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538 results about "Mass fraction" patented technology

In chemistry, the mass fraction of a substance within a mixture is the ratio wᵢ (alternatively denoted Yᵢ) of the mass mᵢ of that substance to the total mass mₜₒₜ of the mixture. Expressed as a formula, the mass fraction is: wᵢ=mᵢ/mₜₒₜ. Because the individual masses of the ingredients of a mixture sum to mₜₒₜ, their mass fractions sum to unity: ∑ᵢ₌₁ⁿwᵢ=1. Mass fraction can also be expressed, with a denominator of 100, as percentage by mass (in commercial contexts often called percentage by weight, abbreviated wt%; see mass versus weight).

Method for preparing graphene reinforced metal-based composite material through discharge plasma (SPS) sintering

The present invention relates to a method for preparing a graphene reinforced metal-based composite material through discharge plasma (SPS) sintering. The method is characterized in that the graphene reinforced metal-based block material is prepared through SPS sintering and has the following advantages that: the preparation method is simple, the material is compact and does not have pores, the graphene mass fraction can be arbitrarily regulated, the distribution is uniform, no aggregation is generated, the material mechanical property isotropy is provided, and the wettability of the metal and the graphene interface is good. The method comprises: (1) reducing graphene oxide through a chemical method or a hydrothermal method to obtain graphene sheets with a sheet layer thickness of not more than 4 nm and sheet layer diameter of not more than 50 [mu]m; and (2) preparing metal powder with a particle size of not more than 200 [mu]m through a rotating electrode atomization method, mechanical crushing or a high-speed ball milling method; (3) carrying out mechanical or ball milling mixing on the graphene powder and the metal powder according to the required mass ratio; and (4) carrying out SPS sintering forming on the mixed powder, wherein the obtained material has characteristics of improved mechanical property, decreased density, good heat conduction capability, and good electric conduction capability, and the performance customizing can be achieved by adjusting the preparation parameters.
Owner:BEIHANG UNIV

Hypoeutectic high-chromium white cast iron and preparation method thereof

The invention discloses a hypoeutectic high-chromium white cast iron, which comprises the following components calculated according to mass fraction: 1.9-2.4 of C, 16-22 of Cr, less than or equal to 0.8 of Si, less than or equal to 0.7 of Mn, 0.5-1.0 of Ni, 1.0-1.7 of Mo, less than 0.04 of S, less than 0.06 of P, 0.05-0.4 of RE, 0.5-1.0 of Cu, 0.05-0.15 of Zn, 0.1-0.3 of V and the balance of Fe. The preparation method comprises the following steps of: defining the mixture ratio according to the requirement of mass fraction and mixing; mixing scrap steel and pig iron in an intermediate-frequency induction furnace and heating the mixture to be melt; after molten iron is smelt, sequentially adding high carbon ferro-chrome, manganese iron, nickel and molybdenum and smelting again; feeding a zinc ingot with small granularity and rare earth or vanadium at the bottom of a casting ladle, covering a steel sheet or scrap iron and compacting; pouring the molten iron into the casting ladle and carrying out metamorphism and deslagging treatment; casting the molten iron and forming to obtain a hypoeutectic high-chromium white cast iron piece; then placing the hypoeutectic high-chromium white cast iron piece into a heat treatment furnace for thermally treating; and quenching and tempering to obtain a hypoeutectic high-chromium white cast iron material with the hardness of 60-66HRC (Hardness Rockwell) and the impact ductility of 10-14J/cm<2>. The hypoeutectic high-chromium white cast iron has the advantages of low cost, high wear resistance and reliable use safety. In addition, the preparation method of the hypoeutectic high-chromium white cast iron is simpler, and is easy in operation and strong in practicability.
Owner:云南化铸科技有限责任公司

TiO2-WO3-SiO2 composite powder used as catalyst carrier and preparation method thereof

The invention discloses and provides a preparation method of TiO2-WO3-SiO2 composite powder used as a catalyst carrier. The method sequentially comprises the following steps: dispersing a metatitanic acid raw material into the slurry through beating, and regulating the concentration of the slurry having the mass fraction of 10 percent to 20 percent and counted with titanium dioxide; respectively adding ammonium paratungstate and white carbon black into the slurry; adding ammonia water and regulating the pH value to be within the range of 5.5 to 8.5; filtering and dehydrating the slurry to obtain a blocky filter cake; mechanically grinding the blocky filter cake obtained after filtering and dehydrating, drying the ground filter cake for 2.5 hours at a temperature of 200 DEG C to 380 DEG C and calcining the dried filter cake for 4.5 hours at a temperature of 380 DEG C to 680 DEG C; and obtaining the TiO2-WO3-SiO2 composite powder after grinding calcined falling materials. The method disclosed by the invention has the advantages of low manufacturing cost, simple process, high specific surface area of a product, high surface chemical activity, and good processing performance. A denitration catalyst prepared from the product has the advantages of high strength, long service life, high catalytic efficiency and the like.
Owner:四川华铁钒钛科技股份有限公司

