6088 results about "Aqueous solubility" patented technology

The invention discloses an oxygen-containing heterocyclic compound salt, and a crystal form and application thereof. The oxygen-containing heterocyclic compound salt disclosed by the invention has a structure as shown in a formula II. The oxygen-containing heterocyclic compound salt and the crystal form thereof provided by the invention have one or more improved characteristics, which are represented by extremely high water solubility, and high dissolution rate and high solubility in physiological related medium simulated gastrointestinal fluid, so that the stability of the oxygen-containing heterocyclic compound under an oxidation condition is remarkably improved, and the stability of the oxygen-containing heterocyclic compound is improved. Low hygroscopicity and good crystal form stability are achieved, and oral absorption and long-term storage of the medicine are facilitated; and the preparation method is simple and suitable for industrial production. # imgabs0 #

The invention relates to a ring structure betaine and double-tailed hydrophobic association polymer fracturing thickening agent and a preparation method thereof. The thickening agent is formed by copolymerization of four monomers, namely acrylamide, 2-allyl methylamino sodium ethanesulfonate, methyl diallyl sulfoethyl betaine and hydrophobic monomer double-tailed long-chain alkyl methyl allyl ammonium chloride. The preparation method comprises the following steps: firstly adding distilled water, then sequentially adding acrylamide, 2-allyl methylamino sodium ethanesulfonate, methyl diallyl sulfoethyl betaine and a hydrophobic monomer double-tailed long-chain alkyl methyl allyl ammonium chloride, adjusting the total concentration, introducing N2 to remove oxygen, adding an initiator, and reacting to prepare an AM / AMES / MDASBA / DCnMAAC quadripolymer, namely the polymer fracturing thickening agent. The thickening agent provided by the invention has good water solubility, and shows good salt resistance in mixed brine with the mineralization degree of greater than or equal to 30000 mg / L. The prepared linear solution and gel formed after crosslinking have high viscosity retention capacity at the temperature of 150 DEG C and the shearing rate of 170 s <-1 >, and the actual construction requirement for fracturing yield increase with the on-site mineralization degree larger than or equal to 30000 mg / L is met.

The invention provides a preparation method of lipidosome containing hair-growing active ingredients, and belongs to the technical field of hair-growing products. According to the invention, active substances are utilized to regulate hormone level, improve scalp blood circulation, stimulate anti-hair loss factors and promote hair growth in multiple directions, and lipidosome formed by lecithin and oil-soluble active ingredients as raw materials is utilized to integrally entrap the active substances, so that the anti-hair loss effect is improved. The defect of weak transdermal ability caused by large water solubility difference among the active substances is overcome, the stability and bioavailability of the active substances can be improved, and the hair growth and development effects of the prepared lipidosome containing the hair growth active components are remarkably improved.

The invention provides sulfonated cellulose. The sulfonated cellulose is obtained by etherifying alkalized cellulose with water-soluble halogenated sulfonate. Compared with the prior art, the sulfonated cellulose provided by the invention contains sulfonic acid groups, hydroxyl groups and other groups, so that when the sulfonated cellulose is used in the drilling fluid, the filter loss of the drilling fluid can be effectively controlled, and meanwhile, the salt pollution resistance, especially the calcium ion pollution resistance, of the drilling fluid can be improved; in addition, sulfonic groups in the product are also beneficial to improving the thermal stability of the drilling fluid, and the application range is expanded. In a word, compared with carboxymethyl cellulose for drilling fluid, sulfonated cellulose provided by the invention has obvious temperature resistance and high-valence metal ion resistance.

The invention relates to a sustained-release scale inhibiting product, its production and use. The scale inhibiting product comprises at least one scale inhibitor, a water soluble or hygroscopic carrier or binder, Activated Carbon for controlling the release rate of the at least one scale inhibitor and an adhesive that adheres the components of the composite.

The present application provides a method for recovering waste electrolyte of lithium-ion batteries, wherein the waste electrolyte contains lithium hexafluorophosphate, comprising the following steps: S1: adding a saline solution as an extractant to the collected waste electrolyte for extraction, separating a lower organic solution and an upper aqueous solution, and recovering the lower organic solution to obtain an organic solvent; S2: adding a water-soluble carbonate and / or a water-soluble phosphate to the upper aqueous solution in step S1, filtering, and separating to obtain a lithium precipitate. The recovery method can achieve efficient separation and recovery of organic solvents and lithium elements in waste electrolytes, is simple and easy to operate, is economical and environmentally friendly, has strong applicability, and can be prepared and produced on a large scale.

