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264results about How to "Short regeneration time" patented technology

S-1 full-silicon molecular sieve and preparation method thereof as well as application of S-1 full-silicon molecular sieve in caprolactam preparation

The invention discloses an S-1 full-silicon molecular sieve and a preparation method thereof as well as application of the S-1 full-silicon molecular sieve in caprolactam preparation. The S-1 full-silicon molecular sieve is prepared by the method comprising the following steps: (1) synthesizing a tetrapropylammonium hydroxide template agent; and (2) synthesizing a molecular sieve: carrying out a reaction on tetrapropylammonium hydroxide liquor and tetraethoxysilane and ethanol, filtering, washing with deionized water, drying reaction liquid, roasting, so as to obtain molecular sieve raw powder; adding silica sol, polyethylene glycol 2000, and stronger ammonia water, sesbania powder and activated carbon powder in the molecular sieve raw powder, kneading in a kneader, then carrying out extrusion; roasting, immersing the roasted product in a NH3-NH3NO3 mixing solution and a hydrofluoric acid solution respectively, washing with deionized water, drying, roasting again so as to obtain the S-1 full-silicon molecular sieve. In the invention, the template agent is cheap; the conversion rate of the cyclohexanone and selectivity of the caprolactam are extremely high; a catalyst can be easily and fast regenerated; and the use of concentrated sulphuric acid is avoided, thus the S-1 full-silicon molecular sieve and the preparation method thereof are environment-friendly.
Owner:CHINA TIANCHEN ENG +1

In-situ regeneration method of ammonium sulfate poisoning denitration catalyst

The invention relates to an in-situ regeneration method of an ammonium sulfate poisoning denitration catalyst and belongs to the technical field of an industrial denitration catalyst. The in-situ regeneration method comprises the following steps: (1) when the concentration of nitrogen oxide in outlet flue gas of an SCR (Semiconductor Control Rectifier) main reactor is close to an emission limit value, switching the flue gas to an SCR reserved reactor; (2) introducing hot gas flow into the SCR main reactor and decomposing an ammonium sulfate layer deposited on the surface of the catalyst under the action of the hot gas flow; continuously introducing the hot gas flow for 1 hour to 8 hours to finish regeneration of the denitration catalyst; (3) switching the flue gas back to the SCR main reactor and continually carrying out a denitration reaction. Under the action of the hot gas flow, ammonium sulfate is decomposed into ammonia gas, sulfur trioxide and water steam and is removed along the flowing of the hot gas flow, so that the denitration performance of the catalyst can be recovered. The in-situ regeneration method of the ammonium sulfate poisoning denitration catalyst has the advantages of simplicity in operation, short regeneration time, low regeneration cost, safety and environmental friendliness, high denitration efficiency of the regenerated catalyst, and no changes of the strength and pore structure of the catalyst.
Owner:SOUTHWEST RES & DESIGN INST OF CHEM IND

Method and device for removing hydrogen sulfide in gas phase through oxidation

The invention discloses a method and a device for removing hydrogen sulfide in a gas phase through oxidation. The device comprises a settling tank, an extracting pump, a filtering membrane, an ultra gravity rotary packed bed, a separator, a balanced tank and a regeneration ultra gravity machine, wherein the extracting pump and the filtering membrane are sequentially connected between the settling tank and the ultra gravity rotary packed bed; the balanced tank is connected between the settling tank and the separator; the ultra gravity rotary packed bed is communicated with the balanced tank; the settling tank and the separator are sequentially connected with the extracting pump and the filtering membrane; and the extraction pump and the filtering membrane are sequentially connected between the settling tank and the regeneration ultra gravity machine. A technology flow of pre-oxidation sweetening, ultra oxidation sweetening, sulfur settlement, and regeneration is adopted for the method. According to the method and the device, the ultra gravity machine is adopted to replace the traditional low-mass-transfer-efficiency reactor, and the ultra gravity rotary packed bed reactor is adopted both in hydrogen sulfide oxidation and catalyst regeneration, the process mass transfer efficiency is intensified greatly, and the regeneration time oxidation sulfur removing time and the desulfurizing agent regenerating time are shortened.
Owner:WUHAN GLT ENERGY & ENVIRONMENTAL TECH CO LTD

Desulfurization and denitrification process utilizing microwave to intermittently irradiate activated carbon

