1942results about How to "Good size control" patented technology

Nanoribbons and nanowires having diameters less than the wavelength of light are used in the formation and operation of optical circuits and devices. Such nanostructures function as subwavelength optical waveguides which form a fundamental building block for optical integration. The extraordinary length, flexibility and strength of these structures enable their manipulation on surfaces, including the precise positioning and optical linking of nanoribbon/wire waveguides and other nanoribbon/wire elements to form optical networks and devices. In addition, such structures provide for waveguiding in liquids, enabling them to further be used in other applications such as optical probes and sensors.

According to the disclosed method, there is provided a structure consisting of a silicon substrate coated with a bottom thin SiO2 layer, a doped polysilicon layer, a refractory metal layer and a top Si3N4 capping layer. Said refractory metal and doped polysilicon layers will form a polycide layer under subsequent thermal treatments. First, a sacrificial layer of a dielectric material such as oxynitride is deposited onto the structure. Oxynitride is impervious to UV radiation and has excellent conformal properties. Then, a layer of a photoresist material is deposited onto the structure and patterned to form a mask. Now the dielectric and top Si3N4 layers are anisotropically etched using the photoresist mask. The mask is stripped and the refractory metal and doped polysilicon layers are anisotropically dry etched down to the SiO2 layer using the patterned dielectric layer as an in-situ hard mask. A conformal layer of Si3N4 is deposited onto the structure, then anisotropically dry etched until the thin SiO2 layer is exposed to form the Si3N4 spacers. Diffusion regions are formed in the substrate by ion implantation. A layer of BPSG is deposited onto the structure and planarized. Contact holes are formed to expose said diffusion regions and filled with a metal to create borderless metal contacts therewith.

A method for producing a material includes providing a metallurgical powder including iron, 1.0 to 3.5 weight percent copper, and 0.3 to 0.8 weight percent carbon. At least a portion of the powder is compressed at 20 tsi to 70 tsi to provide a compact, and subsequently the compact is heated at high temperature and then cooled at a cooling rate no greater than 60° F. per minute to increase the surface hardness of the compact to no greater than RC 25. The density of at least a region of the sintered compact is increased, by a mechanical working step or otherwise, to at least 7.6 grams/cc. The sintered compact is then re-heated to high temperature and cooled at a cooling rate of at least 120° F./min. so as to increase the surface hardness of the compact to greater than RC 25, and preferably at least RC 30. Material made by the method of the invention also is disclosed.

The invention provides a microfluidic device and a method for preparing microgel by using the microfluidic device. The method comprises the steps of (1) taking a solution containing live cells or bioactive molecules, a photocuring agent and a hydrogel prepolymer as an internal phase, taking a mixed solution containing oil and an surfactant as an intermediate phase, and taking a polyvinyl alcohol aqueous solution as an external phase; (2) respectively conveying the internal phase, the intermediate phase and the external phase into a corresponding microchannel of the microfluidic device through a micro pump or a micro injector to form a monodispersed water-in-oil-in-water double emulsion; (3) enabling the monodispersed water-in-oil-in-water double emulsion in the step (2) to pass through an output channel of the microfluidic device, and collecting the monodispersed water-in-oil-in-water double emulsion in the step (2) into a collection vessel filled with an aqueous solution, thus obtaining the microgel immobilizing with the live cells or the bioactive molecules. The preparation of the microgel immobilizing with cells by a one-step method is realized, the obtained microgel is controllable in size, and narrow in size distribution, and meanwhile the survival rate of cells is maintained.

The invention relates to a hyper branched polyamide amine and metal nanometer compound and the preparation method and the application, belonging to the technical field of nanotechnology which is characterized in that: the compound comprises a polymer and metal nanometer particles, the polymer is the hyper branched polyamide amine made of blocking modification the hyper branched polyamide amine of the vinyl-terminated through different small organic molecules with amine, the content of the polymer is 89wt percent to 98wt percent; the metal nanometer particles are golden or silver nanometer particles, the content of the metal nanometer particles is 2wt percent to 11wt percent. During the preparation course, no reducing agent or ultraviolet irradiation is required, the precursor metal compounds are directly added into the hyper branched polyamide amine solution, and the metal nanometer particles with perfect water dispersion is generated only through one-step reaction under ambient temperature, the average particle size of which is one to eight nm, and the size is controllable. The inhibition zone method and the optical density method tested show that: the hyper branched polyamide amine and the metal nanometer particle compound have perfect antibacterial effects to a plurality of bacteria and fungus.

