The invention discloses a method for rapidly analyzing
calcium and
magnesium in
iron ore. The method comprises the following steps: (1) weighing an
iron ore sample,
wetting with water, adding concentrated
hydrochloric acid, concentrated
nitric acid,
hydrofluoric acid and concentrated
sulfuric acid, heating for decomposing the sample, heating for evaporating till white
smoke nearly disappears, cooling, adding
hydrochloric acid, heating till a
solid is completely dissolved, taking down, cooling, transferring to a
volumetric flask, and supplementing to a constant volume with water; (2) moving a solution with the constant volume to a glass
beaker, diluting to a certain volume with water, adding
sodium potassium tartrate, L-
cysteine, a
potassium hydroxide solution and a mixture of a
calcium reagent and
potassium sulfate, titrating with an EDTA
standard solution to an end point, and calculating the content of the obtained
calcium; (3) moving the solution with the constant volume to the glass
beaker, diluting with water, adding the
sodium potassium tartrate, the L-
cysteine, an
ammonia water-
ammonium chloride buffer solution and neolan blue K-naphthol green B, and titrating with the EDTA
standard solution to an end point; (4) calculating the content of the obtained
magnesium by a subtraction method. The method is simple, convenient, fast and easy to master, and has relatively good practicality.