Disclosed is a desulfurization and denitrification process utilizing microwave to intermittently irradiate activated carbon. Two or more adsorption beds filled with activated carbon particles are used for adsorbing or implementing microwave irradiation to flue gas of boilers alternatively. Flue gas is delivered into one of the adsorption beds by an induced draft fan, then the adsorption bed begins to run, and sulfur and nitric oxides in the flue gas are adsorbed by the activated carbon. After the activated carbon in the adsorption bed in running is saturated, the adsorption bed is in a regenerating state so as to be reused. The flue gas is delivered into the other adsorption bed beginning to run so as to be adsorbed, activated carbon particles of the regenerating adsorption bed are irradiated by microwave, sulfur and nitric oxides adsorbed on the surface of the activated carbon are quickly reduced and decomposed into elemental sulfur and nitrogen gas under high temperature, and the different adsorption beds are switched between the running state and the regenerating stage alternatively. Metal oxide is used as a reduction reaction catalyst so as to reduce reduction and decomposition temperature and loss of carbon. By the desulfurization and denitrification process, energy consumption of microwave irradiation can be reduced greatly, loss of carbon can be decreased, and in-situ regeneration of activated carbon is realized. In addition, the desulfurization and denitrification process has the advantages of fine desulfurization and denitrification effect, short time for regeneration of activated carbon, low cost for desulfurization and denitrification, high recovery rate, easiness in industrialized implementing and the like.
Owner:NORTH CHINA ELECTRIC POWER UNIV (BAODING)

Environmentally-friendly biomass compound rubber regenerant and preparation method thereof

ActiveCN102181160ARestore activityAlleviate the shortage trendNatural resinRubber material
The invention provides an environmentally-friendly biomass compound rubber regenerant. The regenerant is prepared from the following raw materials in mass percentage: 60-85% of bio-oil, 10-20% of natural resin and 5-30% of plant polyphenol. The preparation method of the regenerant comprises the following steps: (1) heating the bio-oil to 60-85 DEG C; (2) respectively adding the natural resins andthe plant polyphenol to the bio-oil and evenly mixing; and (3) naturally cooling the evenly mixed product to room temperature to finally obtain the environmentally-friendly biomass compound rubber regenerant product. In the invention, the bio-oil, the natural resins and the plant polyphenol which are extracted from plants are taken as raw materials, and the raw materials are renewable materials, which realizes maximum resource utilization and reduces dependence on petrochemical resource so as to achieve the purpose of green production of reclaimed rubber. The regenerant has the advantages of good rubber regeneration effect, high product quality, low production cost and no pollution and nuisance during the production process. The environmentally-friendly reclaimed rubber produced by the regenerant can be widely applied to various rubber products and can replace rubber materials, thus saving rubber resources.
Owner:KUNMING PHOENIX RUBBERS

Dust filtration system of mixed gas of high-temperature oil gas, water vapour and carbonaceous easy-precipitation substances

The invention discloses a dust filtration system of a mixed gas of high-temperature oil gas, water vapour and carbonaceous easy-precipitation substances. The system comprises a sealed separation chamber communicating a gas inlet pipe and a gas discharge pipe. A filtration mechanism is arranged in the sealed separation chamber. The outer surface of the filtration mechanism communicates with the gas inlet pipe, and the inner surface of the filtration mechanism communicates with the gas discharge pipe. A filtration body regeneration mechanism is arranged in the dust filtration system. According to the invention, the filtration body regeneration mechanism is arranged in the sealed separation chamber communicating the gas inlet pipe and the gas discharge pipe. When the filtration body works for a period of time, the filtration capacity of the filtration body cannot satisfy the requirement of normal working because the filtration capacity is greatly reduced due to tar and coal ash deposits on the surface and pores of the filtration body. The filtration body regeneration mechanism works, and the filtration body is recovered to a desired level. Regeneration is repeated, such that filtration body investment is directly reduced, and filtration body service life is greatly improved.
Owner:HENAN DRAGON INTO COAL TECH CO LTD

Microwave radiation reclaiming method for environment-friendly high-strength reclaimed rubber

The invention discloses a microwave radiation reclaiming method for environment-friendly high-strength reclaimed rubber, and belongs to the technical field of waste rubber reclaiming. The method comprises the following steps of: mixing waste rubber outer tire crown powder with the particle size of 20 meshes, rosin and dipentene according to a certain proportion; uniformly feeding the materials with a certain thickness on a roller way conveying device; determining the length of a roller way according to microwave radiation time; arranging a high-frequency microwave radiation device on the roller way; conveying the materials on the roller way for reclaiming the materials by microwave radiation during conveying; continuously putting the reclaimed rubber materials into a cooling device through the roller way; directly discharging the cooled materials to an open mill for performing refining, wherein the refining temperature is controlled to be 35-50 DEG C; and refining at low temperature on the open mill for 20 minutes to obtain a refined rubber sheet with smooth surface and uniform texture. A test result shows that the tensile strength of the reclaimed rubber is more than 18MPa, the breaking elongation is over 400%, and the Weigert plasticity is 0.35-0.45. The microwave radiation reclaiming method has the advantages of environment friendliness, short reclaiming time, low reclaiming temperature, energy conservation and high production efficiency.
Owner:XUZHOU COLLEGE OF INDAL TECH

