The preparation method comprises the following steps: selecting an
abrasive material base material, mixing the
abrasive material base material with a
silane coupling agent for
chemical modification,
coating the surface with a modified
abrasive material with a functional layer, adding the modified abrasive material into a stirring container, and dispersing to obtain the rough
polishing liquid applied to the
diamond substrate. An
oxidizing agent and a dispersing agent are added into the abrasive dispersion liquid to be stirred to form a
polishing solution, the
particle size distribution condition of the modified abrasive in the
polishing solution is monitored in real time through an online
particle size analyzer, and the ultrasonic power and the
treatment time are automatically adjusted; adding a pH
regulator into the polishing solution by adopting a step-by-step
titration method, and adjusting the pH value to 6-9; the polishing solution is filtered through a micro-
filtration membrane, undispersed particles and impurities are removed, and a polishing solution finished product is obtained; through the
chemical modification and ultrasonic-assisted technology and the real-time monitoring and automatic adjusting process, the
dispersity of the
grinding material and the uniformity of the polishing solution are remarkably improved, and the
particle size distribution of the
grinding material is optimized, so that the high-quality polishing solution is obtained.