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475results about How to "Improve reaction efficiency" patented technology

Device for synthesizing rare earth mixed precipitant through ammonia carbon reinforcement

The utility model belongs to the technical field of rare earth hydrometallurgy and comprehensive utilization of resources, and particularly relates to a device for synthesizing a rare earth mixed precipitant in an ammonia-carbon reinforced manner. The utility model discloses a device for intensively synthesizing a rare earth mixed precipitator by ammonia carbon, which comprises an ammonia carbon intensified synthesis reactor, the ammonia carbon intensified synthesis reactor consists of five groups of plate bundles formed by welding herringbone corrugated plate sheets, and the five groups of plate bundles comprise two groups of gasification plate bundles for gasifying liquid carbon dioxide; the three groups of reaction plate bundles are used for mixing ammonia water and water and reacting with the bulk carbon dioxide, the five groups of plate bundles are wrapped by a metal shell, and an ammonia water, water and liquid carbon dioxide inlet and a circulating cooling water inlet and outlet are reserved outside the shell. Compared with a traditional tower reactor, the tower reactor has the remarkable advantages of being high in equipment integration degree, high in reaction efficiency, low in energy consumption and the like, the energy consumption is saved by 50%, the total investment of equipment is reduced by 50%, the occupied space of the equipment is reduced by 90%, and remarkable innovation is achieved.
Owner:BAOTOU RESEARCH INSTITUTE OF RARE EARTHS +1

Catechol side group-containing polylysine derivative as well as preparation method and application thereof

The invention discloses a catechol side group-containing polylysine derivative as well as a preparation method and application thereof. The preparation method comprises the following steps: (1) dissolving catechol acid in an organic phase, firstly adding NHS, stirring and dissolving until the materials are uniformly mixed, then adding EDC.HCl, and stirring and reacting to obtain a catechol-NHS intermediate solution; (2) dissolving polylysine or a salt thereof in a water phase, and adjusting the pH value to 6.0-7.0 by using an alkaline solution to obtain a solution of polylysine or a salt thereof; and (3) adding the intermediate solution obtained in the step (1) into the polylysine or the salt solution thereof obtained in the step (2), and maintaining the pH value of the reaction system at 5.0-6.0 by using an alkaline solution to obtain the catechol side group-containing polylysine derivative. The preparation method is short in reaction time and mild in reaction condition, and the obtained product is high in grafting rate and high in raw material conversion rate and has a good application prospect in the aspects of tissue adhesives and the like.
Owner:IMEIK TECH DEV CO LTD

Anion exchange membrane electrode and preparation method and application thereof

PendingCN121951615AImprove drainage effectreduce retentionCellsOrganic diaphragmsIonomerPtru catalyst
The invention discloses an anion exchange membrane electrode and a preparation method and application thereof, and belongs to the technical field of new energy material and catalytic electrode preparation, the method comprises the following steps: S1, preparing an anode catalyst slurry comprising a hydrophobic covalent organic framework material, an anode catalyst, an anion exchange ionomer and a solvent; s2, preparing a cathode catalyst slurry of which the components comprise a cathode catalyst, an anion exchange ionomer and a solvent; and S3, respectively spraying or coating the anode catalyst slurry and the cathode catalyst slurry on two side surfaces of an anion exchange membrane or a gas diffusion layer, and carrying out heat treatment to obtain the anion exchange membrane electrode. The method provided by the invention can solve the problems of large gas-liquid-ion three-phase mass transfer resistance, easy shielding of active catalytic sites by ionomers and unbalanced water management in the membrane electrode assembly in the existing AEMWE device.
Owner:ZHEJIANG UNIV +1

