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560 results about "INTRODUCTION device" patented technology

Sample introduction device and method

InactiveUS20140331744A1Reduced discriminationHeating rates and programmes can be varied widelySamplingComponent separationGas analysisGas phase
The present invention relates to an injector for use in gas phase analytical systems and methods comprising a metal housing, provided with a carrier gas inlet, a split outlet, a column outlet of the injector, a sample inlet, a liner, and a heater device comprising at least one coil for radio frequency inductive heating the housing with a predetermined temperature program and for providing a predetermined spatial temperature profile in the injector. The injector according to the invention allows performing gas phase analyses, especially GC analyses with reduced discrimination. Advantages of heating with a heater device comprising a coil for inductive heating include a homogeneous heating profile of the housing including parts connected thereto, with heating rates that can be varied widely. A further advantage is that the injector can be operated as a conventional S / SL injector at a predetermined temperature, or as PTV injector or thermal desorption injector with certain predetermined temperature programs. The invention also relates to a process of making an injector according to the invention, and to a process of refitting an existing S / SL injector. The invention further concerns a gas analytical system comprising an injector according to the invention, and to a process of analysing a sample with such gas analytical system.
Owner:DSM IP ASSETS BV

Instrument system suitable for synchronous on-line detection of adsorption spectrum and fluorescence spectrum

The invention discloses a system for synchronous on-line detection of adsorption spectrum and fluorescence spectrum. The system consists of a reciprocating plunger pump, a sample introduction device, an enrichment device, a detection cell, a light source, a spectrograph, an optical fiber, a computer and a data processing system, wherein the sample introduction device is provided with a six-way valve; a sample passes through the reciprocating plunger pump according to a predetermined time, enters an active carbon enrichment column through the six-way valve and is discharged after online enrichment; after finishing enrichment, the six-way valve is switched; an eluate enters the active carbon enrichment column through the six-way valve; an enrichment substance is washed and enters a flow cell and is discharged after spectrum detection is performed on the enrichment substance; the content of the sample is calculated based on the change of spectrum intensity; and the flow cell is integrally connected with five-way valve formed by a light source radiation optical fiber interface hole, an ultraviolet visible light optical fiber interface hole, a fluorescence spectrum optical fiber interface hole, a liquid inlet pipe hole and a liquid outlet pipe hole. The system realizes the on-line detection of the adsorption spectrum and the fluorescence spectrum; and an instrument has the characteristics of small volume, light weight, good reproducibility, convenient carrying, and fast sample treating speed, so the system has wide application fields.
Owner:XINJIANG MEDICAL UNIV
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