Method for regenerating desalting mixed bed

The invention relates to the field of chemical water production in power plants, and discloses a method for regenerating a desalting mixed bed. In the method, the liquid level in a mixed bed tank reduces to the top of a resin layer before the resin layer is subjected to hydrodynamic backwashing layering, and compressed air is introduced into the mixed bed tank to perform air washing, so the resinis effectively loosened, the water injection pressure of the subsequent backwashing step is reduced, the backwashing layering effect is enhanced, the backwashing layering time is significantly shortened, and the consumption of backwashing water in the resin backwashing layering process is reduced. After the resin is backwashed with water, the control of the concentrations and the flow amounts of aregeneration alkali solution and a regeneration alkali solution can significantly reduce the consumptions of the regeneration alkali solution and the regeneration alkali solution in the resin regenerating process and greatly shortens the regeneration time of the desalting mixed bed. The water production volume of the desalting mixed bed in a single period is high, and the outlet water of the regenerated desalting mixed bed has excellent quality.
Owner:CHINA SHENHUA ENERGY CO LTD +2

Movable skid-mounted natural/coal bed gas adsorption and purification system with external medium heat exchange function

The invention relates to a movable skid-mounted natural/coal bed gas adsorption and purification system with an external medium heat exchange function, which comprises an adsorption tower system and a heat conduction medium heating circulation and cooling circulation system. The adsorption tower system consists of three adsorption towers which are connected in parallel and are switched to be started; one tower is used for adsorption, another tower is used for heating desorption and the third tower is used for cooling; in the heating desorption process, an adsorbent is heated by a high temperature heat conduction medium which is from external circulation so as to be rapidly heated and desorbed, and simultaneously, a small volume of purified process gas is used as regenerated gas to take away impurities generated in the desorption process; and in the cooling process, the adsorbent is cooled by a low temperature heat conduction medium which is from external circulation, so that the temperature of the adsorbent is rapidly reduced and the regeneration process is completed. Regeneration time of the adsorbent can be shortened; consumption of the regenerated gas is reduced; meanwhile, adsorption period is reduced and the heights of the adsorption towers are reduced; and the adsorption and purification system is miniaturized.
Owner:TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI +1

Method for regenerating saturated active carbon adsorbing organic matters through microwave activation of potassium persulfate

The invention relates to a method for regenerating saturated active carbon adsorbing organic matters through microwave activation of potassium persulfate. The method comprises the following steps of: adding a potassium persulfate solution into saturated active carbon; performing microwave irradiation for 5 to 30 minutes; cooling to room temperature; and filtering and cleaning to obtain regenerated carbon, wherein the mass ratio of the saturated active carbon to the potassium persulfate is (1-5):1. Compared with the traditional active carbon regeneration method, the method has the advantages that the regeneration cost is reduced and the regeneration efficiency is improved. Advanced oxidation and microwave irradiation of persulfate are organically combined, so the regeneration efficiency of the active carbon is improved. A chemical catalyst is not used, so new pollutants are not introduced. Due to the action of microwave, the oxidation time is short, the regeneration time is shortened, and the regeneration efficiency is improved and can reach about 80 percent. According to the method, regeneration can be performed for times, namely more than eight times, and the mass loss and the strength loss of the active carbon after regeneration are small.
Owner:DONGHUA UNIV

Active regeneration system and method for diesel engine particulate trap

The invention discloses an active regeneration system and a method for a diesel engine particulate trap. The active regeneration system comprises a high-frequency ceramic body, an electric heating wire, an oxygen pump electrolyte sheet, and an oxygen guide pipe, wherein the high-frequency ceramic body is filled between a filter body of the particle trap and an outer shell of the particle trap, theelectric heating wire is arranged in the high-frequency ceramic body in a penetrating mode, the oxygen pump electrolyte sheet is arranged in the electric heating wire in a penetrating mode, and the oxygen guide pipe is connected with an inlet chamber of the particle trap. One end of the oxygen pump electrolyte sheet penetrates through the oxygen guide pipe and is electrically connected with an oxygen pump power supply, and the electric heating wire is electrically connected with a heating power supply; the gas inlet end of the particle trap is connected with a tail gas inlet pipe, an oxygen sensor is arranged in the tail gas inlet pipe, and the gas outlet end of the particle trap is connected with a tail gas discharge pipe; and a differential pressure sensor is further arranged in the particle trap, and the heating power supply, the oxygen pump power supply, the oxygen sensor and the differential pressure sensor are electrically connected with a controller respectively. The active regeneration system and method for the diesel particulate trap improve the active regeneration efficiency of the diesel particulate trap.
Owner:JIANGSU UNIV