Sintered Fe-Al-based alloy porous material and filtering element employing same

The invention discloses a sintered Fe-Al-based alloy porous material with better high temperature resistance and antioxidant activity, and a filtering element employing the material. The porosity of the sintered Fe-Al-based alloy porous material is 30% to 60%, and the average pore diameter is 0.5 to 50 mum m; the sintered Fe-Al-based alloy porous material is characterized in that the material is mainly composed of Fe, Al and Si; the sum of the weights of the three elements and accounts for more than 90% of the weight of the sintered Fe-Al-based alloy porous material, wherein the weight of Fe accounts for 60% to 85% of the total weight of Fe and Al, and the weight of Si accounts for 0.5% to 8% of the total weight of Fe, Al and Si; Si in the sintered Fe-Al-based alloy porous material exists mainly in the form of silicon solid solution of Fe-Al-based compound or in the form of Fe5Si and is uniformly distributed in the material approximately; the tensile strength of the sintered Fe-Al-based alloy porous material is larger than or equal to 45 MPa, the thickness is smaller than or equal to 5 mm, and the air flux is large than or equal to 80 m<3>/m<2>/kpa/h; after the material is soaked in NaOH solution with the mass fraction of 5% under the ambient temperature for 15 days, the weight loss ratio is less than 0.5%, and after the material is kept in the atmosphere with the temperature of 800 DEG C for 90 hours, the weight gain rate of the material is tested to be lower than 25%.
Owner:CHENGDU INTERMENT TECH

7XXX aluminum alloy

The invention relates to 7XXX aluminum alloy. The 7XXX aluminum alloy comprises the following components by weight percent: 6.6 to 7.6 percent of zinc, 1.25 to 1.80 percent of magnesium, 0.18 to 0.44 percent of copper, less than or equal to 0.06 percent of silicon, less than or equal to 0.16 percent of iron, , less than or equal to 0.03 percent of manganese, less than or equal to 0.03 percent of chromium, less than or equal to 0.02 percent of germanium, less than or equal to 0.02 percent of vanadium, less than or equal to 0.03 percent of titanium, less than or equal to 0.02 percent of zirconium, and less than or equal to 0.03 percent of total weight of manganese and chromium, less than or equal to 0.03 percent of each rest impurity element, less than or equal to 0.10 percent of total weight of rest impurity elements, and the balance of aluminum. On the basis of experiment, the material strength is improved by re-designing the mass fraction and a ratio of Zn to Mg; by re-designing the mass fraction of Cu, the alloy has excellent corrosion resistance, and the oxidation different color problem of silver white can be solved. By strictly controlling the weight percent of the impurity elements such as Mn and Cr, the crystal grains of the alloy material are uniform. Compared with the existing disclosed Al-Zn alloy system, the alloy has better comprehensive performance, and an oxidized membrane formed by oxidizing the material by virtue of anode is more delicate and beautiful.
Owner:TAISHAN CITY KAM KIU ALUMINUM EXTRUSION

High-tungsten high-abrasion-resistant high-speed steel composite roller and preparation method thereof

The invention belongs to the technical field of abrasion-resistant materials and discloses a high-tungsten high-abrasion-resistant high-speed steel composite roller and a preparation method thereof. The high-tungsten high-abrasion-resistant high-speed steel composite roller comprises a roller core, a composite roller outer layer and a composite roller transition layer, wherein the roller core and the composite roller transition layer are made from ductile iron, and the composite roller outer layer is made from high-tungsten high-speed steel. The preparation method includes: firstly, mixing, heating and melting ferrotungsten, ferrochromium, ferromolybdenum, ferrovanadium, waste steel and carburant in an electric furnace, regulating chemical compositions and mass fractions of the chemical compositions of liquid steel on the spot, and pouring the roller outer layer on a centrifuge, wherein the liquid steel comprises the chemical compositions, by weight, 2.2-2.5% of C, 6.5-6.8% of W, 8.6-9.0% of Cr, 4.2-4.5% of V, 2.5-2.8% of Mo, smaller than 0.45% of Mn, smaller than 0.76% of Si, smaller than 0.04% of P and smaller than 0.04% of S; secondly, pouring the transition layer; finally, filling the core to obtain the composite roller. The high-tungsten high-abrasion-resistant high-speed steel composite roller has excellent utilization effects after quenching and tempering treatment.
Owner:枣庄瑞兴机械制造有限公司