Hydrogenation method of waste tire pyrolysis oil

This invention relates to the field of petroleum refining and chemical engineering, and discloses a method for hydrogenating waste tire pyrolysis oil. The method includes the following steps: (1) in the presence of hydrogen, the waste tire pyrolysis oil raw material undergoes a gas-phase desulfurization reaction in a first gas-phase hydrogenation reactor to obtain a gas-phase desulfurization reaction product; (2) the gas-phase desulfurization reaction product is subjected to gas-liquid separation to obtain a gas-phase component and a liquid-phase component; (3) the liquid-phase component is pressurized and mixed with hydrogen, and then subjected to a liquid-phase dearomatics reaction in a second hydrogenation reactor to obtain a liquid-phase dearomatics reaction product; the nitrogen content in the waste tire pyrolysis oil raw material is 3000-10000 μg / g. This method uses waste tire pyrolysis oil from the middle distillate as raw material, achieving deep desulfurization while reducing the removal of nitrogen oxides and monocyclic aromatic hydrocarbon saturation. It also simplifies the overall process flow, reduces the reaction severity, and lowers energy and hydrogen consumption.
Owner:CHINA PETROLEUM & CHEMICAL CORP +1

Micro-channel reactor and micro-channel reaction equipment

The invention discloses a micro-channel reactor and micro-channel reaction equipment, the micro-channel reactor comprises a reaction plate, a support transition plate and a heat exchange plate which are connected in a laminated manner, grooves are processed in the reaction plate to form micro-reaction channels, grooves are processed in the heat exchange plate to form heat exchange channels, and the support transition plate is separated between the reaction plate and the heat exchange plate; the micro-reaction channel comprises at least two micro-channel units and a middle flow channel connected with the adjacent micro-channel units, each micro-channel unit comprises a flow channel inlet, a flow channel outlet and a heart-shaped mixing cavity, an arc-shaped flow baffle and at least one turbulent flow column are arranged in the heart-shaped mixing cavity, the concave side of the arc-shaped flow baffle faces the flow channel inlet, and the convex side of the arc-shaped flow baffle faces the turbulent flow column. And the turbulent flow column is arranged between the arc-shaped flow baffle and the flow channel outlet. Through cooperation of the heart-shaped mixing cavity, the arc-shaped flow baffles and the turbulent flow columns, the particle suspension rate and the mass transfer capacity of the micro-reaction channel are effectively improved, then the reaction efficiency is improved, and the device can be used for achieving continuous preparation of nano-drugs.
Owner:GUANGDONG PHARMA UNIV

Light-enzyme-heat synergistic antibacterial nano composite material and preparation method thereof

The invention relates to the technical field of antibacterial materials, and provides a light-enzyme-heat synergistic antibacterial nano composite material and a preparation method thereof.The preparation method comprises the steps that 1, a copper-based chalcogenide with a plasma resonance effect serves as a structural template, a transition metal oxide intermediate layer and a bismuth oxyhalide epitaxial layer are sequentially constructed on the surface of the copper-based chalcogenide with the plasma resonance effect through a step-by-step continuous solvothermal method, and the copper-based chalcogenide with the plasma resonance effect serves as the structural template; forming a core-shell heterojunction with Z-type energy band matching; (2) pre-assembling a natural enzyme and a monatomic nano-enzyme in a buffer system to form a composite catalytic unit with an electron transfer channel; and (3) by taking the core-shell heterojunction as a polymerization core, under the precise temperature control condition of 0-10 DEG C, initiating active free radical polymerization through an interface, constructing a thermal response polymer shell layer on the surface of the heterojunction, and encapsulating the composite catalytic unit in a functional microdomain of a polymer network in situ. The anti-bacterial fabric can achieve a better synergistic anti-bacterial effect.
Owner:BOZHOU UNIV

Double-jet powder feeding device

The invention discloses a double-jet powder feeding device, which belongs to the technical field of water treatment, and comprises a gas-liquid separation buffer tank for performing gas-liquid separation on mixed slurry, and an exhaust port is formed in the gas-liquid separation buffer tank; the first jet mixing mechanism is used for preliminarily mixing powder and the first water flow; the water supply mechanism is used for mixing water; one end of the second mixing piece is connected with a water outlet of the gas-liquid separation buffer tank; the first jet mixing mechanism comprises a first mixing piece connected with the gas-liquid separation buffer tank at one end and a feeding assembly used for feeding powder to the first mixing piece, and the other end of the first mixing piece and the other end of the second mixing piece are both connected with a water outlet of the water supply mechanism; and the second mixing piece can be used for secondarily mixing the buffered and separated liquid-solid mixed liquid and the second water flow and pressurizing and throwing out the liquid-solid mixed liquid and the second water flow. The device has the effects of effectively solving gas interference, preventing blockage and reflux, and realizing stable, efficient and continuous feeding.
Owner:广东金宗机械有限公司

