The invention discloses a mixed
molten salt method for rapidly preparing short-range ordered
iridium oxide for PEM electrolyzed water, and belongs to the technical field of preparation of catalytic materials. According to the method, the short-range ordered
iridium oxide can be prepared within 20 minutes to 2 hours. High-melting-point mixed
molten salt is introduced as a reaction medium, so that
iridium salt is uniformly dispersed, agglomeration is effectively reduced, and the preparation efficiency is improved; a
morphology control template is not needed, the process is simplified, and the cost is reduced; by adjusting reaction parameters, the morphology and size of
iridium oxide can be flexibly regulated and controlled, the particle size of a single nano
crystal grain is 1.7-2.7 nm, and a short-range ordered structure is formed. The short-range ordered
iridium oxide provides more active sites, enhances the
structural stability, is good in
dispersity, can be directly used as catalyst
slurry, and realizes high catalytic activity under extremely low loading capacity; when the
composite material is applied to a
proton exchange membrane water
electrolysis hydrogen production
anode catalytic material, the catalyst cost is reduced, the
energy conversion efficiency is improved, an
electrolytic cell reaches
high current density under
low voltage, the performance is stable, and green
hydrogen economic development is promoted.