The invention relates to a method for preparing a polyacrylate / amino modified oxidized
graphene compound leather finishing agent by adopting an ultrasonic-assisted method. The method for preparing the polyacrylate / amino modified oxidized
graphene compound leather finishing agent by adopting the ultrasonic-assisted method comprises the following steps: carrying out
ultrasonic dispersion on oxidized
graphene,
sulfur dichloride and
dimethylformamide; adding
dimethylformamide, carrying out spiral evaporating, adding
triethylamine and
ammonia water, carrying out ice bath reaction and suction
filtration, and washing; adding
sodium hydroxide and
bromine, carrying out ice bath reaction, then adding products obtained through suction
filtration, stirring, carrying out suction
filtration, and washing to obtain amino modified oxidized graphene; mixing
sodium dodecyl sulphate,
polyvinyl alcohol 400 and deionized water, dropwise adding part of
methyl methacrylate,
butyl acrylate,
acrylic acid, hydroxyethyl
acrylate and an initiating agent, warming, and then dropwise adding the rest part, so that polyacrylate
emulsion is obtained; and regulating pH of the polyacrylate
emulsion, then adding the amino modified oxidized graphene, and carrying out
ultrasonic dispersion, so that the product polyacrylate / amino modified oxidized graphene compound leather finishing agent is obtained. The method for preparing the polyacrylate / amino modified oxidized graphene compound leather finishing agent by adopting the ultrasonic-assisted method has the advantages that defects of polyacrylate are overcome by utilizing physical and mechanical advantages of graphene and application performance of the polyacrylate / amino modified oxidized graphene compound leather finishing agent is effectively enhanced.