According to the stable organic silicon emulsion and the preparation method thereof provided by the invention, polyglycerol ricinoleate with different polymerization degrees, polydihydric alcohol oleate with different molecular weights and silicon polyether are introduced, so that the emulsifying capacity of the emulsion is improved, and the stability of the emulsion is improved; the polyglycerol ricinoleate serving as an emulsifier and a stabilizer can disperse water-soluble substances and oil-soluble substances, so that all the components are uniformly mixed, the emulsification is more sufficient, and the stability of the emulsion is improved; the emulsion enters the emulsification pump for emulsification under the condition of high rotating speed, so that the particle size of the emulsion is smaller, and the stability is better.

The invention discloses a preparation method and application of monatomic iron-doped carbon quantum dot nano enzyme, and the preparation method comprises the following steps: fully dispersing citric acid, urea and iron salt, and fully reacting in a closed container; the ferric salt is any one of ferric citrate, iron methionine or ferrous lactate. The monatomic iron-doped carbon quantum dot nano-enzyme provided by the invention is good in dispersity, excellent in water solubility and uniform and stable in structure, has efficient antioxidant enzyme activity, can be easily absorbed by plants, can remarkably improve the antioxidant capacity and stress resistance of the plants after being applied, can remove excessively accumulated active oxygen of the plants, and also can effectively inhibit the growth of the plants. The soil heavy metal pollution control agent can control soil heavy metal pollution, also can improve the removal efficiency of antioxidant enzymes in plants, reduce heavy metal absorption and increase the plant yield, has the characteristics of small dosage, low cost, high efficiency, high environmental safety and easy use, and provides a new technology and product choice with practical application value for treatment of soil heavy metal pollution.

The invention relates to a flexible aqueous binder for a lithium battery negative electrode and a preparation method thereof. The preparation method comprises the following steps: firstly, preparing a flexible polyurethane prepolymer containing vinyl by taking hydroxyl-terminated polybutadiene, isocyanate and hydroxyl acrylate as main raw materials; vinyl-containing compounds such as water-soluble acrylic acid (salt) or acrylamide, oil-soluble acrylic ester or acrylonitrile and the like are used as monomers and are combined with a flexible polyurethane prepolymer to prepare the negative water-based binder with flexible cross-linking points through free radical polymerization. The aqueous binder prepared by the technical method provided by the invention can realize point-to-point and point-to-line bonding modes with a pole piece active substance on a microstructure, so that the bonding strength of the active layer material and a copper foil is improved on the premise of not influencing the electrolyte resistance of the binder; and the flexibility of the negative pole piece and the subsequent processing stability are obviously improved.

The present application relates to the technical field of lithium battery materials and binders, and discloses an aqueous polymeric binder, a preparation method therefor and a use thereof. The aqueous polymeric binder is obtained by copolymerizing a polymerization unit comprising an acrylic monomer, an acrylate monomer, an oil-soluble monomer, a water-soluble monomer, and an amphiphilic water-soluble monomer in an aqueous solvent; and the mass percentages of the monomers are as follows: acrylic monomer: 5%-15%; acrylate monomer: 45%-60%; oil-soluble monomer: 10%-40%; water-soluble monomer: 5%-20%; and amphiphilic water-soluble monomer: 5%-10%. The aqueous polymeric binder of the present application is mainly used for bonding of an edge coating of a negative electrode sheet of a lithium-ion battery; on the basis of the specific copolymerization monomer components and proportions, the obtained binder has excellent PP base film bonding performance and electrolyte swelling resistance; in addition, the binder avoids material mixing with a negative electrode, and has good prospects of application.

The invention relates to a particulate composition comprising, or substantially consisting of, urea, an inhibitor, preferably a urease inhibitor and / or a nitrification inhibitor, and an additive, wherein the additive comprises components (i) and (ii): (i) a carboxylic acid or an anhydride, salt, or derivative thereof; preferably a carboxylic acid salt or a carboxylic acid derivative, more preferably a carboxylic acid salt; and (ii) a polar polymer; preferably a water-soluble polar polymer. The invention further relates to a process for preparing the particulate composition, an additive for a particulate composition, and the use of the particulate composition as a fertilizer.