A method and apparatus for process integration in manufacture of a photomask are disclosed. In one embodiment, a cluster tool suitable for process integration in manufacture of a photomask including a vacuum transfer chamber having coupled thereto at least one hard mask deposition chamber and at least one plasma chamber configured for etching chromium. In another embodiment, a method for process integration in manufacture of a photomask includes depositing a hard mask on a substrate in a first processing chamber, depositing a resist layer on the substrate, patterning the resist layer, etching the hard mask through apertures formed in the patterned resist layer in a second chamber; and etching a chromium layer through apertures formed in the hard mask in a third chamber.

The invention discloses a preparation method of functional hollow polymer microspheres. The shell of the functional hollow polymer microspheres is prepared by carrying out precipitation polymerization on a functional monomer and a crosslinking agent in different ratios; and the formed crosslinked shell has a mesoporous structure. The preparation method comprises the following steps: preparing a monodisperse polymer microsphere template by self-stabilization precipitation polymerization; directly adding the reaction system into the shell without separation to form the required functional monomer and crosslinking agent, and preparing core-shell polymer microspheres of which the shell has a crosslinked mesoporous structure by precipitation polymerization; and finally, removing the polymer microsphere core by solvent dissolution to obtain the functional hollow polymer microspheres. The technique is simple, and safe and convenient to operate, has the advantages of mild reaction conditions, no need of special equipment, high preparation efficiency, easy microsphere separation, controllable size, and very high functional group content in the polymer microspheres, and lays a foundation for large-scale industrial production of the functional hollow polymer microspheres.

The invention relates to a preparation method for carbon microspheres with high specific surface area. The preparation method includes the following steps: a carbon material, an alkaline activator, a binder and a solvent are mixed and stirred to obtain slurry, or the alkaline activator, the binder and the solvent are mixed and stirred to obtain slurry; all the materials are granulated to obtain primary carbon microspheres; the primary carbon microspheres go through activation, pickling, washing and drying to obtain the carbon microspheres with the high specific surface area. The preparation method provided by the invention adopts low-value carbonaceous waste materials or amorphous carbonaceous raw powders to prepare the microsphere carbon material with the high specific surface area, so as to meet the use requirements of multiple fields; the preparation technique is simple, the operation is convenient, and large-scale production is facilitated; the prepared carbon microspheres with the high specific surface area have an excellent spherical structure, a high degree of sphericity and a controllable particle size, and barely contain metal impurities.

The invention discloses a mineral polymer foaming material as well as a preparation method and an application of the mineral polymer foaming material. The material comprises the following ingredients in parts by weight: 50 to 100 parts of metakaolin, 0 to 50 parts of admixture, 50 to 100 parts of water glass, 0.1 to 15 parts of foaming agents, 0 to 10 parts of foam stabilizers and 10 to 90 parts of water. A physical foaming method is adopted, the foaming agents and the water are mixed to be made into foams, then, the foams are uniformly mixed with power materials adopting metakaolin powder as main structure materials, next, the water glass is added, the uniform stirring is carried out, the foaming material is manufactured through forming, and the air hole size and the product density of the foaming material are easy to control. The prepared mineral polymer foaming material has the advantages that the density is small, the air hole quantity is great, the tensile strength is higher than that of the common foaming material products, the water resistance is good, the fire resistance is good, and the resistance on high temperature of 1200 DEG C can be realized. The mineral polymer foaming material can be applied to the process fields of heat preservation and thermal insulation of buildings, heat preservation, filtering and adsorption of thermal equipment and the like.

The invention discloses an anisotropic etching method of graphite or grapheme, which is used for realizing crystal orientation of graphene, graphene cutting and patterning. The method comprises the following steps of: performing anisotropic etching on the surface of graphite or grapheme by adopting hydrogen-containing plasma, and forming a plurality of regular hexagonal holes on the surface of graphite or grapheme. All the hexagonal holes have the same orientation, the orientation is matched with the crystal orientation of graphene, etched edges have atomic scale smoothness, and all the edge structures are zigzag configurations. The invention overcomes the limitations existing in the traditional etching method of graphite or grapheme and realizes cutting and patterning graphene with controllable size and atomic scale smooth edges.

The invention relates to a preparing method of a transparent electrode based on a metal nanometer grid. The method comprises the following steps that (1) photoresist coats a silicon substrate in a spin-coating way and is baked; (2) exposure and development are carried out, and the photoresist is etched into a nanometer grid pattern on the silicon substrate; (3) a metal layer is deposited on the photoresist of the nanometer grid pattern; (4) the photoresist is removed through stripping, and a metal nanometer grid formed on the silicon substrate is obtained; (5) bonding agents coat the metal nanometer grid in a spin-coating way, and in addition, a transparent substrate is adhered and cured; (6) the silicon substrate is removed through corrosion, and the transparent electrode based on the metal nanometer grid arranged on the transparent substrate is obtained. The method is simple, the implementation is easy, the integration and the large-scale production are easily realized, and the electrical conductivity and the light transmittance of the prepared transparent electrode are controllable.