A boiler flue gas denitration reaction spraying device

ActiveCN224736063UExtended service lifeEasy to shake off
This utility model relates to a boiler flue gas denitrification reaction spray device, belonging to the technical field of spray device technology. It includes a base and a dust removal tower fixedly connected to the top of the base. The spray tower is fixedly connected to the top of the base, and the dust removal tower contains a dust removal mechanism for removing dust from the flue gas. The dust removal mechanism includes a support plate slidably connected inside the dust removal tower. This boiler flue gas denitrification reaction spray device, by setting up dust removal filter bags and a support plate, and by setting up an air inlet pipe, can filter the dust in the flue gas, ensuring that the flue gas entering the spray tower does not contain a large amount of dust, thus improving the reaction efficiency between reactants and catalysts. Furthermore, by setting up a dual-shaft motor to drive an eccentric wheel to rotate, and by setting up a return spring, the support plate and the dust removal filter bags can vibrate up and down, facilitating the shaking off of dust from the surface of the dust removal filter bags, achieving a dust removal effect and extending the service life of the dust removal filter bags.
Owner:ZIBO BAOXIANG GLASS CO LTD

A method of oligonucleotide inkjet printing

The application provides a method for inkjet printing of oligonucleotides, and belongs to the technical field of in-situ synthesis of oligonucleotides.The method comprises the following steps: modifying the surface of a solid carrier with a chemically active functional group; depositing oligonucleotide synthesis reagents onto the surface of the modified solid carrier by inkjet to perform in-situ synthesis; and the solvent in the oligonucleotide synthesis reagents comprises one or two of glutaronitrile, acetonitrile and propylene carbonate.The application uses a new type of difficult-to-vaporize solvent, greatly reduces the volatilization of reagents during inkjet synthesis and the generation of organic vapors during synthesis, and thus maintains a high in-situ synthesis reaction efficiency of oligonucleotides.
Owner:BEIJING MINGYI INTELLIGENT MFG TECH CO LTD

Method for preparing nitro-mesitylene through micro-channel nitration reaction

The invention discloses a method for preparing nitro-mesitylene through a micro-channel nitration reaction. The method comprises the following steps: respectively conveying mesitylene, fuming nitric acid and sulfuric acid to a micro-channel reaction module through a metering pump, and completing nitration reaction within a retention time of tens of seconds to several minutes. The introduction sequence of nitration reaction materials, the reaction retention time and the reaction temperature are cooperatively controlled, the nitration reaction is completed in the microchannel reactor in a continuous flow mode, operation is easy and convenient, safety is high, efficient continuous production can be achieved, meanwhile, emission of three wastes is reduced, and the industrial application advantages of being environmentally friendly and economical are achieved.
Owner:NANJING UNIV OF SCI & TECH

A cell fluorescence probe anchoring integrin and a preparation method and application thereof

ActiveCN117431056BExtend fluorescence timelinessIncrease binding rateChemical compoundCyclodextrin
The application belongs to the field of biomedical application, and more particularly relates to a cell fluorescence probe anchoring cell integrin, and a preparation method and application thereof. The cell fluorescence probe comprises a polypeptide complex, a fluorescent molecule and a cyclodextrin unit, the polypeptide complex comprises a cysteine-containing peptide, a peptide containing a bonding group and a targeting peptide which are connected in any order, the cyclodextrin unit contains a carbon-carbon double bond functional group, and is combined with the cysteine-containing peptide through a click reaction to form the polypeptide complex, the polypeptide complex is covalently connected to the fluorescent molecule through the bonding group, and the fluorescent molecule is an aggregation-induced emission compound. The double bond functional group of the modified cyclodextrin is bonded to the sulfhydryl group of the terminal cysteine of the polypeptide through a click reaction, and the sulfhydryl group of the terminal cysteine of the polypeptide is bonded to the double bond functional group of the modified cyclodextrin through a click reaction, so that the cyclodextrin is improved to protect the fluorescent molecule and prolong the fluorescent time effectiveness of the fluorescent imaging reagent.
Owner:SHENZHEN SECOND PEOPLES HOSPITAL (SHENZHEN INST OF TRANSLATIONAL MEDICINE)

