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262results about How to "The preparation process is easy to control" patented technology

Preparation method of novel three-dimensional nitrogen doped graphene composite material system

The invention discloses a preparation method of a novel three-dimensional nitrogen doped graphene composite material system. The method comprises the following steps: 1, uniformly dispersing graphene oxide in a solvent at room temperature, adding a selected material and a nitrogen-containing compound, and uniformly mixing to form a mixed solution; 2, reacting the mixed solution at a temperature from room temperature to 150DEG C for 0-8h; and 3, cooling the above obtained product to room temperature, centrifuging, collecting the obtained product, washing, and drying to obtain the nitrogen doped graphene composite material. The three-dimensional nitrogen doped graphene composite material system with the nitrogen content of 8-19% can be efficiently and controllably prepared through the method, and the nitrogen content of the system can be controlled by changing the kind and the amount of the added nitrogen-containing compound, the reaction temperature and the reaction time; and the method is simple, is easy to enforce, allows the yield to be greater than 98.9%, and can be widely used in fields of water treatment, biomedicines, energy generation, conversion and storage devices, electrostatic prevention, heat management, heat conduction and dissipation, sensors, electromagnetic shielding, wave absorption and catalysis.
Owner:SUZHOU INST OF NANO TECH & NANO BIONICS CHINESE ACEDEMY OF SCI

Ultra-large-diameter bamboo winding composite tube and manufacturing method thereof

ActiveCN105715881AImprove axial strengthEnhanced bending and impact resistanceRigid pipesTubular articlesStress distributionFiber
The invention belongs to the related field of composite tubes, and discloses an ultra-large-diameter bamboo winding composite tube. The bamboo winding composite tube comprises a lining layer, a composite strengthening layer and an outer protection layer from inside to outside, and the lining layer is made of fiber blankets or non-woven fabrics with anticorrosive resin in an adhesion manner; the composite strengthening layer is formed in a manner that two different types of bamboo skin curtains are wound outside the lining layer in a layer-by-layer manner according to the proper layer number and the thickness proportion wholly in the ring direction, the bamboo skin curtains are sprayed with the resin in a liquid-leaching manner while winding is carried out, and then bonding curing is carried out; and the outer protection layer is cured on the outer surface of the strengthening layer in a coating manner, and the effects of water prevention, corrosion prevention, radiation prevention and the like are achieved. The invention further discloses a corresponding manufacturing method. Through the ultra-large-diameter bamboo winding composite tube and the manufacturing method, even under the tube diameter obvious expanding condition, the characteristic that the whole structure of the bamboo winding composite tube is free of stress distribution defect can be well kept, and meanwhile comprehensive properties of pressure resistance, ring stiffness, long-term use quality stability and the like can be obviously improved.
Owner:ZHEJIANG XINZHOU BAMBOO BASED COMPOSITES TECH +1

Composite degradable antibacterial artificial cerebral dura mater and preparation method thereof

The invention provides a composite degradable antibacterial artificial cerebral dura mater, comprising a vancomycin or ofloxacin hydrochloride injection, chitosan and sodium beta-glycerophosphate. The invention is characterized in that a spongy collagen biomembrane stent is prepared from a decellularized membrane-like derivative material, a chitosan solution with a concentration of 2% (w / v) and a sodium beta-glycerophosphate solution with a concentration of 56% (w / v) are used and mixed, and since a hydrogel formed by a compound of the chitosan solution and the sodium beta-glycerophosphate solution at a temperature of 37 DEG C has the characteristic of temperature sensitivity, the vancomycin or ofloxacin hydrochloride injection is added into the compound to form a solution which is used for soaking of the prepared spongy collagen biomembrane stent to prepare a suture-free cerebral dura mater, and the hydrogel compound uniformly infiltrates into the spongy collagen biomembrane stent after disposition in an incubator with a temperature of 37 DEG C for 10 min so as to form the absorbable artificial cerebral dura mater with antibacterial activity. The invention further provides a preparation method. The preparation method has the characteristics of convenience in preparation, easy film formation, low cost, convenient operation, etc.
Owner:BEIHUA UNIV

Bacterial cellulose membrane with gradient structure and preparation method thereof