Method for forecasting Ac1 point of martensite refractory-steel weld metal with 9 percent of Cr

The invention relates to a method for forecasting the Ac1 point of martensite refractory-steel weld metal with 9 percent of Cr. The A1 point data of T groups of weld metal with different alloy components are obtained by applying an alloy thermodynamics theory through calculation, a neural network based on error back propagation is constructed, the back propagation (BP) network is trained and tested by utilizing the obtained data, and finally, the output threshold of the trained and tested network is corrected by combining the measured data of the Ac1 point of steel weld metal with 9 percent of Cr so as to obtain a method which can be used for forecasting the Ac1 point of martensite refractory-steel weld metal with 9 percent of Cr. As long as the components (mass fraction) of known weld metal are input, the Ac1 point of weld metal under the condition of the components can be quickly forecasted by utilizing the model. The method for forecasting the Ac1 point of the martensite refractory-steel weld metal with 9 percent of Cr can be used for calculating the Ac1 point of martensite refractory-steel weld metal with 9 percent of Cr under the condition of some kinds of components so as to provide a basis for selecting the postweld heat treatment temperature of the martensite refractory-steel weld metal with 9 percent of Cr. Meanwhile, the method for forecasting the Ac1 point of the martensite refractory-steel weld metal with 9 percent of Cr can also be used for directing the alloying design of the welding material of the martensite refractory-steel weld metal with 9 percent of Cr.
Owner:WUHAN UNIV

In-situ synthesized Al2O3 reinforced molybdenum based composite material and preparation method thereof

The invention discloses an in situ authigenic Al2O3 granule reinforced molybdenum base composite material and a preparation method thereof. The in situ authigenic Al2O3 granule reinforced molybdenum base composite material is prepared with aluminum powder and molybdenum oxide powder, wherein, the mass fraction of the aluminum powder is 0.5 percent to 2.5 percent. Composite material organization prepared is molybdenum base and Al2O3 with the volume fraction of 5 percent to 15 percent, and Al2O3 is distributed evenly in the molybdenum base. The preparation method is as follows: (1) mixing powder is obtained by evenly mixing the aluminum powder and molybdenum oxide; (2) the mixing powder, after heat preservation for 3h in a vacuum sintering furnace at the temperature of 530 DEG C to 550 DEG C under the nitrogen protection, is reduced; (3) the mixing powder is reduced by use of hydrogen at the temperature of 500 DEG C to 550 DEG C for 4h, and at the temperature of 920 DEG C to 950 DEG C for 7h; (4) an isostatic cool pressing is carried out under the pressure of 180MPa to 220MPa and a blank sheet is made by maintaining pressure for 8 minutes to 10 minutes; and (5) the sintering is carried out in the vacuum sintering furnace at the temperature of 1,600 DEG C to 2,000 DEG C for 16h to 18h. The Al2O3 granules are adopted to enhance molybdenum base composite materials, recrystallization temperature reaches more than 1,500 DEG C, the high-temperature strength and rigidity thereof are improved by more than 50 percent compared with TZM molybdenum alloy, and the high-temperature wear resistance thereof is 2 times to 4 times higher than that of the TZM molybdenum alloy. The in situ authigenic Al2O3 granule reinforced molybdenum base composite material has broad application prospect in the high-temperature wear resistance field.
Owner:HENAN UNIV OF SCI & TECH

Low temperature wide-active temperature window SCR denitration catalyst and preparation method thereof

The invention relates to a low temperature wide-active temperature window SCR denitration catalyst. The catalyst comprises a carrier and an active component, wherein the carrier is attapulgite, and the active component is a composition comprising manganese-containing oxide, cerium-containing oxide and copper-containing oxide. The use amount of attapulgite meets a ratio of metal elements to attapulgite of 0.03-0.06mol/20g, the mole percentage of the manganese element in the active component is 50-80%, and a molar ratio of the cerium element to the copper element is 1:10 ~ 1:40. The invention also relates to a preparation method of the catalyst. The preparation method comprises the following steps: adding 20g of purified attapulgite to 100mL of distilled water, sequentially adding 20mL of a manganese nitrate solution with the mass fraction of 50% and certain amounts of cerium nitrate hexahydrate and copper nitrate trihydrate, continuously stirring above added materials for 1h, standing the obtained solution for 4h, drying the obtained material at 80DEG C for 12h, and roasting the dried material in air atmosphere at 500DEG C for 5h; and grinding the roasted material, and sieving the ground material to obtain a 40-60 mesh material used as the catalyst.
Owner:CHINA UNIV OF MINING & TECH (BEIJING)

