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42 results about "Static light scattering" patented technology

Static light scattering is a technique in physical chemistry that measures the intensity of the scattered light to obtain the average molecular weight Mw of a macromolecule like a polymer or a protein in solution. Measurement of the scattering intensity at many angles allows calculation of the root mean square radius, also called the radius of gyration Rg. By measuring the scattering intensity for many samples of various concentrations, the second virial coefficient A₂, can be calculated.

Light scattering detector

The light scattering detector according to the present invention aims at simultaneously measuring the molecular weight and size of particles having varieties of diameters. This detector facilitates the measurement operation and knowing how particles associate or dissociate as time progresses. In this detector, the emitted light (static light scattering measurement light) having a first wavelength by the first light source and the emitted light (dynamic light scattering measurement light) having a second wavelength which is different from the first wavelength by the second light source are combined by a beam splitter 5 and coaxially directed onto the sample sell 10 to which a liquid sample S is supplied. While the irradiated area by the static light scattering measurement light is large, the irradiated area by the dynamic light scattering measurement light, which is coherent light, is narrow. Detectors 12 which selectively detect the first wavelength and detectors 13 which selectively detect the second wavelength are placed so as to encircle the sample cell 10. The detection signals by the detectors 11, 12 and the detection signals by the detectors 13 are separately mathematically-operated by a data processor 15 to calculate the molecule weight and size of the particles in the sample S.
Owner:SHIMADZU SEISAKUSHO CO LTD

Light scattering detector

InactiveUS20080285032A1Dynamic light scattering measurement result can be eliminatedEasy to operateScattering properties measurementsMonitoring particle agglomerationBeam splitterChemical physics
The light scattering detector according to the present invention aims at simultaneously measuring the molecular weight and size of particles having varieties of diameters. This detector facilitates the measurement operation and knowing how particles associate or dissociate as time progresses. In this detector, the emitted light (static light scattering measurement light) having a first wavelength by the first light source and the emitted light (dynamic light scattering measurement light) having a second wavelength which is different from the first wavelength by the second light source are combined by a beam splitter 5 and coaxially directed onto the sample sell 10 to which a liquid sample S is supplied. While the irradiated area by the static light scattering measurement light is large, the irradiated area by the dynamic light scattering measurement light, which is coherent light, is narrow. Detectors 12 which selectively detect the first wavelength and detectors 13 which selectively detect the second wavelength are placed so as to encircle the sample cell 10. The detection signals by the detectors 11, 12 and the detection signals by the detectors 13 are separately mathematically-operated by a data processor 15 to calculate the molecule weight and size of the particles in the sample S.
Owner:SHIMADZU CORP

Laser granularity measurement instrument with combination of dynamic and static light scattering

The invention relates to a laser particle size analyzer combining dynamic and static light scattering, which has a laser, a focusing lens, a sample pool, and a measuring optical path, wherein the measuring optical path is installed on a mechanical arm, and one end of the mechanical arm is connected to the outer edge of a rotating platform. The scattered light signal of the sample is received at different angles; the light emitted by the laser is directed to the sample pool through the focusing lens; the sample pool and the rotating platform are both circular, and the sample pool is set in the center of the rotating platform and does not rotate with the rotating platform. The invention installs the measurement optical path on the mechanical arm, and then drives the mechanical arm to rotate by controlling the rotating platform to realize the reception of scattered light signals at different angles, adopts dynamic light scattering to measure the particle size at a fixed angle, and continuously collects scattered signals at various angles when rotating. Scattering Mie theory to measure particle size, for wide distribution samples, both dynamic light scattering and static light scattering are used to measure, which greatly improves the measuring range and measurement accuracy of the instrument.
Owner:丹东百特仪器有限公司

Quick detection method for resonance light scattering of perfluorooctane sulfonate (PFOS) in environmental water sample

