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Reagent and method for quickly testing content of ammonia and nitrogen in water sample

A rapid determination of ammonia nitrogen content technology, applied in the direction of material analysis through observation of the influence of chemical indicators, analysis through chemical reaction of materials, analysis using chemical indicators, etc., can solve cumbersome steps and long color development time , Operator requirements and other issues

Inactive Publication Date: 2014-02-19
山东益源环保科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The determination of ammonia nitrogen is one of the items that must be checked for environmental water quality. At present, the methods for determining ammonia nitrogen in China are mainly Nessler's reagent spectrophotometry, salicylic acid spectrophotometry, ion chromatography, etc. The steps are cumbersome and the color development time is long. The requirements for operators are high, and it can only be carried out in the laboratory, which is relatively limited

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] A reagent for rapid determination of ammonia nitrogen content in water samples, consisting of three packages: A, B, and C:

[0014] The raw materials of package A are 400g sodium salicylate, 400g sodium potassium tartrate and 10g sodium nitroferricyanide. Add the above reagents into a mortar, grind them thoroughly, and then pack them into 100mg / tubes, which is reagent A.

[0015] The raw material of package B is 100g sodium hydroxide, which is fixed to a volumetric flask of 1000ml, and divided into 10ml / bottle, which is B reagent.

[0016] C is packaged as a 10ml / bottle of sodium hypochlorite solution.

[0017] A method for rapid determination of ammonia nitrogen content in water samples. Open the lid of the small tube of A packaging, add 0.05ml of reagent B to the tube of packaging A, then add 2ml of the water sample to be tested and 0.05ml of reagent C in sequence, cover the lid and shake After uniformity, let it stand for 5 minutes (room temperature 25°C), observe t...

Embodiment 2

[0019] A reagent for rapid determination of ammonia nitrogen content in water samples, consisting of three packages: A, B, and C:

[0020] The raw materials of package A are 600g sodium salicylate, 600g sodium potassium tartrate and 20g sodium nitroferricyanide. Add the above reagents into a mortar, grind them thoroughly, and then pack them into 100mg / tubes, which is reagent A.

[0021] The raw material of the B package is 200g sodium hydroxide, which is fixed to a 1000ml volumetric flask, and divided into 10ml / bottle, which is the B reagent.

[0022] C is packaged as a 10ml / bottle of sodium hypochlorite solution.

[0023] A method for quickly determining the content of ammonia nitrogen in water samples. Open the cap of the small tube of package A, add 0.1ml of reagent B to the tube of package A, then add 4ml of the water sample to be tested and 0.1ml of reagent C in turn, cover and shake After uniformity, let it stand for 10 minutes (room temperature 25°C), observe the color...

Embodiment 3

[0025] A reagent for rapid determination of ammonia nitrogen content in water samples, consisting of three packages: A, B, and C:

[0026] The raw materials of package A are 500g sodium salicylate, 500g sodium potassium tartrate and 15g sodium nitroferricyanide. Add the above reagents into a mortar, grind them thoroughly, and then pack them into 100mg / tubes, which is reagent A.

[0027] The raw material of package B is 160g sodium hydroxide, which is fixed to a volumetric flask of 1000ml and subpackaged into 10ml / bottle, which is B reagent.

[0028] C package is 10ml / bottle of sodium hypochlorite.

[0029] A method for quickly determining the content of ammonia nitrogen in water samples. Open the lid of the small tube of A packaging, add 0.08ml of B reagent to the tube of A packaging, then add 3ml of the water sample to be tested and 0.7ml of C reagent in sequence, cover the lid and shake After uniformity, let it stand for 8 minutes (room temperature 25°C), observe the color ...

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PUM

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Abstract

The invention discloses a reagent for quickly testing the content of ammonia and nitrogen in a water sample. The reagent comprises three packages A, B and C, wherein the package A comprises the following raw materials: 400 g to 600 g sodium salicylate, 400 g to 600 g sodium potassium tartrate and 10 g to 20 g sodium nitroprusside, the reagent is added into a mortar to be fully ground and then is sub-packaged to be 100 mg per tube; the package B comprises the following raw materials: 100 g to 200 g sodium hydroxide, the volume of a volumetric flask is set to be 1000 ml, and the reagent is sub-packaged to be 10 ml per flask; the package C is a sodium hypochlorite solution of 10 ml per bottle. A method for quickly testing the content of ammonia and nitrogen in the water sample comprises the following steps: when the water sample is tested, adding 0.05-0.1 ml of the reagent B into a tube of the package A, adding 2-4 ml of the water sample to be tested and 0.05-0.1 ml of the reagent C in sequence, shaking well, standing at the room temperature of 25 DEG C for 5-10 minutes, observing the color change, and comparing with a standard color card to read out the ammonia and nitrogen concentration of the water sample to be tested.

Description

technical field [0001] The invention relates to an environmental monitoring reagent and method, in particular to a reagent and method capable of quickly measuring the content of ammonia nitrogen in water samples. Background technique [0002] The determination of ammonia nitrogen is one of the items that must be checked for environmental water quality. At present, the domestic methods for determining ammonia nitrogen are mainly Nessler's reagent spectrophotometry, salicylic acid spectrophotometry, ion chromatography, etc. The steps are cumbersome and the color development time is long. The operator has high requirements, and it can only be carried out in the laboratory, which is relatively limited. Contents of the invention [0003] The object of the present invention is to provide a fast, efficient and easy-to-operate reagent and method for quickly measuring the content of ammonia nitrogen in water samples. [0004] To achieve the above object, the technical solution ado...

Claims

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Application Information

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IPC IPC(8): G01N31/22G01N21/78
Inventor 张永顺黄现统徐海峰汤爱华
Owner 山东益源环保科技有限公司
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