This invention relates to the field of medical
ceramic materials technology, and more particularly to a method for preparing a zirconia-based medical
composite ceramic material. The method includes: adjusting the target number of cycles in response to the
slurry mixing state, or compensatingly adjusting the
spray granulation process parameters based on
slurry state parameters; determining whether the current batch of green bodies has a risk of closed pores based on the
green body characteristics, and determining an adjustment feature point based on the actual
shrinkage rate variation; stopping the
sintering heating and adding a holding stage in response to the adjustment feature point, and determining the intermediate holding temperature and the holding stage duration; obtaining the sintered body phase to determine the
tetragonal zirconia retention rate, and determining whether the
sintering adjustment strategy matches the characteristics of the current batch of
slurry based on the sintered body performance; and adjusting the intermediate holding temperature of subsequent
sintering processes based on the tetragonal phase
retention rate deviation in response to the sintered body performance. This invention improves the performance of
ceramic implants by adjusting the sintering
temperature curve based on the characteristics of zirconia-based
powder.