The invention discloses a
reaction product separation device and a
separation method. The
reaction product separation device comprises a circulating
tower, a pressure pump, a cooler, a water removal tank, a
dehydration tower, a feeding pump and a product
tower which are connected in sequence, the product tower is connected with the circulating tower; the circulating tower is also connected with the
raw material water separation tank; by adopting an operation method of
coupling decantation non-sharp separation rectification and
variable pressure crushing azeotropy, the separation device can be used for continuously separating reaction products of a process for preparing
methyl acrylate from
methyl acetate-
formaldehyde in industry, and is simple in process, small in equipment number, simple and convenient to operate and suitable for industrial large-
scale separation.