The invention discloses a method for recovering ethyl pyrimidinol from pirimiphos-methyl synthesis
wastewater. The method comprises the following steps: sequentially carrying out primary extraction,
alkaline hydrolysis, secondary extraction, decoloration, pH value adjustment to 6-7,
reflux and cooling
crystallization on the
wastewater. According to the method disclosed by the invention, other organic matters in the
wastewater can be effectively removed, the product quality is improved, the ethyl pyrimidinol with high purity and high yield can be obtained, the
recovery rate is greater than 99%, the purity exceeds 99%, the
water content is very low, the obtained ethyl pyrimidinol can be used as a
raw material to be directly used for synthesizing a pirimiphos-methyl
active compound, the
utilization rate of the ethyl pyrimidinol is effectively improved, and the method is suitable for industrial production. The method has the advantages of simple process, convenience in operation, low
recovery cost, mild
reaction conditions, high
recovery efficiency, high purity of recovered products, environment friendliness and the like, effectively solves the problem of stink of the ethyl pyrimidinol recovered by the original method, and obviously reduces the three-
waste treatment cost by outsourcing or
incineration treatment, and meanwhile, the method has the advantages of simple process, convenience in operation, low recovery cost, mild
reaction conditions, high recovery efficiency, high purity of the recovered products, environment friendliness and the like.