprises the following steps that a Cu-Ni-Si alloy block is sequentially subjected to first-stage cryogenic multidirectional forging, first aging treatment, second-stage cryogenic multidirectional forging and second aging treatment, and the high-strength weak-texture Cu-Ni-Si alloy is obtained. According to the scheme, a two-step cryogenic multidirectional forging and two-stage aging composite process is adopted, multidirectional twin variants are activated in the forging process, the twin crystal-dislocation interface density is improved, and high-density nucleation sites are provided for a precipitated phase; the two-stage aging promotes a precipitated phase to be uniformly dispersed and precipitated, grain refinement and precipitation strengthening collaboration are achieved, and the strength is remarkably improved while the high conductivity is kept; the multidirectional forging can also weaken the texture, randomize the grain orientation, eliminate the anisotropy, ensure the consistency of mechanical properties in all directions, reduce the cracking risk and prolong the fatigue life.
Owner:HARBIN INST OF TECH

A test method for the second type of residual stress of 4J33 Kovar alloy

The present invention discloses a method for testing the second type of residual stress of 4J33 Kovar alloy, which relates to the field of analytical instruments and material testing technology. The method comprises the following steps: loading an annealed stress-free specimen and a specimen pre-stressed with equibiaxial known stress into a nanoindenter; performing a nanoindentation experiment on the grains entering a marked circle with the test point as the center and twice the average grain size as the radius, obtaining all indentation data pressed into each grain in the marked circle; averaging all indentation data pressed into each grain in the marked circle to obtain an average value of indentation data corresponding to each grain in the marked circle; summing and averaging the average values ​​of indentation data corresponding to all grains in the marked circle to obtain an average value of indentation data corresponding to all grains in the marked circle, and substituting the average value into a residual stress calculation model to obtain the second type of residual stress. The present invention can effectively reduce the influence of grain orientation differences on the accuracy of residual stress testing using the nanoindentation method.
Owner:XI AN JIAOTONG UNIV

A weld ultrasonic beam path correction method of a crystal grain graph neural network

The application discloses a kind of grain map neural network's weld ultrasonic beam path correction method, it is related to the field of welding structure nondestructive testing, by obtaining the EBSD data of weld area, extract grain orientation, grain boundary type and spatial distribution characteristics, construct grain map structure, and calculate initial propagation time weight based on anisotropic sound velocity model;Using graph neural network to learn end to end for grain node and grain boundary edge features, output corrected edge propagation time weight;The time of flight from element to imaging pixel is obtained by shortest path search, and the time of flight predicted by neural network surrogate model is fused and corrected;Finally, the corrected time of flight is used to perform full focus imaging, and the weld defect image after optimizing the beam path is obtained.The method combines material microstructure characteristics and machine learning model, solves the problem that the beam path description is not fine enough in existing weld ultrasonic testing, significantly improves the accuracy and reliability of defect detection.
Owner:DATANG BOILER & PRESSURE VESSEL INSPECTION CENTER CO LTD +3

Grain-oriented electromagnetic steel sheet and method for manufacturing same

The present invention has as its object to provide grain-oriented electrical steel sheet further improved in core loss in control of magnetic domains by forming laser grooves in steel sheet after decarburization annealing and before finish annealing. The grain-oriented electrical steel sheet according to the present invention is a grain-oriented electrical steel sheet having a plurality of grooves on the surface of the steel sheet and provided with a glass coating on that surface, which grain-oriented electrical steel sheet characterized in that an absolute value of an angle θ formed by a direction perpendicular to both a rolling direction and sheet thickness direction of the steel sheet and a longitudinal direction of the grooves is 0 to 40°, a width W of the grooves is 20 to 300 µm, a depth D of the grooves is 10 to 40 µm, and a pitch P of the grooves in the rolling direction is 1.0 to 30 mm and in that the relationship of formula (1) is satisfied when a thickness of the glass coating of flat parts of the steel sheet surface (parts other than grooves) is t1 and the thickness of the glass coating at the deepest parts of the grooves is t2: t2 / t1<1.00
Owner:NIPPON STEEL CORPORATION

Wire rod for adhesive tape steel wire and production control method for grain orientation of wire rod

The invention discloses a wire rod for an adhesive tape steel wire and a production control method for grain orientation of the wire rod. The wire rod comprises the following chemical components in percentage by mass: 0.80%-0.86% of [C], 0.15%-0.35% of [Si], 0.40%-0.55% of [Mn], 0.0030%-0.012% of [P], 0.0040%-0.010% of [S], 0.0010%-0.0040% of [N], 0.0010%-0.0020% of total oxygen, 0.0010%-0.0035% of [Als], 0.00005%-0.0005% of [Ca], 0.00004%-0.0004% of [Se], 0.01%-0.05% of [Cr], less than or equal to 0.02% of [Ni] and the balance of Fe and inevitable impurities. According to the invention, systematic design is carried out from the aspects of chemical components, a smelting process and a rolling process, microalloying is carried out by adopting elements such as aluminum and selenium, the continuous casting process is operated at a constant pulling speed, and the content proportion of pearlite, proeutectoid ferrite and troostite structures of the wire rod is controlled, so that the large-angle grain boundary proportion of the wire rod is greater than 10%; and the metallographic structure requirement of a user on the wire rod for the adhesive tape steel wire is met.
Owner:ANGANG STEEL CO LTD