The invention discloses pulsatilla saponin B4-oleanolic acid self-assembled nanoparticles as well as preparation and application thereof, and relates to the technical field of pharmaceutical preparations. Inspired by compatibility and solubilization of traditional Chinese medicines, the pulsatilla saponin B4-oleanolic acid self-assembled nanoparticles (AB4-OA NPs) are prepared by taking natural active components, namely micromolecular pulsatilla saponin B4 and oleanolic acid, as raw materials; the oleanolic acid has the effects of promoting dissolution and resisting inflammation, the water solubility of the oleanolic acid is improved, the bioavailability is improved, and the anti-inflammatory effect of the oleanolic acid is enhanced. Experimental results show that the AB4-OA NPs can effectively improve the dissolution rate of the oleanolic acid, so that the bioavailability of the oleanolic acid is effectively improved, meanwhile, the AB4-OA NPs has a better anti-inflammatory effect, and the effect is better than that of a single drug with the same dosage. In addition, the synthetic preparation method is simple and convenient, has the advantages of nano-scale drugs, realizes auxiliary-material-free pure drug self-delivery, and improves the delivery efficiency.

The invention provides an adenosine dihydroxysuccinate eutectic crystal and a preparation method and application thereof.In the adenosine dihydroxysuccinate eutectic crystal, the molar ratio of a dihydroxysuccinic acid molecule to an adenosine molecule is 1: (1-4), on the premise that the structure of adenosine is not changed, dihydroxysuccinic acid and adenosine are combined, the water solubility of adenosine is improved, and therefore the adenosine dihydroxysuccinate eutectic crystal is obtained. According to the preparation method, the adenosine which is difficult to dissolve in water is prepared into the water-soluble adenosine dihydroxysuccinate eutectic crystal, so that the water solubility of the adenosine dihydroxysuccinate eutectic crystal can reach 4%, the effects of the adenosine dihydroxysuccinate and the adenosine monomer are not damaged, and the adenosine dihydroxysuccinate and the adenosine monomer have a better synergistic effect; compared with a monomer and a simple mixture, the composition has better effects in the aspects of antibiosis, antioxidation, anti-aging, hair care, hair loss prevention and the like, and has a good application prospect in skin and hair care products.

The invention provides a nitrogen-doped biomass-based fluorescent carbon quantum dot, a preparation method and application, and relates to the technical field of carbon nanomaterials, the method comprises the following steps: mixing a biomass material and deionized water under an ultrasonic condition, adding a nitrogen source, and carrying out ultrasonic dispersion to obtain a uniformly dispersed to-be-reacted solution; reacting the to-be-reacted solution at a preset temperature for a preset time to obtain a mixed product solution; and filtering and dialyzing the mixed product solution to obtain the nitrogen-doped biomass-based fluorescent carbon quantum dot solution. The nitrogen-doped biomass-based fluorescent carbon quantum dot prepared by the method shows a stable fluorescent effect and good water solubility, the free radical clearance rate can reach 90% or above, and the antibacterial rate can reach 99% or above. The method can be used in the fields of drug sustained release, bioimaging and the like.

The invention belongs to the technical field of water-soluble polymer synthesis and drilling fluid application, and relates to a salt-resistant and high-temperature-resistant polymer micro-manganese dispersing agent as well as a preparation method and application thereof. The invention relates to a preparation method of a salt-resistant and high-temperature-resistant polymer micro-manganese dispersant. The preparation method comprises the following steps: dissolving a carboxylic acid-containing monomer and a sulfonic acid-containing monomer in deionized water; dropwise adding a first functional monomer and a second functional monomer, and then adjusting the pH to be neutral to obtain a mixed solution; introducing nitrogen and heating, adding an initiator aqueous solution after the mixed solution is heated to a preset temperature, and obtaining a polymer solution after the reaction is finished; and dropwise adding the polymer solution into a mixed solution of ethanol and acetone, and filtering to obtain the salt-resistant and high-temperature-resistant polymer micro-manganese dispersing agent. The salt-resistant and high-temperature-resistant polymer micro-manganese dispersing agent is small in dosage and good in effect, when 40% potassium formate water and the micro-manganese content are 36%, only 0.2 wt% of the dispersing agent is used, hot rolling can be conducted for 16 h at the temperature of 210 DEG C, and the viscosity reduction effect is kept to be 40% or above.

