The invention relates to the technical field of
plant effective component extraction, in particular to a
camellia nitidissima polyphenol component
microwave-assisted extraction and preparation method, which comprises the following steps: S101, composite pretreatment; s102, preparing an extraction
solvent and loading; s103, setting a dual-frequency
microwave extraction parameter; s104, performing double-frequency
microwave constant-temperature dynamic extraction; s105, stopping extraction and quickly cooling; s106, carrying out online
solid-liquid separation and
impurity pretreatment; s107, carrying out
gradient elution and purification; s108, carrying out
antioxidant protection and concentration; and S109,
freeze drying and finished product preparation. By adopting a composite pretreatment process of ultrahigh pressure and composite enzymolysis, the macrostructure of
cell walls is firstly destroyed by ultrahigh pressure treatment, and
cellulose and
pectin in the
cell walls are further degraded by compound
enzyme to form a continuous component
dissolution channel, so that the problem that the
cell walls are not fully destroyed by a traditional pretreatment mode is fundamentally solved; and meanwhile, the dual-frequency microwave constant-temperature dynamic extraction is combined, so that the extraction rate of the tea
polyphenol is improved.