Method for eliminating surface lenticular defects of ferritic stainless steel cold plate

The application discloses a method for eliminating lisdin grain defects on the surface of ferrite stainless steel cold plates, which comprises the following steps: optimizing continuous casting process, controlling the overheating degree of molten steel at 25-40 DEG C; controlling the electromagnetic stirring intensity as follows: current 1400-1600 A, frequency 3.0-4.0 Hz, and commutation time 10-20 s; controlling the wide surface intensity of crystallizer cooling water at 2600-2800 L / (min.m), controlling the narrow surface intensity of crystallizer cooling water at 2400-2700 L / (min.m), and controlling the cooling water intensity of the secondary cooling section at 1.10-1.30 L / kg; controlling the hot rolling temperature, controlling the rough rolling temperature at 1000-1100 DEG C, and controlling the final rolling temperature of the finishing rolling at 780-880 DEG C; for the cold plates with a thickness of less than 2.0 mm, controlling the total cold rolling deformation rate at more than 70%; and for the cold plates with a thickness of more than 2.0 mm, controlling the total cold rolling deformation rate at not less than 60%. According to the method, the equiaxed crystal ratio of the ferrite stainless steel continuous casting billet is increased to more than 55% by optimizing and controlling the continuous casting process parameters, and finally the grain orientation distribution on the surface of the cold plate is uniform, there is no obvious grain cluster, and the lisdin grain defects on the surface of the ferrite stainless steel cold plate are effectively eliminated by controlling the hot rolling temperature and the total cold rolling deformation rate.
Owner:SHANXI TAIGANG STAINLESS STEEL CO LTD

Fibrous grain three-dimensional crystal modeling and analyzing method and device

The invention discloses a fibrous grain three-dimensional crystal modeling and analyzing method, and belongs to the technical field of finite element analysis. The method comprises the following steps: acquiring a metal wire material fiber grain sample, processing to obtain a ctf file, and importing the ctf file into MATLAB to obtain grain orientation information and grain size distribution data; based on the grain size distribution data, constructing a three-dimensional fibrous grain model to obtain a geo file; importing the geo file into Gmsh software, and carrying out grid division to generate an inp file; on the basis of the grain orientation information, Euler angles with the same number as the three-dimensional fibrous grain models are screened by adopting an Euler angle screening method to obtain Euler angle data, and the Euler angle data passing verification are processed to obtain grain orientation parameters; the grain orientation parameters and the inp file are input into ABAQUS, and independent material attributes related to each grain are generated; finite element analysis is conducted on the fiber crystal grain sample according to the independent material attribute of each crystal grain, an analysis result is obtained, and the modeling accuracy of the fibrous crystal grains is improved through the method.
Owner:WUHAN UNIV OF TECH

Method and system for predicting service life of heat-resistant steel based on low-cycle fatigue crack evolution and fracture

The invention belongs to the technical field of heat-resistant steel life prediction, and discloses a heat-resistant steel life prediction method and system based on low-cycle fatigue crack evolution and fracture, and the method comprises the steps: collecting the original structure morphology of austenitic heat-resistant steel, and obtaining the average grain size and grain orientation characteristics; and calculating the maximum Schmidt factor and the minimum Schmidt factor of each crystal grain by traversing a crystal grain slippage system. Meanwhile, a dislocation slippage theory is taken as a core, a low-cycle fatigue test is combined, shear stress, friction stress, Poisson's ratio and a plastic strain range are introduced, a low-cycle fatigue slippage zone length c and a crack tip fatigue slippage length increment delta CTSD are calculated, elastic and plastic strain tensors and a fatigue hysteretic curve are fused, and a crack tip fatigue slippage zone length delta CTSD is calculated. The crack growth rate and the crack length change rule under different circulation cycles can be accurately obtained, and the prediction error of a general model is reduced. The prediction accuracy of the fracture life of the austenitic heat-resistant steel can be greatly improved, potential safety hazards and resource waste are reduced, and stable operation of equipment under the high-temperature working condition is guaranteed.
Owner:TIANJIN UNIV

Method for analyzing residual stress field of laser shot peening of aviation aluminum alloy with texture