An oral pouch product includes a wrapper and a filling material. The wrapper defines a cavity. The filling material is in the cavity. The filling material includes a dry mixture and a liquid mixture. The dry mixture includes a cellulosic material and a water-soluble filler. The liquid mixture includes an oil and liquid nicotine. The oil includes a triglyceride, a diglyceride, a monoglyceride, or any combination thereof. The liquid nicotine is dissolved in the oil. The filling material is free of water or includes water in an amount less than or equal to 5 weight percent.

The invention relates to a water-soluble carbon chain substance for adjusting transmembrane transport and fluidity of a cell membrane, and preparation and application thereof. The water-soluble carbon chain substance comprises a carbon chain originally having certain water solubility, and the structure of the water-soluble carbon chain substance comprises at least one or more hydrophobic carbon chain parts and one or more hydrophilic groups or residues; the hydrophobic carbon chain part is coupled with water-soluble molecules to form a high-hydrophilicity compound; the water-soluble carbon chain can be used for preventing and treating infections including viruses, bacteria and fungi; anti-aging; the occurrence of neurodegenerative diseases such as Alzheimer's disease is prevented and reduced; by reducing the non-specific phagocytosis of the nano-drug by cells, the effect of the nano-drug on a target focus is enhanced.

The invention relates to the technical field of purification of organic chemicals, in particular to an aroma purification method of leaf alcohol. Comprising the following steps: preparing a methanesulfonic acid magnetic catalyst; esterification of leaf alcohol; and alcoholysis and fractionation of the esterification solution. According to the method, acetic acid is used for esterification of leaf alcohol, then clear water and a sodium carbonate solution are used for washing, the clear water can effectively remove some water-soluble impurities and acidic byproducts, and the sodium carbonate solution not only can neutralize residual acidic substances, but also can promote siloxane impurities in initial leaf alcohol to be hydrolyzed and then taken away by a water phase, so that the content of the siloxane impurities in the leaf alcohol is reduced; in the subsequent process of producing leaf alcohol through alcoholysis of the organic phase I, pure water and ethanol, silyl ether impurities are hydrolyzed in a high-temperature and strong-alkali environment, products are dissolved in waste liquid to be removed, olefine aldehyde impurities with the boiling point lower than that of leaf alcohol are removed through azeotropic fractionation with ethanol, in conclusion, the impurities in the finished product leaf alcohol can be effectively reduced, and the yield of the finished product leaf alcohol is increased. And the prepared finished product leaf alcohol is high in purity and pure in fragrance.

The invention relates to an anti-oxidation composition based on a reverse micelle synergistic technology and a preparation method and application thereof, the anti-oxidation composition comprises a reverse micelle structure and an aqueous solution containing an anti-oxidation active matter, and the reverse micelle structure wraps the aqueous solution containing the anti-oxidation active matter. The reverse micelle structure is used for wrapping the water-soluble antioxidant active matter, oxidation or degradation discoloration of the water-soluble antioxidant active matter is prevented, after the antioxidant active matter such as hydroxytyrosol, ergothioneine and dipotassium glycyrrhizinate is wrapped by the reverse micelle, the stability and the effect are remarkably improved, and after the reverse micelle wrapping, the effect of the antioxidant active matter is improved by 17% or above compared with an aqueous solution before wrapping.

Provided are a water-soluble film capable of maintaining good mechanical strength even when packaging a liquid detergent and the like while maintaining excellent water solubility of the water-soluble film and a package using the same. A water-soluble film of the present invention includes a polyvinyl alcohol resin. When a crystallinity index calculated for a first surface is Fd1 and a crystallinity index calculated for a second surface opposed to the first surface is Fd2 for FT-IR measurement of respective two surfaces of the water-soluble film by ATR technique using a diamond prism, the Fd1 and the Fd2 are 0.22≤Fd1≤0.72, 0.2≤Fd2≤0.65 and Fd1 / Fd2≥1.1.