Amino-graphene preparation system and method for automatically improving separation efficiency thereof

The application discloses a method for automatically improving separation efficiency of an amino graphene preparation system, and relates to the technical field of graphene preparation.The preparation system comprises a graphene preparation detection module, a primary reaction detection module, a middle reaction detection module and a reminding adjustment display module; the graphene preparation detection module, the primary reaction detection module and the middle reaction detection module are used for detecting and controlling reaction temperature, time, reactant quality and other parameters in the process of preparing amino graphene, so as to obtain a first coefficient DYxs1, a second coefficient DYxs2 and a third coefficient DYxs3; the first coefficient DYxs1, the second coefficient DYxs2 and the third coefficient DYxs3 are compared and analyzed with threshold values after being corrected by the reminding adjustment template, an adjustment scheme is obtained, a control command is generated according to the adjustment scheme, accurate control and optimization are performed, and then efficient preparation and separation of amino graphene are realized, and the preparation and separation effect of the amino graphene is improved.
Owner:SHENZHEN A OLEFIN TECH CO LTD

A method for preparing oxyhalide electrolyte using retired batteries to recover lithium carbonate

PendingCN122725358Alow costRealize functional utilization
The application discloses a method for preparing halide oxide electrolyte by recycling lithium carbonate from retired batteries, and relates to the technical field of all-solid-state battery electrolyte materials, which directly synthesizes halide oxide solid electrolyte by mechanical chemical reaction of low-purity recycled lithium carbonate containing impurities and metal halide; the impurities in the low-purity lithium carbonate include at least one of Al, Fe, Ni, Co, Mn, F, P, Na and K. The application replaces traditional raw materials such as high-purity lithium oxide with low-cost crude recycled lithium carbonate, does not need deep purification, and significantly reduces the preparation cost; meanwhile, the application creatively converts the inherent impurity elements such as Al and F in the recycled lithium carbonate into functional components, so that a stable interface passivation layer containing Al2O3 and LiF is formed in situ at the positive electrode interface in the battery cycle process, the interface side reaction is effectively inhibited, and the electrochemical stability is improved. The method has the advantages of simple process, high reaction efficiency and easy scale production, and the prepared electrolyte has high ionic conductivity and excellent cycle stability.
Owner:NINGBO ORIENTAL UNIVERSITY OF TECHNOLOGY

A device and process for the continuous synthesis of nitrobenzene

PendingCN122298306AAchieve serializationAutomate operationBenzeneNitrate
This invention discloses a continuous synthesis apparatus and process for nitrobenzene. The synthesis apparatus includes a mixed acid preparation system, a continuous benzene nitration system, an organic phase continuous stratification system, and a continuous water washing-alkali washing-water washing system. The process includes: concentrated sulfuric acid and concentrated nitric acid are pumped into the mixing module of the mixed acid preparation system to obtain a mixed acid solution; benzene and the mixed acid solution are pumped into the microchannel reactor of the continuous benzene nitration system; the nitrated material is cooled and then pumped into the continuous organic phase stratification system; the resulting intermediate organic phase nitrate enters the next processing unit; the organic phase nitrate and water enter the continuous water washing-alkali washing-water washing system for washing to obtain the final product, nitrobenzene. The synthesis apparatus and process of this invention achieve continuous production of nitrobenzene throughout the entire process, realizing continuous and automated operation from raw material benzene to the final product, nitrobenzene.
Owner:CHINA PETROLEUM & CHEMICAL CORP +2

