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155results about How to "Improve quality score" patented technology

Copper sulfide anode and preparation method thereof

The invention provides a copper sulfide anode and a preparation method thereof, solving the problems of the conventional copper sulfide electrode that the bonding force of active substances and current collectors is poor and the anode conductivity is lowered because of a binder and also solving the problems of the integrated copper sulfide electrode which is synthesized in situ in a solution that the quantity of active substances is small and the preparation period is long. The copper sulfide anode is prepared by the following steps: uniformly spreading elemental sulfur which is prepared according to the sulfur carrying amount of foamy copper is 0.03-0.3g/cm<2> on the foamy copper, putting into a furnace, and carrying out in-situ reaction under a protection gas at a temperature of 155-350 DEG C so as to obtain the laminated copper sulphide which takes a foamy copper three-dimensional network structure as a framework, namely an integrated porous copper sulphide anode. By utilizing the copper sulfide anode, the application of the three-dimensional structured integrated porous anode in a lithium battery is widened, the energy density of a lithium battery anode is improved, and the performances of a lithium battery are improved. The copper sulfide anode is simple in preparation process, low in equipment requirement, low in cost and convenient for industrial production.
Owner:XIANGTAN UNIV

X-ray fluorescence thin layer mass thickness measurement system and method based on reference element

The invention relates to the technical field of X-ray fluorescence analysis, aims at overcoming the defects that the measurement results of an existing X-ray fluorescence measurement system and methodcan be easily influenced by fluctuation of performance of an instrument and the existing X-ray fluorescence measurement system and method are not applicable to measurement on mass thickness of a thinlayer taking metal elements as major components, and provides X-ray fluorescence thin layer mass thickness measurement system and method based on a reference element. The measurement system comprisesan X-ray tube, a collimator, a detector, a base and a control terminal, wherein the input terminal of the collimator is connected with an exit portal of the X-ray tube, and a tungsten pinhole is formed in the output terminal of the collimator; the control terminal is respectively electrically connected with the X-ray tube and the detector; a reference layer containing the reference element is pasted and placed on the surface of the substrate, and the surface of the reference layer is used for placing a standard sample layer or a to-be-measured sample layer; the X-ray tube is used for emittingX rays, and the base is located on a light path of the X rays; the X rays vertically irradiate the reference layer after passing through the collimator and the tungsten pinhole; and the detector is used for receiving X-ray excited fluorescence.
Owner:NORTHWEST INST OF NUCLEAR TECH

Marine diesel engine waste heat recovery system based on combination of thermoelectric power generation and organic Rankine cycle, and a method thereof

The invention discloses a marine diesel engine waste heat recovery system based on combination of thermoelectric power generation and the organic Rankine cycle, and a method thereof. The marine dieselengine waste heat recovery system comprises a diesel engine intake subsystem, a diesel engine cooling subsystem, an exhaust gas flow path, a TEG subsystem, an ORC subsystem, a seawater cooling subsystem and an electronic control center. A thermoelectric generator is arranged between the exhaust gas flow path and the diesel engine cooling subsystem to form the TEG subsystem, and the temperature differences between the exhaust gas flow path and the diesel engine cooling subsystem are used for generating electricity; the ORC subsystem and the exhaust gas flow path exchange heat through an ORC evaporator; the ORC subsystem converts thermal energy into electrical energy sent from a generator coaxially connected with an expander through a thermodynamic cycle; the seawater cooling subsystem is used for ultimately condensing ORC working media and diesel engine coolants; the electronic control center is part of a diesel engine ECU, and is used for controlling the driving loop. The marine diesel engine waste heat recovery system has the advantages that the exhaust gas waste heat of a diesel engine and the temperature differences between exhaust gases and the coolants are fully utilized, thewaste heat is recycled and converted into the electric energy for ships and other electrical equipment, and accordingly, the energy conversion efficiency of diesel oil is further improved.
Owner:ZHEJIANG UNIV +1

Phase change material microcapsule coated by thermoset phenolic resin and preparation method thereof