The invention discloses a quick detection method for resonance light scattering of perfluorooctane sulfonate (PFOS) in an environmental water sample, and relates to the field of environmental analysis. A resonance light scattering analysis method is adopted in the method. The method comprises the following steps of: sequentially adding 0.40mL of 4.2*10<-4>mol / L rhodamine 6G solution and 1.0mL of butadiene rubber (BR) buffer solution with pH of 3.29 into a 10mL color comparison tube, swirling the solution uniformly, and adding the pretreated water sample to be detected; after uniform swirling mixing, fixing the volume to 10mL by using 18.2Momega ultrapure water, and immediately performing synchronous scanning on a fluorescence spectrophotometer in lambda ex=lambda em, wherein both the excitation slit and the emission slit are 5 nanometers, and the voltage is 400V; recording the scattered spectrum in a wavelength range of 220 to 420 nanometers; and performing preliminary qualitative analysis and quantitative analysis on whether the environmental water sample contains the PFOS according to the scattered signals at the wavelength of 313 nanometers. If the water sample contains the PFOS, the scattering intensity at the wavelength of 313 nanometers is enhanced; otherwise, the scattered signals at the wavelength of 313 nanometers are not changed. The invention is characterized in that: the method for detecting the PFOS in the environmental water sample is simple, quick and sensitive, and low in detection cost.
Owner:SOUTHWEST UNIV

Light scattering-based monodisperse aerosol particle size and concentration measuring device

The invention provides a light scattering-based monodisperse aerosol particle size and concentration measuring device, and belongs to the technical field of measuring. According to the light scattering-based monodisperse aerosol particle size and concentration measuring device, light beam emitted by a laser passes through an optical attenuator, a beam expander, a first diaphragm, and a scattering cavity, and enters into a light trap; the upper wall and the lower wall of the scattering cavity are provided with a gas inlet pipe and a gas outlet pipe; a photosensitive area is formed via cross of the connection line of the gas inlet pipe and the gas outlet pipe with the light beam; a spherical mirror is arranged in the scattering cavity; and the focus of the spherical mirror and the center of the photosensitive area are superposed. The light scattering-based monodisperse aerosol particle size and concentration measuring device is capable of solving a technical problem that simultaneous rapid detection on particle size and concentration of high concentration monodisperse aerosol generated by standard aerosol generators can not be realize using conventional instrument. Beneficial effects are that, light scattering principles are adopted, particle counting method of pulse detection and spectrophotometric method of direct-current level detection are combined, rapid detection of the particle size and concentration of monodisperse aerosol can be realized without using filter membranes and destroying aerosol particles . The light scattering-based monodisperse aerosol particle size and concentration measuring device is used for providing means for calibration and source tracing of aerosol particle size and concentration detection-related instrument.
Owner:ZHEJIANG MEASUREMENT SCI RES INST

Method and device for measuring particulate matters by using dual wavelength polarized light scattering

The invention discloses a method and device for measuring particulate matters by using dual wavelength polarized light scattering. The method includes the following steps: 1) letting a to-be-measuredparticulate matter sample flow through a scattering cavity test area with a constant speed, and irradiating the test area after a laser is processed through polarization; 2) making an incident laser polarization state horizontally polarized, measuring the Stokes vector (S0, S1, S2, S3)<T> of scattered light at a specific angle after incident light is scattered by current particulate matters, calculating Hdop as a main index reflecting particulate matter morphology, calculating Pdop as a main index reflecting particulate matter absorption, and calculating Rdop as a main index reflecting particulate matter components; 3) making the incident laser polarization state being 45 DEG linear polarization, the rest operation being the same with the step 2); 4) making the incident laser polarizationstate being right-hand circular polarization, the rest operation being the same with the step 2); and 5) analyzing the integration attribute of the current particulate matters through an obtained index set. The method can realize on-line rapid comprehensive analysis on the integration attribute of particulate matters. In addition, the device can maximumly reduce the number of detectors.
Owner:SHENZHEN GRADUATE SCHOOL TSINGHUA UNIV

Device and method for detecting scattered light based on cooperation of ultrasonic modulation

The invention provides a device and method for detecting scattered light based on cooperation of ultrasonic modulation. The device comprises an ultrasonic excitation device, a laser scattering detection device, a motion platform, a sample table, a photodiode, a diode amplifier and a digital oscilloscope. After combination of the ultrasonic modulation technology with the laser scattering defect detection technology, ultrasonic modulation is carried out on the surface of a detected sample; with introduction of dynamic changes of defect characteristics in a moving state, a static light scatteringeffect of defects in the state is observed and analyzed; and the amplitude and phase changes of the scattered light intensity are analyzed to realize defect detection. According to the invention, ultrasonic modulation is added in scattering detection and two defect detection results are provided; and a visual defect distribution image is provided in a scanning manner. The device and method for detecting scattered light based on cooperation of ultrasonic modulation can be applied to defect detection of precision optical elements and are particularly suitable for finished product detection of ultra-precision optical elements with strict requirements on sub-surface defects.
Owner:ZHEJIANG UNIV

