1874results about How to "Good linear relationship" patented technology

The invention relates to a health monitoring method used for a cable system in a cable structure which carries out a plurality of mechanical calculations based on the mechanical calculation benchmark model of a structure; the calculation times are equal to the quantities of the cables. In each calculation, one cable is supposed to have unit damage; the result for each calculation forms vector for calculating a current cable force; a cable force change vector is obtained by using the vector for calculating the current cable force to subtract an initial cable force vector; all the cable force change vectors form a cable force change identity matrix. The noninferior solution of the current damage vector of the cable can be fast calculated by utilizing proper arithmetic such as multi-target optimizing arithmetic according to the approximating linear relation of the current cable force vector (formed by all the current cable forces that are actually detected), the cable force change identity matrix, a unit damage scalar and the current cable damage vector (formed by all the current damage quantities), thus being capable of more accurately confirming the position and the damage degree of the damaged cable.

The invention provides a method for simultaneously determining one hundred pesticide residuals in a traditional Chinese medicine through ultrahigh performance liquid chromatography-tandem quadrupole mass spectrum. The method comprises the following steps: immersing traditional Chinese medicine powder with ultrapure water, extracting with acetonitrile containing 0.1% acetic acid through a homogenate method, carrying out solid phase dispersing purification with N-propylethylenediamine and graphitized carbon, detecting in a timesharing multi-reaction monitoring mode through the ultrahigh performance liquid chromatography-tandem quadrupole mass spectrum, and quantifying with an external standard curve method. 88% of pesticides have good linear relations in a range of 5-500ng/mL, correlation coefficients are above 0.99, and the correlation coefficients of above 98% of the pesticides are above 0.97; the average recovery rate of the pesticides with the low concentration of 10mug/kg, the middle concentration of 50mug/kg and the high concentration of 100mug/kg is 70-130%, and the relative standard deviation is less than 0.15; and the detection limit is equal to or less than 0.01mg/kg, so routine detection requirements can be completely satisfied. The method has the advantages of strong versatility, good selectivity, high sensitivity, and rapidness and simplicity.

An off-resonance photoacoustic spectrometric detection and analysis device consists of a photoacoustic spectrometric module (8). The photoacoustic spectrometric module (8) comprises a light source module (2-1), a photoacoustic signal generation module (2-2), an optical power measurement module (2-3) and a fault diagnostic analysis module (2-4). Optical signals generated by an infrared incoherence light source in the light source module (2-1) are focused by an ellipsoidal reflector to form a focused light beam, the focused light beam is modulated into light of specific frequency and wavelength by chopping blades of an optical chopper and optical filters and then transmitted to the photoacoustic signal generation module (2-2), and the fault diagnostic analysis module (2-4) calculates each gas concentration according to to-be-tested gas photoacoustic signals generated by irradiation, diagnoses faults and alarms. The off-resonance photoacoustic spectrometric detection and analysis device can be used for quantitative detection of gases such as SF6, CF4, SO2F2, SOF2, SO2, SF4 and H2O and is applicable to onsite online monitoring.

The invention discloses a method for controlling the quality of Moluo Dan, which comprises the discrimination method for thin layer of Ophiopogon japonicus, pseudo-ginseng, Sanguisorba officinalis, angelica sinensis, Ligusticum wallichii and corydalis tuber, as well as the content determining of paeoniflorin (C23H28O11) in white Chinese herbaceous peony. The white Chinese herbaceous peony contained in each 1g of Moluo Dan is expressed by C23H28O11, which shall not be less than 0.8 mg.

The invention discloses a health monitoring system of a cable system in a cable structure on the basis of strain monitoring; a plurality of times of mechanical calculation is carried out on the basis of the reference model of the mechanical calculation of a structure, the times of the calculation is equal to the number of cables. Supposing that only one cable has unit damage during each calculation, the calculation result of each time constitutes a current strain calculation vector; a strain change vector is obtained by that each current strain calculation vector minus an initial strain vector; all the strain change vectors constitute a unit damage strain change matrix. According to the similar linear relation between the current strain vector (constituted by the current measured strain of all the given points) and the initial strain vector, the unit damage strain change matrix, an unit damage scalar and a current cable damage vector (constituted by current damage amount of all cables), the noninferior solution of the current cable damage vector can be figured out fast by utilizing the suitable algorithms of multi-objective optimization algorithm, etc., therefore, the position and the degree of damage of the damaged cable can be determined accurately.