The invention discloses a rapid hemostasis powder material for massive hemorrhage. The rapid hemostasis powder material for massive hemorrhage is tannic acid modified carboxymethyl chitosan. The invention also provides a preparation method and application of the rapid hemostasis powder material for massive hemorrhage, and a rapid hemostasis microgel composition containing the rapid hemostasis powder material for massive hemorrhage. The rapid hemostasis powder material and microgel composition for massive hemorrhage have excellent water solubility, hemostasis performance and biocompatibility, have multiple effects of sterilization, anti-inflammation, wound healing promotion and the like, and are beneficial to rapid healing of wound parts after hemostasis.

The invention discloses high-temperature and high-pressure filtrate reducer sulfonated asphalt for drilling fluid and a preparation method of the high-temperature and high-pressure filtrate reducer sulfonated asphalt, and belongs to the technical field of filtrate reducers. A comb-shaped side chain is introduced into a benzene ring of SEBS, the benzene ring is endowed with a comb-shaped structure, the structure strongly interacts with sulfonated asphalt, asphalt dispersion is optimized, agglomeration is avoided, 5-(2-hydroxyethyl) uracil is introduced, the oleophylic and hydrophilic characteristics are balanced, the acting force between asphalt particles is reduced, the reaction efficiency and uniformity of asphalt and fuming sulfuric acid are improved, and the sulfonated asphalt is prepared. The dispersant promotes uniform dispersion of asphalt, accelerates sulfonation reaction and improves sulfonated asphalt quality. The surface activity of the modified SEBS and the sulfonated asphalt form a net structure, so that the water solubility of the asphalt is enhanced, the drilling fluid is convenient to blend, the liquid surface tension is reduced, and the bubble formation condition is destroyed. A quaternary ammonium salt group is introduced, a well wall is stabilized by utilizing an opposite attraction principle, clay hydrophobicity is promoted, hydration and expansion are inhibited, and collapse is prevented. The modified sulfonated asphalt is resistant to temperature and pressure, good in filtration resistance and stable in filtration control at high temperature and high pressure.

The invention belongs to the field of nano material preparation, and particularly relates to a preparation method of nanoscale silicon dioxide alcohol-soluble sol. The method comprises the following steps: dissolving a water-soluble polymer in an ammonia water solution, and then adding absolute ethyl alcohol to form a polymer micelle; adding tetraethyl orthosilicate into the micelles, obtaining a nanoscale silicon dioxide nanoparticle mixed solution after the reaction is finished, then dispersing the nanoscale silicon dioxide nanoparticle mixed solution in deionized water through centrifugation, then centrifuging to obtain pure silicon dioxide particles, dispersing the pure silicon dioxide particles in absolute ethyl alcohol, adding a silane coupling agent KH570 at the same time, and performing ultrasonic dispersion to obtain the nanometer silicon dioxide nanoparticles. And carrying out ultrasonic dispersion to obtain the nanoscale silicon dioxide alcohol-soluble sol.

A method for producing a fluoroelastomer is provided by which a fluoropolymer having excellent dispersion stability in water can be efficiently produced using an aqueous medium having a reduced environmental burden and without essentially requiring an emulsifier.　The method for producing a fluoroelastomer comprises polymerizing monomers including TFE and PAVE in an aqueous dispersion that contains substantially no water-soluble emulsifier and comprises an aqueous medium and a first fluoropolymer, which includes TFE units and PAVE units, thereby producing a second fluoropolymer. In the first fluoropolymer, the proportion of the PAVE units to the sum of the TFE units and the PAVE units is 20-95 mol%. In the second fluoropolymer, the proportion of PAVE units to the sum of TFE units and the PAVE units is 20-95 mol%. Before initiation of the polymerization of the monomers, the content of the first fluoropolymer is 0.01-4.0 mass% with respect to the mass of the whole aqueous dispersion.