Venturi adjustable mechanism for dry desulfurization tower of refractory kiln

ActiveCN224731111UAdjust flow rateImprove reaction efficiency
The utility model relates to dry desulfurization tower technical field, and disclose refractory kiln dry desulfurization tower venturi adjustable mechanism, including venturi, the inner wall fixed assembly of venturi has fixed frame, the inner wall sliding connection of fixed frame has baffle no.
Owner:ZHENGZHOU QINHE ENG TECH CO LTD

Method for deeply recovering phosphorus and vanadium from molten iron containing phosphorus and vanadium

The invention discloses a method for deeply recovering phosphorus and vanadium from molten iron containing phosphorus and vanadium, which comprises the following steps: treating the molten iron containing phosphorus and vanadium by adopting an oxygen blowing method, in the oxygen blowing method, directly blowing mixed gas into the molten iron by utilizing a spray gun, the volume concentration of the oxidizing gas is 18%-50%. The method has the advantages of improving the recovery rate of phosphorus and vanadium, reducing the smoke amount and the like, and also has the characteristics of low cost, short process, environmental friendliness, less carbon emission, high heat utilization rate, full utilization of resources and the like.
Owner:CHINA ENFI ENG CORP +1

Method for synthesizing tonalid intermediate HMT

The invention discloses a method for synthesizing a tonalid intermediate HMT, and belongs to the technical field of organic synthesis. According to the method, a specific liquid catalyst and an organic solvent are selected to prepare a catalyst phase, raw materials required for synthesis of tonalid are mixed according to a reasonable ratio to form a raw material phase, then the two phases are introduced into a microchannel reactor for a catalytic reaction, and after the reaction is completed, a target product is obtained through post-treatment steps such as quenching, water washing and rectification. Aiming at the defects that a solid catalyst in the prior art is difficult to realize homogeneous reaction and the reaction process is violent and difficult to control, by optimizing catalyst type selection and reaction process design, a reaction system has good homogeneous property, the reaction process is milder and is easy to accurately regulate and control, the stability and reliability of product preparation are effectively improved, and the method is suitable for industrial production. The method is suitable for industrial large-scale production.
Owner:NANPING QINGHUA TECH CO LTD

Use of divinyltetrazine in linear polypeptide cyclization

PendingCN122145546AAchieving bisulfhydryl staple cyclizationImprove stabilityPeptide/protein ingredientsPeptide preparation methodsAnnulationOctene
The application discloses application of a divinyl tetrazine in cyclization of a linear polypeptide, and a structure formula of the divinyl tetrazine is; the linear polypeptide has at least two free mercapto groups, and the vinyl groups of the divinyl tetrazine are subjected to Michael addition reaction with corresponding mercapto groups to form a ring. The application provides a new use of the divinyl tetrazine, the divinyl tetrazine can be subjected to high-efficiency Michael addition reaction with two natural cysteine mercapto groups on the linear polypeptide through the vinyl groups, so that double-mercapto peg cyclization of the linear polypeptide is realized, and the purpose of limiting the conformation of the linear polypeptide and improving the stability of the linear polypeptide is achieved. Moreover, the divinyl tetrazine can be subjected to a reverse electron demand Diels-Alder reaction with trans-cyclooctene (TCO) after the two vinyl groups are subjected to reaction with mercapto groups, so that functional polypeptides can be modularly constructed by coupling with functional molecules modified with TCO, and related applications are realized.
Owner:LIANGZHU LAB

A reaction kettle

ActiveCN117680072BPromote movement in close proximity to each otherincrease collision
The application discloses a reaction kettle, which comprises a kettle body, a plurality of partitions are fixedly and assembledly connected in the kettle body, through the partitions, a kettle cavity in the kettle body forms a plurality of reaction cavities; the reaction kettle further comprises a layered stirring mechanism, the layered stirring mechanism comprises a stirring shaft, a pushing spiral plate assembly is fixedly and assembledly connected on the stirring shaft, the pushing spiral plate assembly comprises a plurality of lower pushing liquid spiral plates and upper pushing liquid spiral plates; the layered stirring mechanism further comprises stirring assemblies which are respectively located between the lower pushing liquid spiral plates and the upper pushing liquid spiral plates; in the stirring process, the lower pushing liquid spiral plates push reaction materials upwards, the upper pushing liquid spiral plates push reaction materials upwards, the pushing mode of the reaction materials by the lower pushing liquid spiral plates and the upper pushing liquid spiral plates increases the dissolving, crushing and mixing effects of the stirring assemblies on the materials, and the material reaction process is effectively and greatly increased.
Owner:ANQING SHUGUANG PETROCHEMICAL OXO CO LTD