Reflective lens for ultrathin backlight module group

The invention discloses a reflective lens for an ultrathin backlight module group, and the reflective lens comprises a loading edge, a support column, a transmission cylinder, a central cylinder, a first light scattering groove, and a second light scattering groove. The lens is of a double-layer cylindrical surface structure. The lower surface of the lens is provided with a light source cavity, and the lower surface of the lens around the light source cavity is provided with the support column. A side edge of the lens is provided with the loading edge. The upper surface of the lens is providedwith the first light scattering groove, and the second light scattering groove is disposed below the first light scattering groove. The upper surface of the lens at an outer side of the first light scattering groove is provided with a light scattering and diffusion groove. The first light scattering groove, the second light scattering groove and the light scattering and diffusion groove enable the upper surface of the lens to be segmented into the central cylinder and the transmission cylinder. The central cylinder is located at the center of the transmission cylinder, and a central axis of the central cylinder is coaxial with the central axis of the transmission cylinder. The lens is large in light outgoing angle, is uniform in outgoing light, and reduces the thickness of the backlight module group.
Owner:ANHUI COREACH TECH

Hydrophobic associated polymer molecular weight distribution curve testing method

InactiveCN105203482ALow molecular weightCumulative percentage data is scarceColor/spectral properties measurementsPolymer scienceFiltration
The invention provides a hydrophobic associated polymer molecular weight distribution curve testing method. According to the method, hydrophobic association in a hydrophobic associated polymer solution is eliminated firstly under a proper solvent condition, polyelectrolyte effect is shielded, so that macromolecules are in a unimolecular dispersion state in a weak solution, then millipore filter membranes with different pore diameters are selected based on the membrane pore size separation principle, and a hydrophobic associated polymer is graded by means of a millipore filter membrane flow test device so that polymers with different molecular weights are separated; fitting of a percolate mass and filtration time relation curve is conducted with a quadratic equation so as to obtain the mass of a polymer solution in any grade, the concentration of the polymer solution in any grade is measured with the spectrophotometric method, and then the accumulated percentage composition of each grade is calculated. The molecular weight of the hydrophobic associated polymer in any grade is measured accurately with the static light scattering and viscosity method, and a molecular weight integral distribution curve or differential distribution curve is obtained according to the molecular weight of each grade and the accumulated percentage composition.
Owner:SOUTHWEST PETROLEUM UNIV

A subsurface defect detection device and method based on ultrasonic modulation

The invention provides a device and method for detecting scattered light based on cooperation of ultrasonic modulation. The device comprises an ultrasonic excitation device, a laser scattering detection device, a motion platform, a sample table, a photodiode, a diode amplifier and a digital oscilloscope. After combination of the ultrasonic modulation technology with the laser scattering defect detection technology, ultrasonic modulation is carried out on the surface of a detected sample; with introduction of dynamic changes of defect characteristics in a moving state, a static light scatteringeffect of defects in the state is observed and analyzed; and the amplitude and phase changes of the scattered light intensity are analyzed to realize defect detection. According to the invention, ultrasonic modulation is added in scattering detection and two defect detection results are provided; and a visual defect distribution image is provided in a scanning manner. The device and method for detecting scattered light based on cooperation of ultrasonic modulation can be applied to defect detection of precision optical elements and are particularly suitable for finished product detection of ultra-precision optical elements with strict requirements on sub-surface defects.
Owner:ZHEJIANG UNIV

Method for Determination of Molecular Weight Distribution Curve of Hydrophobically Associating Polymers

The invention provides a method for determining the molecular weight distribution curve of a hydrophobically associative polymer: firstly, under suitable solvent conditions, the hydrophobic association in a solution of the hydrophobically associative polymer is eliminated, the polyelectrolyte effect is shielded, and the macromolecules are dissolved in a dilute solution. Then, using the principle of membrane pore size separation, microporous membranes with different pore sizes were selected, and the hydrophobically associative polymers were classified by the microporous membrane flow experimental device to separate polymers with different molecular weights. Use quadratic equation to fit the relationship between filtrate mass and filtration time to obtain the mass of each fraction of polymer solution, measure the concentration of each fraction of polymer solution by spectrophotometry, and then calculate the cumulative percentage of each fraction . Combined with static light scattering and viscosity method, the molecular weight of each fraction of the hydrophobically associative polymer is accurately determined, and the molecular weight integral distribution curve or differential distribution curve is obtained according to the molecular weight and cumulative percentage of each fraction.
Owner:SOUTHWEST PETROLEUM UNIV
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