1512 results about "Succinimide" patented technology

A lubricating oil composition for internal combustion engine, comprising a lubricating base oil; (A) a triphosphate represented by formula (1) below in an amount of 0.01 to 0.2 percent by mass in terms of phosphorus; (B) succinimide and/or derivative thereof in an amount of 0.01 to 0.3 percent by mass in terms of nitrogen; (C) an alkali metal or alkaline earth metal detergent in an amount of 0.05 to 1 percent by mass in terms of metal; and (D) a phenol-based and/or amine-based anti-oxidants in an amount of 0.01 to 3 percent by mass: O=P(OR<1>)3 (1) wherein the groups of R<1 >are each independently a hydrocarbon group having 1 to 30 carbon atoms and are the same or different from each other. The lubricating oil composition is excellent in anti-wear properties, base number retaining properties, high temperature detergency, and low friction characteristics.

The invention discloses a polysaccharide-dopamine composite biogel and application of the biogel. A preparation method of the biogel comprises the following steps: dissolving 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride and N-hydroxy succinimide sodium in an MES (Methyl Ester Sulfonate) buffer solution with a pH value being 5-6 in an inert gas atmosphere so as to prepare an EDC (ethylcarbodiimide) mixed solution, subsequently adding the EDC mixed solution into a polysaccharide solution for reacting at 20-30 DEG C for 0.5-1 hour, then adding a dopamine solution for further reacting at 20-30 DEG C for 1-4 hours, dialyzing a reactant by taking distilled water as a dialyzate, taking trapped fluid for freezing and drying to obtain the polysaccharide-dopamine composite biogel. The polysaccharide-dopamine composite biogel is simple and effective in modification method and capable of increasing the surface viscidity of the cartilage tissue, reducing loss of therapeutic drugs or implanted cells and facilitating the repairing of the cartilage injury.

The present invention provide a lubricant composition comprising a lubricant base oil, wherein said lubricant composition contains 0.08% by mass or less of zinc dithiophosphate or no zinc dithiophosphate as phosphorus amount for total amount of said lubricant composition, contacts metallic materials containing lead, and contains at least a kind of additive selected from a group consisting of following (A)˜(D): (A) organomolybdenum compounds (except molybdenum dithiophosphate); (B) borate ester and/or derivatives thereof; (C) organomolybdenum compounds, and borate ester and/or derivatives thereof; and (D) organomolybdenum compounds, and borated alkyl or alkenyl succinimide.

The present invention relates to an unleaded aminated aviation gasoline of high motor octane number (MON) and low toluene insoluble deposit formation containing an additive for controlling said deposits selected from the group consisting of high molecular weight hydrocarbyl amines, high molecular weight hydrocarbyl succinimide, high molecular weight hydrocarbyl substituted Mannish bases, and mixtures thereof, and optional carrier oil(s), to an additive concentrate for controlling toluene insoluble deposits, and to a method for producing the additive concentrate.

The invention discloses a preparation method of polydopamine modified alginic acid microspheres, which comprises the following steps of: under the protection of nitrogen, grafting dopamine to alginic acid by use of N-hydroxysuccinimide and 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride; polymerizing the synthesized dopamine modified alginic acid under the slight alkaline condition to obtain a polydopamine modified alginic acid solution; dropwise adding the polydopamine modified alginic acid solution into a CaCl2 solution by a syringe; and aging to obtain polydopamine modified alginic acid microspheres. The method disclosed by the invention is simple in process, and the prepared modified alginic acid microspheres have higher swelling resistance and good mechanical properties.