A jet loop reactor

ActiveCN224672718USolve piling technical issuescontact stabilityPhase mixingLiquid circulation
The embodiment of the application provides a kind of jet loop reactor, it is related to the technical field of chemical equipment, including the reactor body and the loop reactor of jet device.The reactor body is equipped with reaction liquid feed inlet, gas discharge port and reaction liquid discharge port.Jet device is longitudinally arranged along the reaction liquid feed inlet and is interconnected with each other mixing channel, contraction channel and expansion channel, mixing channel is equipped with liquid circulating feed inlet and reaction liquid nozzle, and separated liquid enters mixing channel and mixes with reaction liquid by circulating feed inlet, contraction channel gradually shrinks along the material flow direction, and expansion channel gradually expands along the flow direction, by the synergistic effect of mixing channel, contraction channel and expansion channel in jet device, combined with the double circulation flow channel formed by flow guide piece, the gas-liquid-solid three-phase mixing effect is strengthened, effectively prevent solid deposition and bubble coalescence, with the advantages of uniform mixing, high reaction efficiency and stable operation.
Owner:STATE NUCLEAR ELECTRIC POWER PLANNING DESIGN & RES INST CO LTD

Naphthalene water reducer neutralization reaction device capable of automatically adding alkali

ActiveCN224071976URealize electric lifting functionImprove lifting stabilityChemical/physical/physico-chemical stationary reactorsFeed devicesPhysical chemistryNaphthalene
The utility model discloses a naphthalene water reducer neutralization reaction device capable of automatically adding alkali, and belongs to the technical field of water reducer production equipment. The naphthalene water reducer neutralization reaction device with the automatic alkali adding function comprises a reaction tank, a tank cover is installed at the top end of the reaction tank, four supporting columns are installed on the outer side of the bottom end of the reaction tank, a cooling mechanism is installed on the outer side of the reaction tank, an alkali liquor tank is arranged on one side of the reaction tank, a ring pipe is installed on the inner side of the reaction tank, and a plurality of alkali liquor spray heads are installed at the bottom end of the ring pipe. The top end of the alkali liquor tank is provided with a liquor feeding mechanism for supplying liquor to the annular pipe, the top end of the annular pipe is provided with a cleaning mechanism for cleaning the alkali liquor spray head, the reaction tank is internally provided with a mixing mechanism, the bottom end of the reaction tank is provided with a liquor outlet pipe, and one end of the liquor outlet pipe is provided with a valve. The neutralization reaction efficiency is improved, and the practical value is relatively high.
Owner:LAIWU ZHAOXIN NEW MATERIAL CO LTD

Powder injection type drying decanter centrifuge

ActiveCN224641298UIncrease solid contentloose texture
The utility model relates to a horizontal screw centrifuge technical field discloses a kind of powder spraying type drying horizontal screw centrifuges, to solve the defect of overcoming the high moisture content of solid phase material of existing horizontal screw centrifuge easy to stick. The utility model is under the centrifugal field by superstrong instantaneous mixing and penetration: in the centrifugal field of up to hundreds even thousands of times gravity acceleration, dry powder particles spouted from powder spout can be "pressed into" the filter cake being extruded by screw conveyor dehydration with very high relative speed, this forced mixing under high G force, far more than ordinary mixer can compare, it can make dry powder instantaneously, uniformly penetrate into the micro-pore structure of filter cake, realize molecular level contact, greatly improve the reaction efficiency and hygroscopic efficiency of drying agent (such as quicklime, fly ash etc.), make the filter cake discharged solid rate significantly improve, and texture loose, uniform.
Owner:NANJING MONYA CENTRIFUGE TECH DEV CO LTD

