Graphene functional cotton fabric and preparation method thereof

A technology of olefin cotton fabric and graphene, applied in the fields of smart wear and functional textiles, can solve the problems of poor durability, complicated operation, poor water resistance, etc., and achieve the effects of easy large-scale production, simple preparation process, and excellent electrical conductivity.

Active Publication Date: 2017-07-04
山东利特纳米技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The application of graphene materials in textiles has attracted more and more attention because of its unique two-dimensional structure and remarkable electrical and mechanical properties. It has become a new way of research on related functional textiles. Excellent electrical and mechanical properties. For example, the Chinese invention patent application with the application number 201510540291.8 discloses a graphene/cotton flexible conductive fabric and its preparation method. The surface of the cotton fabric is covered with graphene oxide by dipping-drying method, and then Graphene oxide is reduced to graphene by in-situ chemical reduction method, thus endowing cotton fabric with good electrical conductivity, but there is a problem of poor durability
The Chinese invention patent application with the application number 201610665999.0 disclose

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] The preparation method of a graphene functional cotton fabric of this embodiment is that the graphene oxide is first modified by amino or sulfhydryl, and then compounded with multi-reactive group reactive dyes to obtain graphene oxide reactive dyes. The fabric is dip dyed in the obtained graphene oxide reactive dye to obtain graphene oxide cotton fabric, and finally reduced by a reducing agent to obtain graphene functional cotton fabric, including the following process steps:

[0024] Step 1: Graphene oxide modification

[0025] Dissolve 1 part by mass of graphene oxide in 1 part by mass of 1% stearylamine alcohol solution, ultrasonically treat it at 20°C for 10 hours, take it out and separate by suction, clean it with pure water, and dry it at 20°C for 2 hours. Obtain modified graphene oxide;

[0026] Step 2: Composite of modified graphene oxide and reactive dyes

[0027] Dissolve 1 part by mass of Reactive Brilliant Blue KD-B in 10 parts by mass of pure water, add 1 part by ...

Embodiment 2

[0033] The preparation method of a graphene functional cotton fabric of this embodiment is that the graphene oxide is first modified by amino or sulfhydryl, and then compounded with multi-reactive group reactive dyes to obtain graphene oxide reactive dyes. The fabric is dip dyed in the obtained graphene oxide reactive dye to obtain graphene oxide cotton fabric, and finally reduced by a reducing agent to obtain graphene functional cotton fabric, including the following process steps:

[0034] Step 1: Graphene oxide modification

[0035] Dissolve 1 part by mass of graphene oxide in 1.5 parts by mass of 1% stearylamine alcohol solution, ultrasonically treat it at 50°C for 5h, take it out and separate by suction filtration, clean it with pure water, and dry it at 70°C for 1.5h. Prepare modified graphene oxide;

[0036] Step 2: Composite of modified graphene oxide and reactive dyes

[0037] Dissolve 1 part by mass of Reactive Scarlet KD-B in 15 parts by mass of pure water, add 0.4 parts b...

Embodiment 3

[0043] The preparation method of a graphene functional cotton fabric of this embodiment is that the graphene oxide is first modified by amino or sulfhydryl, and then compounded with multi-reactive group reactive dyes to obtain graphene oxide reactive dyes. The fabric is dip dyed in the obtained graphene oxide reactive dye to obtain graphene oxide cotton fabric, and finally reduced by a reducing agent to obtain graphene functional cotton fabric, including the following process steps:

[0044] Step 1: Graphene oxide modification

[0045] Dissolve 1 part by mass of graphene oxide in 2 parts by mass of 1% stearylamine alcohol solution, ultrasonically treat it at 80°C for 1h, take it out and separate by suction, clean it with pure water, and dry it at 120°C for 1h. Obtain modified graphene oxide;

[0046] Step 2: Composite of modified graphene oxide and reactive dyes

[0047] Dissolve 1 part by mass of reactive medium yellow KD-B in 20 parts by mass of pure water, add 0.25 parts by mass o...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention provides a graphene functional cotton fabric and a preparation method thereof, which belong to the technical fields of intelligent wearing and functional textile. The graphene functional cotton fabric is characterized in that graphene oxide is subjected to amination or sulfhydrylation modification, then is composited with a multi-active reactive dye to obtain a graphene oxide reactive dye, the cotton fabric is subjected to dip dyeing in the graphene oxide reactive dye under ultrasonic condition to obtain the graphene oxide cotton fabric, and the graphene functional cotton fabric is reduced by a reducing agent. The graphene functional cotton fabric integrates dyeing and conductivity functions, endows the common cotton fabric with excellent electricity function of graphene, and stability, high temperature resistance and friction color fastness are obviously increased.

Description

Technical field [0001] The invention relates to the technical field of smart wear and functional textiles, in particular to a graphene functional cotton fabric and a preparation method thereof. Background technique [0002] With the continuous development of human society, the simple functions of decoration, covering, and warmth of existing clothing will not meet people's needs. Functional textiles have gradually become the mainstream of current textile product research and development, such as smart wear, electromagnetic shielding fabrics, Anti-static clothing, etc. The application of graphene materials in textiles due to their unique two-dimensional structure and remarkable electrical and mechanical properties has attracted more and more attention, and has become a new way of research on related functional textiles, aiming to give textiles graphene materials Excellent electrical and mechanical properties. For example, the Chinese Invention Patent Application No. 201510540291.8...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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IPC IPC(8): D06P1/38D06P1/673D06P3/66
CPCD06P1/38D06P1/673D06P3/66
Inventor 苏启顺宋肖肖苏阳刘同浩
Owner 山东利特纳米技术有限公司
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