A cross linking maleic anhydride-vinyl acetate copolymer preparation method belongs to the field of copolymers. At present, the research on maleic anhydride-vinyl acetate copolymers mostly focuses on the polymerization research of linear polymers. The invention introduces a monomer, cross linking agents and initiators into medium to dissolve under the condition of nitrogen protection, and reacts for 2 to 24 hours under the temperature of 60 DEG C to 90 DEG C; the monomer is maleic anhydride Man and styrene St, the mol ratio is 1:1, and the mass concentration in the polymerization system is 5 percent to 45 percent; the initiators are organic peroxides or azo compounds, and are 0.05 percent to 1 percent of the total mass of the monomers; the cross linking agents are polyfunctionality alkene organic compounds, and are 0.08 percent to 8.8 percent of the total mass of the reactions system, and the rest is the alkyl ester of medium organic acid. The invention does not use surface active agents or stabilizers, can realize the adjustment and control of crosslinking polymer particle size, appearance and chemical physical properties through the adjustment of the addition amount of the cross linking agents.

This invention provides one supersonic phase control array test device, which comprises supersonic phase control array detector, supersonic trigger and receive board, main control board and computer, which comprises the following steps: the supersonic trigger and receive board first generates supersonic wave according to the parameter trigger; supersonic echo signal order is through array element switch circuit, signal amplification adjust circuit, A/D converter, digital echo data from control chip inner memory unit; under control board coordination, the echo data are through data to send high speed data transmission module to personal computer to get test result.

The invention relates to a direct graphene film transfer method. Currently, transferring graphene films from metal surfaces is quite inconvenient. The method includes: using the chemical vapor deposition method to grow a graphene film on a copper foil; using oxygen plasma cleaner to clear graphene on one side of the copper foil to obtain a combination of the single-layer graphene film with the copper foil; flatly attaching a transfer carrier onto the surface of the graphene film and drip adding an organic solvent of a proper quality to increase the interaction between the transfer carrier andthe graphene film; using etchant solution to clear the copper foil to obtain a combination of the single-layer graphene film with the transfer carrier; using deionized water to clean the graphene film for multiple times; and using a filter paper to clear the deionized water on the surface of the graphene film. Using the direct graphene film transfer method avoids the graphene films from being damaged by transfer media such as organic colloid and the like, single-layer graphene films of 100 micrometers or more can be obtained, simple equipment is required, product dimension is controllable, production safety is high, and industrial application is easy to implement.

The invention discloses a metal/grapheme nanocomposite and a preparation method thereof. The method comprises a photo-reduction one-step method and a photocatalytic reduction one-step method. The photo-reduction one-step method comprises the steps as follows: a grapheme oxide and metal complex acid or inorganic salt and a photo-reduction agent are mixed at the room temperature or under the condition of an ice-water bath, and under the light condition, organic negative hydrogen donors reduce metal ions and the grapheme oxide, so that a product is obtained. One approach of the photocatalytic reduction one-step method comprises the steps as follows: the grapheme oxide and the metal complex acid or salt are mixed in a DMF (dimethyl formamide) water solution containing a reducing agent, a metal ligand and a photocatalyst or in a water solution, catalysis is performed through the catalyst under the light condition, and at the same time, the reducing agent reduces the metal ions and the grapheme oxide, so that a product is obtained; and the other approach of the photocatalytic reduction one-step method comprises the steps as follows: the grapheme oxide and a metal organic complex are mixed in a DMF water solution containing the reducing agent and the photocatalyst or in a water solution, then catalysis is performed through the catalyst under the light condition, and the reducing agent reduces the metal organic complex and the grapheme oxide, so that a product is obtained.

The invention provides a preparing method of a multielement nanometer composite strengthening thermal-resisting aluminum matrix composite. The surface of nanocarbon is coated with a metal ion precursor in advance, the nanocarbon is evenly scattered in aluminum powder, the precursor is converted into oxide through thermal treatment, reactive sintering and densifying treatment are carried out on the obtained composite powder, and the multielement nanometer strengthening aluminum matrix composite is obtained. The nanocarbon has the high specific surface area, the feature size of the nanocarbon is far larger than that of the nanometer oxide, and therefore a proper amount of nanometer oxide can be loaded and evenly led into the aluminum powder, metallic oxide, carbide, an intermetallic compound and other multielement nanometer strengthening phases are generated through the in-situ reaction, and the tissue stability and the thermal resistance of the aluminum matrix composite are improved coordinately. The method achieves the purposes of even leading of high-volume-content multielement nanometer strengthening phases and the space occupation control, and the conventional powder metallurgy technology can be adopted for preparing the multielement nanometer composite strengthening thermal-resisting aluminum matrix composite.

