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Catalytic reaction method

A catalytic reaction and reaction technology, applied in the direction of chemical instruments and methods, chemical/physical/physical chemical mobile reactors, chemical/physical processes, etc., can solve the problem of rotating bed high gravity field device application has not yet been publicly reported, catalytic reaction Problems such as large equipment volume and low catalyst utilization rate can achieve the effect of reducing equipment volume, shortening residence time, and reducing equipment size

Inactive Publication Date: 2004-06-30
CHINA PETROLEUM & CHEM CORP +2
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Problems solved by technology

Due to the poor mass transfer effect, the diffusion problem in the constant gravity field has become the main factor hindering the smooth progress of the catalytic reaction.
In practical applications, the catalytic reaction under normal gravity field generally has the following disadvantages: 1. The amount of catalyst is large, and the utilization rate of the catalyst is low; 2. The mass transfer is slow; 3. The residence time of the material is long, the by-products are many, and the production efficiency is low; 4. , large energy consumption; 5, catalytic reaction equipment volume is large
For example, the application of the rotating bed supergravity field device in the catalytic reaction has not yet been published.

Method used

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Embodiment 1

[0032] C in a rotating bed reactor 4 The fractions are fully hydrogenated. C 4 The full hydrogenation of fractions is a gas-liquid-solid three-phase reaction, and the material used is H 2 、C 4 Distillate, its main components are: butane, butene, butadiene and butyne, the catalyst used is Pt / Al 2 o 3 or Pd / Al 2 o 3, Temperature: 10~180°C, Pressure: 2~40atm, Speed ​​400~1500rpm. C 4 Distillate space velocity 10~100hr -1 , hydrogen / unsaturated bond mol / mol (hydrogen / (butene+2×butadiene+2×butyne+3×vinylacetylene)): 1.0~1.2, the circulation ratio of raw material and product: 5~9: 1.

[0033] Such as figure 1 As shown, 30ml of catalyst is fixed on the rotor 2 of the rotary bed reactor, hydrogen is introduced into the reactor tangentially from the gas phase inlet 1, and the liquid phase C 4 The fraction is sprayed to the inner edge of the high-speed rotating catalyst layer by the liquid distributor 3, and the hydrogen and C 4 The distillate is strongly turbulent on the c...

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Abstract

The present invention discloses a catalytic reaction method. Said method can make the catalytic reaction be implemented in the supergravitational field. Said method utilizes the rotary bed supergravitational field equipment as reactor, on the rotor of said rotary bed supergravitational field equipment a porous catalyst layer and / or a porous filler layer are fixed, and the described catalytic reaction is homogeneous reaction or heterogeneous reaction. Said invention cal reduce catalyst consumption, raise utilization rate of catalyst, raise stability of catalyst and can reduce denergy consumption, etc.

Description

technical field [0001] The invention relates to a method for catalyzing a reaction, in particular to a method for carrying out a catalyzing reaction in a supergravity field. Background technique [0002] Catalytic reactions are widely used in chemical industry, petrochemical industry, biochemical industry and environmental engineering. Almost all catalytic reactions have the problem of internal and external diffusion, such as the diffusion between the reaction materials, the diffusion between the reaction materials and the catalyst, the diffusion between the product and the catalyst, etc. Due to the poor mass transfer effect, the diffusion problem in the constant gravity field has become the main factor hindering the smooth progress of the catalytic reaction. In practical applications, the catalytic reaction under normal gravity field generally has the following disadvantages: 1. The amount of catalyst is large, and the utilization rate of the catalyst is low; 2. The mass t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J8/10B01J19/28
Inventor 杨元一戴伟李振虎陈建锋郭锴郭奋
Owner CHINA PETROLEUM & CHEM CORP
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