A quantitative detection method of
thallium content in converter
graphite ball, steps include: 1) the pretreatment of converter
graphite ball; 2) the preparation of
standard solution series; 3) the detection of
thallium content in converter
graphite ball.The application finds that the suitable
pretreatment method of converter graphite ball is carbon removal by burning, and then high-
chloric acid and dilute
nitric acid are used to dissolve salt, by which the converter graphite ball can be completely dissolved, thereby the stability of
quantitative determination of
thallium content in converter graphite ball is improved, the
pretreatment method is simple, fast and operable; the method is suitable for the quantitative detection of thallium content in converter graphite ball with thallium content not less than 0.0062 μg / L, the
recovery rate of thallium is as high as 99.1%, the analysis accuracy is high, the detection
lower limit is as low as ppb level, the sensitivity is high, and the method has the advantages of simple operation, simple analysis condition and low labor intensity.Therefore, the application has significant
economic benefits and the advantages of simplicity and economy.