Methods of fabricating a semiconductor device including a dual-hybrid liner in which an underlying silicide layer is protected from photoresist stripping chemicals by using a hard mask as a pattern during etching, rather than using a photoresist. The hard mask prevents exposure of a silicide layer to photoresist stripping chemicals and provides very good lateral dimension control such that the two nitride liners are well aligned.

The invention discloses sodium borosilicate glass doped with In2S3 quantum dots and a preparation method thereof. According to the sodium borosilicate glass doped with the In2S3 quantum dots, the In2S3 quantum dots are uniformly doped into sodium-borosilicate-based glass, and the sodium-borosilicate-based glass contains the following ingredients in percentage by mass: 5-15% of Na2O, 15-30% of B2O3 and 55-80% of SiO2; and the doped amount of the In2S3 quantum dots is 0.1-5.0% of the mass of the sodium-borosilicate-based glass. The sodium borosilicate glass doped with the In2S3 quantum dots is prepared in a manner that a sol-gel method is combined with atmosphere control, has excellent third-order nonlinear optical performance and heat stability, and has high light transmittance in visible-infrared regions, thereby being an important candidate material which is expected to produce high-speed full-light logic devices.

The invention discloses a macromolecular microcarrier and a preparation method thereof, belonging to the technical field of biomedicine. The preparation method comprises the following steps of: splitting a silk solution and a drug solution into micrometer grade liquid drops with core-shell structures under the action of a high-voltage electric field by adopting a coaxial high-voltage electrostatic technology and a freeze drying method; concreting through liquid nitrogen, and then preparing the microcarrier which is difficult to dissolve in water through freeze drying. The microcarrier is in the shape of a microsphere with the core-shell structure, and the diameter of the microsphere is 100-500 micrometers; the shell of the microcarrier comprises the components of silk fibroin; the random-coil conformation of silk fibroin molecules is 80-90 percent; the shell is in a porous structure, and an aperture is 5-20 micrometers; and a core of the microcarrier comprises the components of water-soluble drugs. The silk microcarrier has extensive application prospect in the fields of cell culture, drug release, and the like.

The invention discloses a preparation method of graphene on a diamond (111) surface, which mainly comprises the steps of: (1) growing an undoped diamond transition layer on a substrate: placing the substrate on a substrate support of a cavity of a hot filament chemical vapor deposition system, and growing a diamond transition layer; (2) growing a B-doped diamond film on the diamond transition layer; and (3) forming the grapheme through annealing and self-organization. By the preparation method, larger-size samples can be prepared, and the size is from nano scale to micron scale even millimeter scale. The method for preparing the graphene through self-organization, and is easier to realize; the grown grapheme has higher area controllability, can reach the micron scale or larger size which cannot be realized by most existing methods. In addition, the diamond has multiple excellent characteristics, and the boron-doped diamond substrate is not symmetrical, therefore, the graphene formed on the boron-doped diamond substrate can easily generate an energy gap, which is more beneficial to application of the graphene to devices.

The invention belongs to the technical field of photoelectric functional nano-materials, and particularly relates to a flexible transparent conductive oxide nanofiber membrane and a preparation method thereof. A precursor is composed of salt of a metallic oxide, salt of a doped element, an adhesive and a solvent, the precursor is sprayed on a substrate through electrospining equipment, and then high-temperature calcination is carried out to obtain the flexible transparent conductive oxide nanofiber membrane. The flexible transparent conductive oxide nanofiber membrane prepared with the method has flexibility, high conductivity and high visible-light permeability; no flexible substrate material is needed, and use of the flexible transparent conductive oxide nanofiber membrane is facilitated; the flexible transparent conductive oxide nanofiber membrane prepared with the electrostatic spinning method is controllable in size, high in repeatability, simple in process, high in efficiency and low in cost, and industrial preparation can be achieved.

The invention relates to a biological medical porous titanium material and a preparation method thereof. The preparation method, namely a method adopting powder metallurgy, is to add spherical particles of novel polymethyl methacrylate pore-forming agent to prepare a structure provided with a rough surface and three-dimensionally communicated open pores, wherein the number, the shape and the size of the pores can be controlled, namely, the porosity degree is less than 70vol. percent, the open porosity factor is more than 60 percent, the average pore diameter is less than 500 mums, the Young's modulus in compression is more than 0.3 GPa, the compressive strength is more than 40MPa, and the bending strength is more than 50MPa. The biological medical porous titanium material can be widely applied in the field of biological medical implants such as dental implants, artificial joints, spinal orthopaedic internal fixed systems, medullary internal nails and orthopaedic armor plates.