The invention discloses a bacterial cellulose membrane in a gradient structure and a preparation method of the bacterial cellulose membrane. The bacterial cellulose membrane is prepared by the steps of adding crop starch in a fermentation culture solution, heating for gelatinizing the mixture, adding a thickening agent into the gelatinized mixture, and carrying out static culture; and the bacterial cellulose membrane has a gradient structure with continuous transition from a compact upper surface downwards to a loose lower surface. The in-site fast controllable preparation of the gradient structure of the bacterial cellulose membrane can be realized by adjusting the proportion of the crop starch to the thickening agent. The preparation method of the bacterial cellulose membrane disclosed by the invention has the advantages that the resources of raw materials are wide, biosynthesis process is mild and pollution-free, and the product is environment-friendly, safe, low in production cost, controllable in process and designable and has a bright large-scale production prospect. The bacterial cellulose membrane with the gradient structure is suitable for the fields of cosmetics and biomedical materials including a facial mask, a cooling paste, a wound dressing, an artificial skin and the like.
Owner:DONGHUA UNIV

Rotary writing method of multi-core fiber grating

The invention provides a rotary writing method of a multi-core fiber grating, which comprises the following steps of stripping one section of coating on a multi-core fiber; fixing the multi-core fiber on a fiber fixture after cleaning treatment; arranging the fiber fixture on a rotary optical device; tightly attaching the multi-core fiber to a mask; regulating the rotary optical device so that one fiber core aligns with a writing optical source; starting an excimer laser, and conducting exposure after the optical source becomes parallel light through collimating and beam expanding; connecting one end of the multi-core fiber to a broadband optical source, and connecting the other end to a spectrograph; monitoring grating formation through the spectrograph, and stopping exposure after achieving the required reflectivity; regulating the rotary optical device to a proper angle so that the next fiber core of the multi-core fiber rightly aligns with the writing source for writing fiber by fiber; and packaging. The invention has the advantages of simple implementation and easy control, and can improve the writing quality of the grating; a plurality of manufactured multi-core fiber gratings are integrated in one fiber, which improves the integration of optical devices in the fiber and can be used for simultaneously measuring a plurality of physical quantities and multi-dimension information.
Owner:HARBIN ENG UNIV

Preparation method for tetragonal phase nano barium titanate

The invention provides a preparation method for tetragonal phase nano barium titanate. The preparation method comprises the steps as follows: i), preparing water solutions of barium chloride and oxalic acid respectively, and mixing alcoholic solution of butyl titanate and oxalic acid solution uniformly to obtain titanium oxyoxalate complex ion solution; ii), adding titanium oxyoxalate complex ion solution obtained in the step i) into a supergravity reactor as a circulating flowing phase to control the supergravity level; and meanwhile, dropping barium chloride solution to obtain white barium titanyl oxalate precipitation suspension as a precursor of barium titanate, and keeping the pH value of the whole system at 2.5-3.5 during reaction; and iii),ageing the precipitation suspension obtained in the step ii), leaching, washing and drying to obtain white barium titanyl oxalate power. The preparation method provided by the invention has the advantages that tetragonal phase nano barium titanate can be prepared; and the particle size of the prepared power can be controlled to be within the range of 30-90 nm; the average particle size is small, and the particle size is narrow in distribution; and the degree of crystallinity is high, and the crystal formation is intact.
Owner:XIANGTAN UNIV

Method for preparing large-grain spherical praseodymium neodymium oxide

The invention relates to a method for preparing large-grain spherical praseodymium neodymium oxide, belonging to a preparation technology of material. The method comprises the following steps of: taking praseodymium neodymium chloride solution as raw material, taking ammonium bicarbonate as precipitator, preparing basic praseodymium neodymium carbonate, and washing, filtering, centrifugally dripping and firing basic praseodymium neodymium carbonate precipitate, to obtain the spherical praseodymium neodymium oxide product with the centre grain diameter being from 25 to 30 mu m. The precipitation temperature and concentration of the basic praseodymium neodymium carbonate in the method are key factors, the precipitation temperature is less than 85 DEG C to obtain the praseodymium neodymium carbonate rather than the basic praseodymium neodymium carbonate, the preparation technology is easy to control, the large-grain praseodymium neodymium oxide product with the centre grain diameter being from 25 to 30 mu m is produced by a factory conventional praseodymium neodymium carbonate preparation working procedure, and the praseodymium neodymium oxide is even in grain distribution, good in dispersity and spherical in appearance.
Owner:INNER MONGOLIA UNIV OF SCI & TECH +1
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