A kind of method for analyzing residual stress field of laser shot peening of aviation aluminum alloy containing texture, based on X-ray diffraction method, grain orientation information and laser shot peening finite element simulation result analysis residual stress, using chemical milling to strip layer, based on X-ray diffraction, grain orientation information and ABAQUS laser shot peening finite element simulation, the residual stress field generated by laser shot peening of 2024T351 aluminum alloy is analyzed, it is a complete method suitable for residual stress analysis of strong texture material, the method is aimed at the problem of layer-by-layer stripping of material, the anisotropy phenomenon caused by grain preferred orientation and the problem of poor data reliability, the method of analyzing residual stress by X-ray diffraction is optimized in details, including the combined application of chemical milling stripping layer, residual stress calculation considering grain orientation information and data screening.The present application makes the inner surface of chemical milling window flat by plane layer-by-layer stripping, which has a positive effect on improving the accuracy of residual stress test, and reliable stress data is obtained.
Owner:NORTHWESTERN POLYTECHNICAL UNIV +1

Multifunctional grain orientation silicon steel sheet demagnetization equipment and demagnetization method thereof

The invention discloses multifunctional grain orientation silicon steel sheet demagnetization equipment which comprises an optical detection module, a non-magnetic scale carrier module, a weighing module and a demagnetization moving module. The non-magnetic scale carrier module is fixedly installed on the supporting platform through the supporting frame, the supporting frame is installed close to the supporting stand column, the weighing module is arranged in the supporting frame and fixedly installed on the supporting platform, and the degaussing moving module is fixedly installed on the supporting platform and installed on one side of the supporting frame. The equipment can measure the geometric dimension, measure the included angle between the sample extension direction and the cutting direction, judge whether burrs exist on the edge of the sample or not, measure the dimension of the sample and demagnetize the sample.
Owner:CHANGSHU INSTITUTE OF TECHNOLOGY

Weak-texture medium-entropy alloy for additive manufacturing and processing method of weak-texture medium-entropy alloy

The invention provides a weak-texture additive manufacturing medium-entropy alloy and a processing method thereof, and belongs to the technical field of medium-entropy alloys. The CoCrNi-based medium-entropy alloy forms orderly-arranged columnar crystals after additive manufacturing, the medium-entropy alloy subjected to additive manufacturing is subjected to heat treatment under the specific condition, crystal grains in the medium-entropy alloy grow again in a recrystallization mode, a discontinuous sigma phase and a discontinuous L12 phase are separated out, the discontinuous L12 phase separated out at the high temperature promotes grain boundary migration, and therefore the grain boundary migration is promoted. The effect of grain refinement is achieved; due to the fact that discontinuous precipitation phases are different in migration pushing direction and speed of each grain boundary, the randomness of the grain growth direction is enhanced, the generated grain orientation is more uniform, the strong texture generated by additive manufacturing is weakened, and meanwhile the strengthening effect of the precipitation phases enables the material to have the excellent mechanical property.
Owner:EAST CHINA UNIV OF SCI & TECH

Multi-scale collaborative analysis method for sintering microstructure of MLCC ceramic body

The invention discloses a multi-scale collaborative analysis method for a sintering microstructure of an MLCC ceramic body, and the method comprises the steps: cutting an MLCC ceramic sample, and carrying out the layer-by-layer scanning through FIB equipment, and obtaining three-dimensional image data; the grain orientation change is monitored through high-temperature EBSD equipment, and the form, size and distribution of grains are recorded; in combination with FIB-SEM and EBSD data, grain size, porosity and grain orientation are extracted, and a microstructure-performance relation model is established by utilizing regression analysis and a neural network; a deep Q network or deep reinforcement learning is adopted to optimize multi-scale model parameters, new data in the sintering process are adjusted in real time, the relation among microcosmic, mesoscopic and macroscopic scales is optimized, the optimization requirements of all scales are balanced through a multi-objective optimization method, and the macroscopic performance is improved.
Owner:GUANGDONG FENGHUA BANGKE ELECTRONIC CO LTD +1

Preparation method of preferred orientation copper foil

The invention discloses a preparation method of a preferred orientation copper foil, and relates to the technical field of metal material processing. According to the method, the copper raw material is subjected to plastic deformation through an asymmetrical rolling process, high-density dislocation and deformation energy storage are introduced, then a multi-stage annealing process is adopted, temperature gradient and heat preservation time regulation and control are combined, and collaborative optimization of grain recrystallization and preferred orientation is achieved. Through the synergistic effect of rolling deformation and annealing, the copper foil with the grain orientation consistency larger than or equal to 95% and the thickness of 0.1-1 mm can be prepared, and the method has the advantages of being low in defect and high in orientation consistency and is suitable for macro production in the fields of power transmission, electronic packaging, flexible circuits and the like.
Owner:ELECTRIC POWER RES INST OF GUANGXI POWER GRID CO LTD