The invention discloses a visible and reversible fluorescent probe which comprises a cyanine fluorescent group and a benzothiazole group, and the general formula of the probe is shown in the description. The preparation method of the reversible fluorescent probe comprises the following steps: (1) dropwise adding phosphorus oxychloride into salicylaldehyde and paraformaldehyde for reaction, so as to obtain a product 1; (2) enabling the product 1 and hexamethylene-tetramine to react, so as to obtain a product 2; (3) enabling the product 2 and 2-aminobenzenethiol to react at the room temperature, so as to obtain a product 3; (4) enabling the product 3 and a compound 4 to react, so as to obtain the visible and reversible fluorescent probe. According to the ratiometric fluorescent probe provided by the invention, obvious color variation can be found out under natural light or an ultra-violet lamp, and the qualitative detection of sulfur dioxide gas can be implemented under natural light or a hand-held ultra-violet lamp, so that the operation is simple, high convenience and quickness are achieved, and the effect is remarkable; the fluorescent probe can effectively prevent interference from other impurities in samples, and is excellent in selectivity; in addition, the cumbersome pre-processing process of samples is avoided, so that the detection efficiency is high.

The invention relates to the field of analytical chemistry and food safety, and provides a high performance liquid chromatography detection method for residual quantity of multiple ultraviolet absorbents in cosmetics. A cosmetic sample of 0.4g is weighed and placed in a plastic centrifuge tube of 50 ml, sample extraction liquid of 20ml is added, after the cosmetic sample of 0.4g and the sample extraction liquid of 20ml are mixed for 2 minutes in a vortex mode, sonic oscillation extraction is carried out for 20 minutes, 8000 revolutions per minute centrifugation is carried out for 10 minutes and, and supernate is to be purified; and after test solutions sequentially pass through microfiltration membranes of 0.45 micrometer and 0.20 micrometer, a high performance liquid chromatograph is adopted to carry out qualitative determination and quantitative assay. The detection method has the advantages of being simple, fast, accurate, efficient, and the like, and can detect 12 ultraviolet absorbents at the same time. Technical indexes of detection minimum, the recovery rate, the degree of precision, and the like all meet relevant demands for ultraviolet absorbent detection in sun block cosmetics at home and abroad. The method is suitable for detection and monitoring of the ultraviolet absorbents in the sun block cosmetics, and has great significance on promoting of import and export trade of cosmetics of our country, ensuring of safety of the cosmetics, and guarantee of human body health.

The invention relates to an EML4-ALK (echinoderm microtubule associated protein like4-anaplastic lymphoma kinase) fusion gene fluorescent quantitative PCR (polymerase chain reaction) assay kit, which is applicable to assay of EML4-ALK fusion gene mutation in lung adenocarcinoma. The kit comprises probes, primers and positive controls, which are specially designed for conserved sequences of 9 fusion variations of the EML4-ALK fusion gene. The kit can be used for quickly and accurately assaying 9 most common EML4-ALK fusion gene variations with high sensitivity, namely 9 fusion variations of 7 variant subtypes, which are subtype 1 (E13; A20), subtype 2 (E20; A20), subtype 3 (E6a/b; A20), subtype 4 (E14; A20), subtype 5 (E2a/b; A20), subtype 6 (E18; A20) and subtype 7 (E14; A20), so that a real-time fluorescent quantitative PCR system for assaying 9 most common EML4-ALK fusion gene variations can be established.

The invention provides a minitype optical fiber FP sensor produced by fetosecond laser pulse, which is to produce a small cavity with rectangle cross section, and full penetration through fiber core on an ordinary single-mode optical fiber, and the depth of the small cavity satisfies: (D+d)/2<=h<=D, wherein D is the diameter of the fiber, d is fiber core diameter. The invention also provides the production method of the invention. The sensor is superior in not only the special physical characteristic of miniaturization, integration, Convenience for production and reuse, strong harsh environment resistance capability, but also having negative temperature sensitivity and improving the sensitivity of axial load in a certain extent, and being applied in the optical sensing field in the future.

The invention relates to a preparation method of a graphite oxide phase carbon nitride modified electrode. The preparation method comprises the following steps: (1) preparing graphite oxide phase carbon nitride; and (2) preparing a graphite oxide phase carbon nitride sensor. The electrode is applied to detecting heavy metal ions. Graphite oxide phase carbon is of a three-dimensional hole structure which is large in specific surface area and contains hydrophilic groups such as hydroxyl, carboxyl, and epoxy groups. The graphite oxide phase carbon is applied to an electrochemical sensor. The heavy metal ions Cu<2+> are detected by virtue of a different pulse stripping voltammetry, and influence of factors such as enriching time, enriching potential, the pH value of a solution, and modification amount on stripping peak current can be optimized. Under an experimental condition that the enriching time is 300s, the enriching potential is -0.6V, the pH value of the solution is 4.68 and the modification amount is 12 microliters, a standard curve represents a good linear relationship, wherein the linear range is (1.60*10<-15>-6.31*10<-15>mol/L, the linear equation is ip(microA)=1.2533C(micro mol/L)+6.2232, the correlation coefficient (R) is 0.9989, and the limit of detection (S/N=3) reaches 1*10<-16>mol/l. The electrode has ultrahigh sensitivity to heavy metal ion detection.