Method for synthesizing mg-o-based catalyst and use thereof

PendingCN122682592AAvoid component inhomogeneity caused by mismatchAvoid the problem of uneven components
The application discloses a MgO-based catalyst synthesis method and application thereof, relates to the technical field of catalyst preparation, and comprises the following steps: dissolving magnesium salt, lanthanum salt, cerium salt, calcium salt and nickel salt in deionized water, stirring uniformly to obtain a metal salt solution; adding citric acid into the metal salt solution and stirring intensively until uniform to form a mixed gel; pouring the mixed gel on a medium-speed qualitative filter paper, transferring and drying to obtain a dry gel; roasting the dry gel with the filter paper, grinding the roasted dry gel with a mortar to obtain a grinding powder; and transferring the grinding powder to a muffle furnace for calcination to obtain a uniform composite metal oxide catalyst; the MgO-based catalyst is prepared by combining the dry gel method with the combustion decomposition method, the preparation process is simple, the conditions are easy to control, the preparation process is easy to repeat, the product pollution risk caused by the introduction of sodium hydroxide precipitator is eliminated, the preparation cost and process difficulty are reduced, and the method is suitable for large-scale production. + ​
Owner:새틀라이트뉴머티리얼즈알앤디컴퍼니리미티드

Catalyst for preparing anisole through phenol methanol etherification as well as preparation method and application of catalyst

The invention relates to a catalyst for preparing anisole through phenol methanol etherification as well as a preparation method and application of the catalyst. The catalyst takes aluminum phosphate as a carrier and is doped with zirconium oxide; on the basis of the mole number of Al, the mole ratio of P to Al is (0.05-2): 1, and the mole ratio of Zr to Al is (0.08-0.20): 1. Dropwise adding the aluminum-zirconium mixed aqueous solution into the phosphorus source aqueous solution, stirring, standing and washing to obtain a solid sample; and drying and roasting the solid sample to obtain the aluminum phosphate catalyst. Under the action of the catalyst, phenol and methanol are catalyzed to generate anisole. Compared with the prior art, the phenol conversion rate is greater than or equal to 50%, the anisole selectivity is greater than or equal to 85%, highly toxic dimethyl sulfate and a large amount of alkali are not needed, the process is green, the cost is low, separation is simple, and the method is suitable for large-scale industrial production of anisole.
Owner:SHANGHAI INST OF TECH

An environmental protection equipment for roasting waste desulfurizer

ActiveCN224650270UOptimizing the Reaction TemperatureAccurate heat supplement
The utility model discloses a kind of for waste desulfurizer's calcination environmental protection processing equipment, including boiling roasting furnace, boiling roasting furnace inside is provided with combustion cavity, combustion cavity is wide on top and narrow on bottom, multiple temperature measuring devices are fixedly installed in combustion cavity inner wall;Boiling roasting furnace is annular fixed and is communicated with multiple combustion-supporting pipes and multiple gas burners, gas burner and combustion-supporting pipe are all inclined to set, multiple gas burners and multiple combustion-supporting pipes are one-to-one correspondence, combustion-supporting pipe is close to the low side of combustion cavity center, and one end of gas burner in combustion cavity is close to combustion-supporting pipe.The utility model in the present application, the cooperation of gas burner, combustion-supporting pipe and component, can accurately heat the middle or top position in boiling roasting furnace, avoid that temperature gradient is too large, ensure that all waste desulfurizer is at optimum reaction temperature, reduce the incomplete reaction caused by insufficient temperature, improve reaction efficiency.
Owner:JIANGSU FUYOU CHEM CATALYTIC PURIFICATION ENVIRONMENTAL PROTECTION MATERIAL CO LTD