The present invention relates to an engine oil lubricant composition for use in internal combustion engines comprising one or more molybdenum containing compounds that deliver 1-1000 ppm molybdenum to the finished oil, one or more phosphorus containing compounds that deliver 25-650 ppm phosphorus to the finished oil, and one or more poly(meth)acrylate viscosity index improvers (VI improvers) that may or may not be functionalized, for improved fuel economy and turbocharger related deposits. In addition, the composition comprises an antioxidant system which is carefully balanced to provide improved fuel economy, comprising an aminic antioxidant, a phenolic antioxidant and an ashless dithiocarbamate. Additionally, the formulated oil may contain a dispersant poly(meth)acrylate, in addition to the PAMA VI improver, to reduce the amount of traditional succinimide dispersants.

A process is disclosed for producing with good productivity a cross-linked polyaspartic acid resin having biodegradability and high water absorbency. The process features inclusion of one of the following steps: (a) a polysuccinimide, which has been brought into a dispersed state by a dispersant, and a cross-linking agent are reacted to produce the cross-linked polyaspartic acid resin; (b) imide rings of a cross-linked polysuccinimide are subjected to a hydrolysis reaction while controlling a swelling degree of a resulting gel, whereby the cross-linked polyaspartic acid resin is produced; and (c) a gel of a cross-linked polysuccinimide, which has been obtained by reacting a cross-linking agent to a solution of a polysuccinimide in an organic solvent, is disintegrated to subject imide rings of the cross-linked polysuccinimide to a hydrolysis reaction, so that the cross-linked polyaspartic acid resin is produced. The process may also include one or both of the following steps as needed: (d) a gel of the cross-linked polyaspartic acid resin is washed with water and/or a water-miscible organic solvent; and (e) the polysuccinimide is produced using a basic amino acid as a cross-linking agent.

The present invention provides a lubricating oil composition with excellent torque capacity and shifting characteristics suitable for use as automatic or continuously variable transmission fluids, which composition comprises a base oil and, on the basis of the total mass of the composition, (A) a sulfonate detergent in an amount of 0.01 to 0.3 percent by mass in terms of metal (MeA); (B) a salicylate detergent in an amount of 0 or more than 0 and 0.1 percent by mass or less, in terms of metal (MeB); and (C) a boron-containing succinimide type ashless dispersant in an amount of 0.001 to 0.1 percent by mass in terms of boron (BoC); (MeB)/(MeA) being 0, or greater than 0 and 1.5 or less, and (MeA)/(BoC) being from 0.001 to 20.

The invention discloses a preparation method of a polyamide composite nanofiltration membrane, which comprises the following steps of partially hydrolyzing a polyacrylonitrile-based membrane under alkaline and heat treatment conditions, and activating the membrane in 1-ethyl-(3-dimethyl amino propyl) carbonyl diimine hydrochloride ethylene dichloride-hydrogen chloride (EDC-HCl) and N-hydroxyl succinimide (NHS); and then sequentially immersing the membrane in water phase monomer piperazine with low concentration and organic phase monomer benzenetricarbonyl trichloride, and the polyamide composite nanofiltration membrane is prepared by interfacial polymerization. The preparation method of the polyamide composite nanofiltration membrane has the advantages that compared with a traditional method, the method utilizes monomer solution with low concentration to perform the interfacial polymerization, high permeation flux can be obtained under ultra-low pressure (0.1MPa), and filter dye solution and saline solution have high separation selectivity.

The invention discloses a method for preparing a graphene oxide-chitosan composite material. The method includes the steps that a chitosan solution is prepared; secondly, a graphene oxide solution is prepared, a 1-ethyl-(3-dimethylaminopropyl)carbodiimide (EDC) solution is added into the graphene oxide solution during stirring, stirring reaction is conducted after dropwise addition, then an N-hydroxyl succinimide (NHS) solution is dropwise added into the graphene oxide solution, stirring reaction is conducted, and an activated hydroxyl graphene oxide solution is obtained; thirdly, the activated hydroxyl graphene oxide solution is dropwise added into the chitosan solution and stirred, the mixture is poured into a mould after being cooled to room temperature, and the cross-linked graphene oxide-chitosan composite material is obtained after freezing drying. The novel graphene oxide-chitosan composite material having an interface bonding function is provided, compared with non-cross-linked composite materials, mechanical properties of the composite material are greatly improved, and use of the composite material in the aspect of the bone induction technology is achieved.