The invention discloses a phase change material microcapsule coated by thermoset phenolic resin and a preparation method thereof. The capsule uses a phase change material as a capsule core and the thermoset phenolic resin as the capsule wall. The mass ratio of materials of the microcapsule is that 20-75% of the phase change material, 0.5-3% of an emulsifying agent, 2-10% of a catalyst, 20-60% of thermoset phenolic resin prepolymer and 0.2-10% of a reaction terminating agent. The preparation method comprises heating and melting the phase change material, mixing the phase change material with the emulsifying agent, distilled water and the catalyst to form emulsion, heating the emulsion to 40 DEG C to 80 DEG C, dropwise adding the thermoset phenolic resin prepolymer, keeping constant temperature for 20-100minutes after finishing dropwise adding, adding the reaction terminating agent, adjusting the potential of hydrogen (pH) to about 7.0 with organic acid or inorganic acid, vacuumizing to evaporate moisture, and obtaining the phase change material microcapsule coated with the thermoset phenolic resin. The particle diameter of the phase change material microcapsule ranges from 0.5mum to 4mum. The phase change material microcapsule can be used for manufacturing building materials, thermal storage thermoregulation textiles, crop growth protection agents and the like.
Owner:李雨杉

Method for concentrating at low temperature and pretreating concentrated solution

The invention relates to a method for concentrating at low temperature and pretreating concentrated solution. The method mainly comprises the following steps: 1, preparing mass percentage of formaldehyde solution for reacting to be between 3 and 15 percent; 2, adding frozen diluted formaldehyde solution into a concentration autoclave; 3, adding n-butyl aldehyde and alkali metal hydroxide solution into the autoclave by two parts for two times; 4, dripping methanoic acid into concentrated solution; 5, pumping the acidified concentrated solution into a formaldehyde stripping tower to remove formaldehyde, methanol and partial water; and 6, pumping distillate into a dealcoholizing tower if the mass percentage of the methanol in the distillate obtained in the step five exceeds 2 percent, and distilling the methanol thereinto under normal pressure condition. The concentrated solution obtained through low temperature concentration, step feed and pressurized formaldehyde stripping / dealcoholizing pretreatment has high selectivity, can effectively prevent the formaldehyde, the methanol and the like from reacting with trimethylolpropane in subsequent separating and refining processes and generating unexpected byproducts, thereby improving the quality and the yield of the trimethylolpropane.
Owner:NANTONG BAICHUAN NEW MATERIAL CO LTD +2

Screening device for preparing nanofluids and method for preparing nanofluids

The invention discloses a screening device for preparing nanofluids. The screening device for preparing the nanofluids comprises a flow channel, a fixed screen plate, a dynamic screen plate, an upper peristaltic pump and a lower peristaltic pump, wherein the dynamic screen plate is closely adhered on the fixed screen plate; screen holes in the fixed screen plate are aligned with screen holes in the dynamic screen plate; the circumferential size of the fixed screen plate is equal to the circumferential size of the flow channel; the circumferential size of the dynamic screen plate is less than the circumferential size of the flow channel; gaps are formed in the dynamic screen plate; grooves are formed in the upper part of the fixed screen plate; the gaps in the fixed screen plate correspond to the grooves in the fixed screen plate; the dynamic screen plate and the fixed screen plate divide the flow channel into an upper layer flow channel located above the dynamic screen plate and a lower layer flow channel located below the fixed screen plate; the upper peristaltic pump is connected with two ends of the upper layer flow channel; and the lower peristaltic pump is connected with two ends of the lower layer flow channel. The screening device can remove poorer-dispersity nano-agglomerates parts contained in nano-particles; meanwhile, the invention also discloses a method for preparing the nanofluids; and with the adoption of the method, obtaining of the mass fraction of required nano-particles can be guaranteed and the dispersity of the nanofluids can be improved.
Owner:TONGLING TONGFEI TECH

Process for extracting and refining flavone in highland barley seedlings by enzymolysis-membrane ultrafiltration

