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2704results about "Foam dispersion/prevention" patented technology

A kind of water-soluble polyether modified silicone defoamer and its preparation and compounding method

InactiveCN102284198ASelf-emulsifying abilityGood dispersionInksCoatingsPresent methodEther
The invention relates to a water-soluble polyether modified silicone defoamer. The preparation method of the polyether-modified silicone defoamer comprises the following steps: firstly, adding terminal allyl polyoxyalkylene ether into a container for stirring, removing water; then adding solvent and low hydrogen-containing silicone oil into the above solution and stirring; then The catalyst is added to carry out stirring and heating reaction under N2 atmosphere and reflux condensation conditions; after the reaction is completed, the solvent and low boilers are removed to obtain the water-soluble polyether modified silicone. The invention also provides a compounding method of the water-soluble polyether modified silicone defoamer prepared by the above preparation method. The defoaming agent solves the problems that polysiloxanes are difficult to dissolve in water, have poor high temperature resistance and strong alkali resistance, and polyether defoaming agents have unsatisfactory defoaming speed and foam suppression time. The compounding method of water-soluble polyether-modified silicone defoamer solves the problems of incomplete emulsification of simethicone-type defoamer, demulsification when used, low temperature resistance and poor foam suppression ability.
Owner:黄山市强力化工有限公司

Method for preparing defoaming agent composition

The invention discloses a method for preparing a defoaming agent composition, belonging to the technical field of fine chemical preparation. The invention provides a defoaming agent composition widely used for removing harmful foams in industrial production. The defoaming agent composition comprises the following components: (1) polysiloxane RaSiO(4-a) / 2; (2) a coupling agent; (3) fine filler particles such as silicon dioxide and the like; (4) organic silicon resin; (5) polyether modified polysiloxane MDx(CH3GSiO)yM, wherein M is chain link R'2SiO1 / 2, D is chain link R'2SiO2 / 2, G is polyether radical-(CH2)z(EO)g(PO)hR'' and (6) an alkaline catalyst. The preparation method comprises the following steps: (1) heating the polysiloxane and the coupling agent together in a stirring machine, adding the alkaline catalyst to carry out a polymerization reaction at the temperature of 40-140 DEG C; (2) after crosslinking the mixture, adding the organic silicon resin and the polyether modified polysiloxane, carrying out a reaction again for 1-7 h at the temperature of 80-140 DEG C, and then adding the fine filler particles to mix uniformly, carrying out a reaction for 1-6 h at temperature of 90-180 DEG C; (3) after finishing the reaction, keeping the mixture for 0.1-1.5 h at the vacuum degree of -0.01 to -0.08 MPa, and finally, cooling to the room temperature to obtain white active materials that are defoaming agent compositions.
Owner:JIANGSU SIXIN SCI-TECH APPL RES INST CO LTD

Preparation method of high-viscosity organic silicon defoamer

InactiveCN104069654AIncrease the molecular chain lengthGood defoaming performanceFoam dispersion/preventionRoom temperatureOil phase
The invention discloses a preparation method of a high-viscosity organic silicon defoamer. The preparation method comprises the following steps of preparing a silicon grease by using organopolysiloxane, dewatering particles, catalysts and silicon resin under 180-240 DEG C, and stirring and uniformly mixing the silicon grease, polyether modified silicone oil and an emulsifying agent under 72-78 DEG C so as to obtain an oil phase mixture, dissolving a dispersing thickening agent in water; then adding a sodium hydroxide solution to uniformly stir to obtain emulsifying thickening water, adding the emulsifying thickening water into an oil-phase mixture, and carrying out emulsifying stir on the oil-phase mixture under 72-78 DEG C to obtain a coarse emulsifying object; and homogenizing the coarse emulsifying object under 50-55 DEG C to obtain a fine emulsifying object, adding residue water into the fine emulsifying object, stirring and uniformly mixing the fine emulsifying object under room temperature so as to obtain the high-viscosity organic silicon defoamer. The preparation method provided by the invention has the advantages that high-viscosity simethicone is utilized as an emulsifying main raw material, and thus, the obtained high-viscosity organic silicon defoamer has an ultra-strong defoaming speed and an anti-foam effect.
Owner:道尔达(西安)新材料有限公司
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