Device and method for regenerating waste rubber at normal pressure, medium temperature and low consumption

InactiveCN103205016ARecycling, environmental protection, energy saving and high efficiencyLow costChemical industryPlastic recyclingWaste rubberDrive motor
The invention relates to a device and a method for regenerating waste rubber at normal pressure, medium temperature and low consumption, and belongs to the field of reutilization of the waste rubber. The device comprises two parts, wherein the first part is a heating reaction kettle which comprises a tank body, a stirring paddle, a heater, a temperature sensor, a paddle driving motor, a first material inlet and a first material outlet; the second part is a cooler which comprises a cylinder body, a spiral, a cooling flow channel, a spiral driving motor, a second material inlet and a second material outlet; and the material outlet of the heating reaction kettle is connected with the material inlet of the cooler. The regeneration process flow which utilizes the device comprises the following steps of: simultaneously adding metered waste rubber, softening agents and activating agents to the heating reaction kettle; reacting at 160-250 DEG C for 15-40 minutes, and then opening a connecting valve to enter the cooler; conveying for 8-15 minutes through the spiral, and cooling materials to be lower than 80 DEG C. The device and method which are disclosed by the invention have the advantages of low manufacturing cost and environmental protection and energy saving in a production process, effectively solve the problem of wall adhesion of rubber powder in a regeneration process and are stable in product quality.
Owner:QINGWEI RUBBER SUQIAN +1

Novel ion exchange fiber and its application

The invention discloses a novel ion exchange fiber and its application. The ion exchange fiber is directly prepared by directly selecting raw materials having ion exchange functions without obtaining functional groups through a chemical treatment of grafting. The preparation method of the ion exchange fiber is simple, is in favor of the industrialized continuous production of products, and has a low economic cost. The ion exchange fiber prepared in the invention has the advantages of large exchange capacity, fast elution and adsorption speed, and the like. The filament diameter and the exchange capacity of the ion exchange fiber prepared in the invention are 5-100mum and 3.0-5.8mmol / g respectively. The matrix fiber of the ion exchange fiber has good comprehensive performances comprising good mechanical performances, high temperature resistance, acid and alkali resistance and the like. The preparation method of the novel ion exchange fiber comprises the following steps: mixing the raw materials comprising polystyrene (PS) and polyethylene (PE) with a compatilizer according to a certain weight ratio, adjusting an optimum spinning temperature, and carrying out melt spinning to prepare the base material of the ion exchange fiber; and carrying out chemical treatment of the base material to prepare the cation exchange fiber having sulfonic groups. The novel ion exchange fiber can be widely applied to the environmental protection field, the medicine and health field, the metallurgical filed, the water treatment field, the chemical adsorption field, the resource recovery field and the like.
Owner:冯淑芹

Electrothermic type diesel engine exhaust gas grain catcher

The invention provides an electrothermic type diesel engine exhaust gas grain catcher, which comprises a conductive central tube, corrugated sheet filter elements, hold-down strips, flat plate filter elements, insulating coatings, a conductive metal strip, an outer ring insulating layer and a metal shell. The flat plate filter elements with the same width are superposed on a lower layer of the corrugated sheet filter elements to form a filter element, the head end of the filter element is flat and level, and is superposed and welded with a bus of the conductive central tube; the tail end of the filter element is closely welded together with the conductive metal strip; two hold-down strips coated with the insulating coatings are welded on straight edges of two ends of the corrugated sheet filter elements respectively; the filter element is wound into a cylindrical filter element by taking the conductive central tube as an axis, and outer layer of the filter element is bound up with the outer ring insulating layer and then is placed in the metal shell; and the height of the hold-down strips is the same as that of the wave crests of the corrugated sheet filter elements. The electrothermic type diesel engine exhaust gas grain catcher integrates the functions of filtering and heating, and has the characteristics of high filtration rate, low exhaust back pressure, direct and overall energization and heating, small power consumption, short regeneration time and simple and reliable control.
Owner:广东新力金属有限公司
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