The invention relates to the technical field of extraction and refinement of flavonoids compounds in highland barley seedlings, in particular to a process for extracting and refining flavone in highland barley seedlings by enzymolysis-membrane ultrafiltration. The process comprises the following six steps: pretreatment, beating, enzymolysis, extraction, ultrafiltration and drying; wherein in the step of pretreatment, fresh highland barley seedlings with the growth height of 25-40cm are cut; the weight ratio of cellulose to the highland barley seedlings is 1: 100-1000, the temperature is 30-60DEG C, the PH value is 3.5-6, and the stirring time is 0.5-4 hours; in the step of extraction, the weight ratio of highland barley seedling slurry to ethanol of 40-95 percent is 1: 3-10, reflux extraction is carried out for 1-3 hours, and extract obtained in twic is emerged; and in the step of ultrafiltration, the extract is respectively micro-filtered by microfiltration membranes of 1, 0.5 and 0.1mu m, micro-filter filtrate is ultra-filtered by the ultrafiltration membranes, the operating pressure is 0.15-0.25MPa, the temperature is 25-45DEG C, the ultra-filter filtrate is ultra-filtered by the ultrafiltration membranes, the operating pressure is 0.15-0.25MPa, the temperature is 25-45DEG C, and the filtrate is collected. The process is convenient, and the flavone has high yield, high purity and remained activity.
Owner:青海藏源上草药业科技有限公司

Green environmental protection low-temperature impact-resistant PVC-U electrical casing

The invention discloses a green environmental protection low-temperature impact-resistant PVC-U electrical casing. The green environmental protection low-temperature impact-resistant PVC-U electricalcasing comprises the following raw materials in parts by weight: 90-110 parts of PVC resin, 4-6 parts of calcium-zinc composite stabilizer, 6-10 parts of AMB resin, 0.1-1 part of PE wax, 0.1-1 part ofstearic acid, 10-30 parts of inorganic filler, 2-4 parts of processing modifying aid and 2-3 parts of titanium dioxide. As the new calcium-zinc stabilizer replaces the traditional lead salt stabilizing system and the toughening modified ternary copolymer resin (AMB resin) is added, the low-temperature performance is obviously improved compared with the traditional PVC electrical casing, the product still has good toughness at minus 15 DEG C, and meets the construction requirements of the cold market place in the north; compared with the traditional CPE toughening system, the AMB resin dispersed sea-island energy absorption toughening system has obvious advantages, the sea-island energy absorption toughening system can maintain good rigidity at higher temperature. The products are environmental protection green building materials, more in line with modern home decoration requirements.
Owner:ANHUI YONGGAO PLASTIC IND DEV CO LTD

Production and refining method of alpha, alpha'-dinitroanthraquinone

The invention relates to a refining method of alpha, alpha'-dinitroanthraquinone. The method comprises the following steps: carrying out a dinitration reaction on anthraquinone under the effect of a low ratio of sulfuric acid and a high ratio of nitric acid at a low temperature, and distilling concentrated nitric acid at 60-75DEG C in a vacuum condition after completing dinitration reaction the according to a method disclosed in a patent of CN101423477A; slowly cooling materials to a temperature of below 35DEG C when the nitric acid distillation is finished, keeping the temperature for 1h, and precipitating alpha, alpha'-dinitroanthraquinone through crystallization; and filtering a mixture, beating a filter cake in water, refiltering, washing to the pH to above 5, and drying to obtain high quality alpha, alpha'-dinitroanthraquinone. According to the method of the present invention, the distillation amount of concentrated nitric acid can be conveniently controlled to adjust the concentration of nitric acid in a system, so alpha, alpha'-dinitroanthraquinone can satisfy quality requirements; crystallization is carried out below 35DEG C, so generated coarse crystals of alpha, alpha'-dinitroanthraquinone are easy to filter; and the concentration of nitric acid is low in filtering, so operating environment is substantially improved.
Owner:JIANGSU JIHUA CHEMICAL CO LTD
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