A device for recycling waste heat of phosphorus trichloride reaction

ActiveCN224599330UAchieving stirringEnhanced mixing process
The application relates to the technical field of waste heat recovery, and discloses a phosphorus trichloride reaction waste heat recycling device, which comprises a base, a reaction kettle and an energy storage box are fixedly installed at the top of the base, the reaction kettle is located at the left side of the energy storage box, a function box is fixedly installed at the top of the reaction kettle, the same piston cylinder is fixedly installed at the top of the energy storage box and the right side of the function box, a motor is fixedly installed on the top inner wall of the function box, a stirring mechanism is arranged in the reaction kettle, a feeding pipe is arranged at the left side of the reaction kettle, a jacket is arranged outside the reaction kettle, and an oil feeding pipe is arranged at the left side of the jacket. The application has the following advantages and effects: the piston mechanism is arranged, when the piston plate slides to the right, gas is pressed into water in the energy storage box through the breather pipe, the water is uniformly heated by the water disturbance in the process of the bubble rising and breaking in the water, and the purpose of avoiding the situation that the local water temperature is too high or too low can be achieved.
Owner:JINGZHOU LUYUAN CHEMICAL TECHNOLOGY CO LTD

Polypropylene composite filler based on electrocatalytic oxidation coal gasification fine slag as raw material and preparation method thereof

The invention discloses a preparation method of a polypropylene composite filler based on electrocatalytic oxidation coal gasification fine slag as a raw material, the preparation method comprises the steps of raw material treatment, system modification, material electrolytic oxidation and material post-treatment, the polypropylene composite filler comprises polypropylene resin and the polypropylene composite filler, based on the total weight of the composite material, the usage amount of the composite filler is 5-20wt%, and the usage amount of the composite filler is 5-20wt%. The raw materials comprise an environment-friendly functional auxiliary agent accounting for 0.5-5% of the total weight of the composite material, and the functional auxiliary agent is selected from one of a weather-proof agent, a halogen-free flame retardant and a bio-based antibacterial agent. The method has the advantages that the low-temperature plasma pretreatment and the composite modifier assisted electrocatalytic oxidation process are combined, a large number of active sites can be quickly and efficiently introduced on the surface of the coal gasification fine slag through the low-temperature plasma treatment, and the surface energy and the reaction activity of the coal gasification fine slag are remarkably enhanced.
Owner:LINHUAN COKING +1

Biomass pyrolysis gas catalytic device

The utility model discloses a biomass pyrolysis gas catalytic device, and particularly relates to the technical field of biomass pyrolysis, the biomass pyrolysis gas catalytic device comprises a reaction furnace and a heating device, the top of the reaction furnace is provided with a feed port and a gas inlet, and the bottom of the reaction furnace is provided with a discharge port and a gas outlet; a plurality of layers of sealing drawing plates which can slide along the reaction furnace and can be drawn out are arranged on one side surface of the reaction furnace, the sealing drawing plates are used for placing ore catalysts, and the heating device is connected with the reaction furnace and is used for heating the reaction furnace. The deactivated catalyst can be conveniently and quickly replaced, the reaction stability is improved, and the reaction efficiency is improved.
Owner:INSTITUTE OF ENVIRONMENT AND SUSTAINABLE DEVELOPMENT IN AGRICULTURE CAAS

A continuous reaction and separation integrated device for oil and gas field chemical additive production

The utility model discloses a kind of continuous reaction and separation integrated equipment of oil and gas field chemical additive production, it is related to chemical additive production technical field, including stirred tank reactor, the intermediate outer wall of stirred tank reactor is fixed with fixed ring, the upper end of fixed ring is equidistantly provided with four groups of lifting tracks, one group of movable ring is arranged between the side wall of four groups lifting tracks, the side wall equidistantly of movable ring is provided with four groups of sliding block, four groups sliding block are respectively with the inner wall of one group lifting track and inlaying sliding connection, the inner wall of movable ring is provided with electromagnet, the inner diameter of movable ring is greater than the outer diameter of stirred tank reactor, movable ring is nested in the outside of stirred tank reactor.The utility model of a kind of continuous reaction and separation integrated equipment of oil and gas field chemical additive production can be adsorbed separation to the magnetic substance inside reactor by external electromagnet, let the efficiency of separation be higher.
Owner:GANSU SAIMAIKE ENERGY TECH CO LTD