The invention belongs to the technical field of acyclic compounds, and particularly relates to a preparation method of tert-butyl peroxyisobutyrate. Stirring and cooling a solvent, a tert-butyl hydroperoxide aqueous solution and deionized water to obtain a mixed solution A; adding liquid caustic soda and a solid base catalyst into the mixed solution A under a stirring condition, and continuously stirring for reaction to obtain a mixed solution B; under the stirring condition, isobutyryl chloride and a water-soluble distributing agent are added into the mixed solution B, stirring reaction continues to be conducted, and a mixed solution C is obtained; standing and layering the mixed solution C, separating to obtain a tert-butyl peroxyisobutyrate crude product, and refining the tert-butyl peroxyisobutyrate crude product to obtain the tert-butyl peroxyisobutyrate. According to the method, the raw material utilization rate is increased, the reaction speed is increased, the reaction time is shortened, and the product yield is high.

The invention provides a photosensitive resin composition containing an anthracene methyl quaternary ammonium salt photosensitizer and application of the photosensitive resin composition, a structural main body anthracene ring of the photosensitizer is introduced into methylene substituted by a quaternary ammonium group at a position 10 and / or a position 9, and an acid radical or halogen is adopted as an equilibrium anion; compared with a commercially available anthracene photosensitizer, the photosensitizer has excellent fat solubility and good water solubility through introduction of the quaternary ammonium salt on the premise that the photobleaching property is retained, great potential is brought to formula design of the photosensitive composition, and development waste in a later development process can be greatly reduced; the method can be widely applied to the photo-curing fields of dry films, paints, coatings, printing ink, forming materials and the like.

The invention relates to the technical field of high-barrier environment-friendly packaging films, and discloses a high-barrier environment-friendly packaging film with an antibacterial function, the high-barrier environment-friendly packaging film comprises a base layer, a nano composite barrier layer, a bio-based functional layer and an outer protective layer from bottom to top in sequence, and the layers are tightly attached through a coated starch-based adhesive. According to the high-barrier environment-friendly packaging film with the antibacterial function, good biodegradability of polyhydroxyalkanoate adopted in the base layer film, polycaprolactone which is adopted in the nano-composite barrier layer film and has a biodegradable function and konjac glucomannan in the biological functional layer film are utilized; the composite packaging film can be decomposed into carbon dioxide and water by microorganisms in various environments, has excellent flexibility and processability, can adapt to different packaging requirements, provides basic flexibility, structural support and green and environment-friendly effects for the whole packaging film, and has a wide application prospect. The procyanidine arranged in the outer protective layer film provides stronger antibacterial property and water solubility for the whole packaging film.

The invention provides a nano imbibition displacement agent suitable for shale oil reservoirs and a preparation method thereof, and the nano imbibition displacement agent comprises the following raw materials in parts by weight: 30-50 parts of sulfonated graphene oxide, 10-15 parts of silane coupling agent modified nano silicon dioxide, 10-20 parts of water-soluble cellulose ether, 10-20 parts of fatty alcohol-polyoxyethylene ether, 5-8 parts of lower alcohol and 50-80 parts of water. Graphene oxide reacts with concentrated nitric acid to prepare acidified graphene oxide, then the acidified graphene oxide reacts with thionyl chloride to prepare acylating-chlorinated graphene oxide, and the acylating-chlorinated graphene oxide reacts with a sodium aminobenzene sulfonate derivative to prepare the graphene oxide. Electrostatic repulsive force is generated among graphene oxide particles through surface sulfonation treatment, the dispersing capacity among the particles is improved, agglomeration and flocculation among the particles are avoided, and the recovery efficiency is improved; sulfonated graphene oxide cooperates with a large-molecular-weight water-soluble cellulose ether surfactant, so that the temperature resistance and the salt resistance of the nano imbibition displacement agent can be remarkably improved.

The invention discloses biphase gel loaded with natural antioxidants as well as a preparation method and application of the biphase gel. The biphase gel is obtained by mixing oil gel and hydrogel in a mass ratio of (20: 80)-(80: 20) through a physical effect, wherein the hydrogel is composed of a water-soluble natural antioxidant and a polysaccharide aqueous solution; the oleogel is composed of an oleogel agent, a fat-soluble natural antioxidant, a small molecule emulsifier and edible oil. According to the present invention, the water-soluble nutrients are loaded in the hydrogel, and the fat-soluble nutrients are loaded in the oil gel to prepare different types of the two-phase gel nutrient delivery systems simultaneously loading the hydrophilic and hydrophobic natural antioxidants so as to effectively improve the steady-state protection effect and the bioavailability of the nutrients.