Graphene functional cotton fabric and preparation method thereof
A technology of olefin cotton fabric and graphene, applied in the fields of smart wear and functional textiles, can solve the problems of poor durability, complicated operation, poor water resistance, etc., and achieve the effects of easy large-scale production, simple preparation process, and excellent electrical conductivity.
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Embodiment 1
[0023] The preparation method of a graphene functional cotton fabric of this embodiment is that the graphene oxide is first modified by amino or sulfhydryl, and then compounded with multi-reactive group reactive dyes to obtain graphene oxide reactive dyes. The fabric is dip dyed in the obtained graphene oxide reactive dye to obtain graphene oxide cotton fabric, and finally reduced by a reducing agent to obtain graphene functional cotton fabric, including the following process steps:
[0024] Step 1: Graphene oxide modification
[0025] Dissolve 1 part by mass of graphene oxide in 1 part by mass of 1% stearylamine alcohol solution, ultrasonically treat it at 20°C for 10 hours, take it out and separate by suction, clean it with pure water, and dry it at 20°C for 2 hours. Obtain modified graphene oxide;
[0026] Step 2: Composite of modified graphene oxide and reactive dyes
[0027] Dissolve 1 part by mass of Reactive Brilliant Blue KD-B in 10 parts by mass of pure water, add 1 part by ...
Embodiment 2
[0033] The preparation method of a graphene functional cotton fabric of this embodiment is that the graphene oxide is first modified by amino or sulfhydryl, and then compounded with multi-reactive group reactive dyes to obtain graphene oxide reactive dyes. The fabric is dip dyed in the obtained graphene oxide reactive dye to obtain graphene oxide cotton fabric, and finally reduced by a reducing agent to obtain graphene functional cotton fabric, including the following process steps:
[0034] Step 1: Graphene oxide modification
[0035] Dissolve 1 part by mass of graphene oxide in 1.5 parts by mass of 1% stearylamine alcohol solution, ultrasonically treat it at 50°C for 5h, take it out and separate by suction filtration, clean it with pure water, and dry it at 70°C for 1.5h. Prepare modified graphene oxide;
[0036] Step 2: Composite of modified graphene oxide and reactive dyes
[0037] Dissolve 1 part by mass of Reactive Scarlet KD-B in 15 parts by mass of pure water, add 0.4 parts b...
Embodiment 3
[0043] The preparation method of a graphene functional cotton fabric of this embodiment is that the graphene oxide is first modified by amino or sulfhydryl, and then compounded with multi-reactive group reactive dyes to obtain graphene oxide reactive dyes. The fabric is dip dyed in the obtained graphene oxide reactive dye to obtain graphene oxide cotton fabric, and finally reduced by a reducing agent to obtain graphene functional cotton fabric, including the following process steps:
[0044] Step 1: Graphene oxide modification
[0045] Dissolve 1 part by mass of graphene oxide in 2 parts by mass of 1% stearylamine alcohol solution, ultrasonically treat it at 80°C for 1h, take it out and separate by suction, clean it with pure water, and dry it at 120°C for 1h. Obtain modified graphene oxide;
[0046] Step 2: Composite of modified graphene oxide and reactive dyes
[0047] Dissolve 1 part by mass of reactive medium yellow KD-B in 20 parts by mass of pure water, add 0.25 parts by mass o...
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