SnSe/rGO thermoelectric composite material and preparation method thereof

The invention relates to a SnSe/rGO thermoelectric composite material and a preparation method thereof. The mass fraction x of rGO in the thermoelectric composite material ranges from 0.1 wt% to 3 wt%, and the preparation method comprises the steps of s1, preparing graphene oxide dispersion liquid for standby application; s2, SnCl2. 2H2O and NaOH are fully reacted in deionized water according to acertain proportion; s3, adding NaBH4 into the Na2SnO2 aqueous solution obtained in the S2, and uniformly mixing the NaBH4 and the Na2SnO2 aqueous solution; s4, adding the graphene oxide dispersion liquid obtained in the step S1 into the solution obtained in the step S3, mixing and stirring in an argon environment, and then heating to boil; s5, preparing a NaHSe solution with the same amount of substance as Na2SnO2 in S2, and then adding the NaHSe solution into the mixed solution obtained in S4; S6, keeping the stirring rate in S4 and reacting at the boiling temperature; and S7, after the reaction is finished and cooling is conducted, performing suction filtration and collection on the reaction solution and then placing the solution in a vacuum drying box to be fully dried, and s8, performing the spark plasma sintering on the composite powder obtained in the S7, and obtaining the SnSe/rGO thermoelectric composite material.
Owner:CHONGQING UNIV

Method for enabling waste active carbon powder to be used for sintering, sintering mixture and sinter

The embodiment of the invention provides a method for enabling waste active carbon powder to be used for sintering, a sintering mixture and sinter. The waste active carbon powder is generated when sintering smoke is purified by active carbon. The method includes the steps that the waste active carbon powder and coke powder are mixed according to the mass ratio of (12-37.8):(62.2-88), and sinteringfuel is obtained; the granularity of the waste active carbon powder is smaller than or equal to 3 mm, wherein the mass fraction of the waste active carbon powder with the granularity smaller than 0.5mm is 70%-80%; the granularity of the coke powder is smaller than or equal to 8 mm, wherein the mass fraction of the coke powder with the granularity smaller than 0.5 mm is 10%-15%; the sintering fuel, to-be-sintered iron ore powder and a solvent are mixed, and the sintering mixture is obtained; the mass ratio of the sintering fuel to the to-be-sintered iron ore powder is (3-6):(75-90); and afterbeing pelletized, the sintering mixture is sintered. By the adoption of the method, the sintering rate can reach 88.87%, the yield of the sinter can reach 76.44%, the prepared sinter is good in metallurgical performance, the drum strength of the sinter is larger than 81%, the SO2 concentration of exhausted smoke is not larger than 38 mg/m<3>, and the NOx concentration is not larger than 94 mg/m<3>. Meanwhile, secondary utilization of the waste active carbon powder is achieved.
Owner:武汉钢铁有限公司

Low-cost high-plasticity soluble magnesium alloy material and preparation method thereof

The invention discloses a low-cost high-plasticity soluble magnesium alloy material and a preparation method thereof. The magnesium alloy comprises the components of MgAlZn<c>Mn<d>Ca<e>Ni<f>Si<g>Sn<h>, wherein a, b, c, d, e, f, g and h represent the mass fraction of each element, b ranges from 0.5%-15%, c is in the range of 0.1%-6%, d is in the range of 0.05%-2%, e is in the range of 0.01%-3%, f is in the range of 0.01%-6%, g is in the range of 0%-2%, h is in the range of 0%-5%, and the sum of a, b, c, d, e, f, g, and h is equal to 100%; and after smelting, casting, homogenization treatment, hot extrusion and aging treatment are carried out, the required alloy material is obtained. According to the low-cost high-plasticity soluble magnesium alloy material and the preparation method thereof, compared with the prior art, the magnesium alloy material prepared by the components and the process is adopted, the cost is low, the production is convenient and fast, a finished product hasgood strength and high plasticity, and can be rapidly dissolved in a solution containing a microscale electrolyte, the low-cost high-plasticity soluble magnesium alloy material is suitable for a soluble downhole tool used in oil processing and preparing and gas field fracturing process, the downhole tool prepared by the material is adopted and can be self-dissolved after service is finished, the subsequent procedures such as flowback, drilling and milling can be omitted, the construction efficiency is greatly improved, the construction cost is saved, and the energy consumption is reduced.
Owner:大同高镁科技有限公司