A method of preparing a composite coating for a back mold insert

The present application relates to a kind of preparation methods of post mould insert composite coating in the field of mould accessory manufacturing, comprising: extracting grain orientation and interface bonding state information from initial transition layer surface, using ion beam scanning technology to analyze grain distribution uniformity and interface stress, determine coating bonding force basic parameter;According to microdefect distribution data, the influence degree of defect on thermal fatigue resistance is analyzed by combining preset threshold range, and the real-time evaluation result of coating performance is obtained;Improved gradient composite coating is generated by optimized deposition process, and the change trend of microdefect is scanned again using online detection system, to determine the improvement range of coating durability and production efficiency;Key performance indicators are extracted from simulation results, combined with the data log of online detection system, process parameters are iteratively optimized by gradient descent algorithm, and the final stable coating preparation scheme is obtained.
Owner:DONGGUAN LONGCHI MOLD ACCESSORIES CO LTD

Grain structure engineering for metal gapfill materials

A method for depositing copper onto a substrate includes grain engineering to control the internal structure of the copper. In some embodiments, the method comprises depositing a grain control layer conformally onto a copper seed layer in a structure on the substrate where the grain control layer is a non-conducting material, etching the grain control layer using a direct deep reactive ion etch (DRIE) process to remove portions of the grain control layer on horizontal surfaces within the structure, and depositing a copper material onto the structure such that at least one grain parameter of the copper material is controlled, at least in part, by a remaining portion of the grain control layer on vertical surfaces of the structure. In some embodiments, the deposited copper material in the structure has a <111> grain orientation normal to a horizontal surface of the structure.
Owner:APPLIED MATERIALS INC

A method, system and medium for controlling the volume fraction of variants in high-temperature alloys

This application discloses a method, system, and medium for controlling the volume fraction of variants in a superalloy, relating to the fields of materials science and engineering. The method comprises: obtaining grain orientation data of any target superalloy sample and constructing a finite element model; obtaining the volume fractions of various variants in the target superalloy sample after electrolytic corrosion; performing tensile tests on the target superalloy sample at different temperatures and different tensile rates to obtain the material properties and true stress-strain curve of the target superalloy; using finite element software that imports the finite element model and a crystal plasticity constitutive model, sequentially performing tensile simulations and creep simulations of the target superalloy to determine the optimal operating conditions corresponding to the expected volume fraction of variants in the target superalloy; and, under the optimal operating conditions, heat treating the target metal alloy using a creep tensile machine to obtain the target superalloy with the expected volume fraction of variants. This application enables precise control of the volume fraction of variants in a superalloy.
Owner:DONGGUAN UNIV OF TECH

Grain-oriented electrical steel sheet and method for manufacturing same

A grain-oriented electrical steel sheet according to an embodiment of the present disclosure includes: an electrical steel sheet substrate; and an insulating film layer that is disposed on the electrical steel sheet substrate. At least one deformation portion having a linear shape is formed on a surface of the electrical steel sheet substrate, and a natural corrosion potential value of the electrical steel sheet is -350 mV or more.
Owner:POHANG IRON & STEEL CO LTD

Tantalum target material, method for producing the same, and use thereof

The application belongs to the field of target material preparation, and particularly discloses a tantalum target material, a preparation method and application thereof. In the method, stress annealing, cold forging and heat treatment, two-stage rolling in different directions, intermediate static pressure treatment and recrystallization annealing are sequentially performed on a tantalum ingot, and each step is matched with each other, so that the tantalum target material has more uniform grain distribution, finer grains and a higher proportion of {111} grain orientation, thereby controlling the sputtering rate and sputtering stability, improving the uniformity of sputtering film and achieving the purpose of improving the film quality.
Owner:PIONEER FILM MATERIALS (ANHUI) CO LTD

A method for rapid non-destructive evaluation of material strength and plasticity based on EBSD data

The application relates to the technical field of material performance evaluation, and provides a material strength and plasticity rapid nondestructive evaluation method based on EBSD data, which comprises the following steps: adopting an EBSD technology to characterize a material surface state, obtaining a backscattering diffraction pattern and obtaining original EBSD data and a grain orientation map of the material; based on the reconstructed grain orientation map, microstructure characteristic parameters of each grain in a target region of the sample are extracted respectively; based on the extracted microstructure characteristic parameters, a plasticity sensitivity coefficient of each grain is calculated; based on the slip distribution characteristics of the grains under the plasticity sensitivity coefficient, the target region of the sample is divided into a plasticity deformation dominant area and a strength dominant area, and partition visualization is realized through space mapping and different color filling; and based on the respective microstructure characteristic parameters of the areas, microstructure-mechanical property evaluation models are respectively established, so that the material strength and plasticity are rapidly evaluated.
Owner:EAST CHINA UNIV OF SCI & TECH