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1208 results about "Perfluoropolyether" patented technology

Perfluoropolyether (PFPE) is a type of liquid lubricant used in the aerospace industry for over 30 years. The main properties of PFPE are being temperature resistant between 215 K–530 K (depending on specific composites), having very low outgassing compared to other fluids (vapour pressure of 6e-8 torr) and having a dielectric strength of around 15.7 MV/m.

Method for synthesizing novel perfluoropolyether alkoxysilane applied to anti-fingerprint paint

The invention aims to provide a method for synthesizing novel perfluoropolyether alkoxysilane applied to anti-fingerprint paint through reaction of perfluoroalkyl ether acyl fluoride, allyl amine and trimethoxy silane. The method is characterized by comprising the following steps: (1) adding perfluoroalkyl ether acyl fluoride and allyl amine into a reaction vessel at the molar ratio of 1 to (1-1.1), adding a certain amount of solvent and alkali into the reaction vessel, and performing stirring overnight at a room temperature; performing filtration, performing distillation under reduced pressure to remove the solvent, and performing silica gel column separation, wherein an eluting agent is composed of heptane and ethyl acetate at the ratio of 6 to 1, and a product is obtained after the solvent is removed; (2) a certain amount of product obtained in the step (1) and a catalyst are added into a reaction kettle, sealing the reaction kettle, performing nitrogen protection, placing the reaction kettle in oil bath, heating the reaction kettle to specified temperature, and performing stirring for reaction for 48 hours; quickly cooling the reaction kettle to room temperature after the reaction is finished; performing distillation under reduced pressure on the product of the reaction to remove solvent, and then performing separation and purification through silica gel columns to obtain the product (namely the novel perfluoropolyether alkoxysilane). The product prepared by the invention is applied to anti-fingerprint paint, has the characteristics of fingerprint reduction, easiness in cleaning, wear resistance and the like, and is suitable for lots of base materials, such as glass, plastic, metal and films.
Owner:JIANGNAN UNIV
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