The invention relates to a tumor-targeted T1-T2 double nuclear magnetic resonance imaging contrast agent and a preparation method and an application thereof. The contrast agent comprises hyaluronic acid-coated ferroferric oxide composite magnetic nanoparticles, wherein the molecular formula of hyaluronic acid is as shown in the specification; n is an integer of 17-290. The preparation method of the contrast agent comprises the following steps: (1) dissolving hyaluronic acid into deionized water, introducing a gas, and heating to obtain a reaction system A; (2) dissolving ferric salt and ferrous salt into a strong acid to obtain a solution B; (3) injecting the solution B into the reaction system A, adjusting the pH to be alkaline, and then refluxing at a high temperature to obtain a reaction system C; and (4) cooling a reaction system C to a room temperature, and dialyzing to obtain the contrast agent. The invention further provides an application of the contrast agent in T1 and T2 weighted imaging in in-vivo and in-vitro nuclear magnetic resonance. The contrast agent provided by the invention has superparamagnetism and outstanding T1 and T2 relaxation enhancement effects, and is suitable for being used as a T1-T2 double nuclear magnetic resonance imaging contrast agent.

The invention discloses preparation and quality detection method of compound prescription cortex phellodendri chinensis fluid. The quality detection method comprises the identification of forsythia fruit, cortex phellodendri, honeysuckle and dandehon herb, the checking of lonicerae flos, and the content determination of forsythin and berberine hydrochloride. According to the determination method, spots with the same colors are formed in a qualified test article thin-layer chromatogram and in corresponding positions of a reference substance thin-layer chromatogram, and negative control is interference-free, and the method is good in selectivity, simple and accurate. The checking method of lonicerae flos adopts a high performance liquid chromatography, is good in specificity, and can distinguish the situation that lonicerae flos is adopted in the compound prescription cortex phellodendri chinensis fluid to pretend honeysuckle flower to charge material. The content determination of forsythin and berberine hydrochloride is good in linear relation and high in recovery test accurancy, has good repeatability and stability, can accurately and strictly detect the quality of the compound prescription cortex phellodendri chinensis fluid, and guarantees a high quality standard level of the compound prescription cortex phellodendri chinensis fluid.

The invention relates to an abandoned land remote sensing recognition method based on texture and vegetation indexes. The characteristics of multiple sensors, multiple resolutions, multiple spectra and multidate remote sensing data are utilized, the spectra and the textural features of remote sensing images, and the vegetation index features are combined, and the abandoned land remote sensing recognition method based on the texture and the vegetation indexes is established by structuring a remote sensing image registration and fusion framework, a spectrum and texture feature space and a vegetation index time sequence. Compared with an existing abandoned land remote sensing recognition method, the abandoned land remote sensing recognition method based on the texture and the vegetation indexes solves the precision problem brought by broken cultivated land, reduces artificial involvement subjectivity and improves abandoned land recognition efficiency. The abandoned land remote sensing recognition method based on the texture and the vegetation indexes is characterized in that a remote image registration and fusion unit, a typical spectrum and texture feature unit, a vegetation index time sequence feature unit and an abandoned land recognition and information extraction unit are included. Through the abandoned land remote sensing recognition method with the four units, the distribution information and data of abandoned land in a large range area can be recognized fast and precisely, and auxiliary decision-making data support can be provided for land utilization, grain guarantee and the like.

The invention relates to the technical field of edible oil, and provides a method for detecting the adulterated tea oil. The method comprises the following steps of: firstly, establishing a refractive index, an iodine value, a saponification value and an oleic acid content adulteration detection model, determining the adulteration type by detecting the sample, then, determining an adulteration quantity model through ultraviolet spectrum full-wave scanning, and comparing the data to obtain the determined adulteration quantity. According to the method provided by the invention, not only can the adulteration type for the tea oil be identified, but also the adulteration quantity can be detected, so that cheap edible oil can be prevented from being used for personating expensive tea oil. The method provided by the invention has the characteristics of being economical and simple, excellent in repeatability and high in accuracy, and the like, can be practically used for the teal oil adulteration detection work, and can guarantee and safeguard the benefits of consumers.