Preparation method of chromium-silicon alloy sputtering target material

The invention provides a preparation method of a chromium-silicon alloy sputtering target material. The preparation method comprises the following steps that chromium powder and silicon powder are subjected to ball-milling and mixing in a protective atmosphere to obtain a mixture, and the mass fraction of the silicon powder in the mixture is not more than 16wt%; the obtained mixture is loaded into a mold and compacted, and then vacuum-pumping treatment is carried out; after the vacuumizing treatment is completed, first heat treatment is carried out, and the pressure in the first heat treatment process does not exceed 6 MPa; second heat treatment, first pressurization, second pressurization and heat preservation and pressure maintaining are carried out in sequence; after heat preservation and pressure maintaining are finished, protective gas replacement is carried out till the pressure ranges from-0.06 MPag to-0.08 MPag, and then cooling in furnace is carried out; and machining is carried out to a required size to complete the preparation of the chromium-silicon alloy sputtering target material. According to the preparation method, the chromium-silicon alloy target material with the silicon content not exceeding 16wt% can be prepared, and the density of the prepared target material is greater than 99%, the purity is greater than or equal to 99.95%, and the requirements of magnetron sputtering on the purity and density of the target material are met.
Owner:KONFOONG MATERIALS INTERNATIONAL CO LTD

Method for preparing unleaded free-cutting brass

A method for preparing unleaded free-cutting brass is used for production by means of a powder activation sintering process. Powder and binder include, in mass fraction ratio, sintering activator which contains from 0.2% to 0.5% of phosphorous copper powder and from 0.06% to 0.40% of second-phase micropowder, binder which contains from 0.5% to 1.0% of zinc stearate, from 0.3% to 0.5% of dispersant PVA (polyvinyl alcohol), and the rest percentage of brass powder. Sintering is performed after mixing and pressing, and the sintering process includes that heating is performed from the room temperature to the sintering temperature ranging from 830 DEG C to 850 DEG C in a reducing atmosphere, wherein the heating time ranges from 2 hours to 5 hours, and the sintering time ranges from 45 minutes to 75 minutes. The second-phase micropowder is graphite micropowder, hexagonal boron nitride micropowder, manganese sulfide micropowder or molybdenum disulfide micropowder, the granularity of the second-phase micropowder ranges from 1 micrometer to 10 micrometers, the granularity of the brass powder is not larger than 106 micrometers, and the granularity of the phosphorous copper powder is not larger than 75 micrometers. The brass prepared by the method does not contain lead, bismuth and antimony, and the method is environment-friendly, suitable for mass production and low in production cost.
Owner:HUNAN TERRY NEW MATERIALS COMPANY

Powder for laser cladding in-situ self-generated vanadium carbide reinforced iron-based alloy and preparation method

The invention discloses powder for laser cladding in-situ self-generated vanadium carbide reinforced iron-based alloy and a preparation method. The alloy powder prepared by a vacuum gas atomization method comprises, by mass, 4.00%-4.40% of C, 16.00%-18.00% of V, 8.00%-10.00% of Cr, 0.90%-1.30% of Si, 1.00%-2.00% of Mo, 0.90%-1.20% of Mn, 0.40%-0.70% of Ni, 0.30%-0.50% of Al, P, S, less than or equal to 300 ppm of O, and the balance Fe, wherein the total mass fraction of P and S is less than or equal to 0.03%. The preparation method comprises the steps that the alloy powder clads the surface oflow-carbon alloy steel base material through laser by adopting a CO2 laser processing system in a synchronous powder feeding mode, the cladding-layer powder absorbs laser energy to form a molten poolon the surface of the base material, a C element and a V element in the molten pool react to generate an in-situ self-generated V8C7 ceramic reinforced phase, and meanwhile, the cladding layer and the base material form good metallurgical bonding. By preparing the in-situ self-generated V8C7 particle reinforced iron-based alloy laser cladding layer, the hardness and the wear resistance of the surface of a low-alloy steel component can be remarkably improved, and the method can be widely applied to laser manufacturing and remanufacturing of mechanical parts under friction and wear working conditions in the industrial field, and has remarkable economic and social benefits.
Owner:SHENYANG POLYTECHNIC UNIV
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