A power transmission fluid composition, a power transmission containing the fluid, a method of operating a power transmission with the fluid and method of improving friction durability for a power transmission fluid. The power transmission fluid includes (a) a base oil and (b) an additive composition having therein (i) at least one ashless dispersant; (ii) a metal detergent providing greater than about 100 ppm metal in the power transmission fluid composition; (iii) a friction modifying amount of an imidazoline; (iv) a succinimide friction modifier; and (v) a non-hydroxy tertiary amine friction modifier other than (iii).

The invention relates to a fatty group polyester-polyamino acid copolymer with biology function and its synthesis method in the field of macromole biological medicine material technique. The block copolymer comprises: the two block copolymer (A) of fatty group polyester -polyamino acid with biology function and three block copolymer (B), and polyoxyethylene-fatty group polyester-polyamino acid three block copolymer (C). The synthesis method comprises: synthesizing the block copolymer of the carboxylic which is protected by benzyl, doing catalytic reduction to the palladium wood coal or hydrolyzing hydrogen bromide to generate the corresponding polymer with free carboxyl, then using NHS (N- hydroxyl succinimide-sauba) to active the flank carboxyl of the polyamino acid section, reacting it with short peptide, sugar or drug with RGD to obtain the fatty group polyester-polyamino acid copolymer with biology function.

An additive composition and lubricating fluid are disclosed that provide high steel-on-paper friction durability, good metal-metal extreme pressure performance characteristics and synchronizer performance. The lubricating fluid includes a base oil, a succinimide dispersant, a succinimide friction modifier, and a phosphonate. Also disclosed is a method for lubricating a dual clutch transmission employing a plurality of wet clutches, with the lubricating fluid of the disclosure.

The invention relates to the chemical field and particularly relates to a novel synthesis method for preparing a key intermediate 5-bromine-2-chlorine-4'-ethyoxyl diphenylmethane of a drug dapagliflozin for treating diabetes mellitus II. The preparation method comprises the following steps: enabling a starting raw material ortho-toluidine to firstly perform bromization and then perform chlorination after diazotization on a benzene ring with N-bromo-succinimide; then, in the presence of a halogenating agent, performing halogenating reaction of beta-position; and finally, performing Friedel-Crafts alkylation synthesis with phenetole, thereby obtaining the key intermediate. The preparation method is simple and convenient, economical and relatively high in reaction yield in each step, and suitable for industrial production.

The invention discloses an affinity chromatography medium employing tetrapeptide as a functional ligand and a preparation method of the affinity chromatography medium. The method comprises the following steps: adding dry matrix and allyl bromide to a dimethyl sulfoxide solution, activating, and reacting activating matrix with N-bromo succinimide; enabling bromo alcoholized matrix to react with hexamethylendiamine to obtain amino activating matrix; sequentially washing with deionized water, absolute ethyl alcohol and anhydrous N,N-dimethyl formamide, adding an N,N-dimethyl formamide solution containing tetrapeptide, 2-(7-azobenzotriazole)-N,N,N',N'-te-tramethyluronium hexafluorophosphate and N,N-diisopropylethylamine, and coupling a tetrapeptide ligand; and putting a medium coupled to tetrapeptide in a mixed liquid of sodium acetate and acetic anhydride to obtain the affinity chromatography medium employing tetrapeptide as the functional ligand. According to the novel chromatography medium developed by the method, a functional group is tetrapeptide composed of tyrosine, phenylalanine, arginine and histidine, and is designed on the basis of a protein A binding site of an antibody Fc segment; the antibody binding selectivity is greatly improved; and the affinity chromatography medium can be applied to efficient separation of an antibody.

This invention relates to a preparation method for poly-asparagic acid resin, which takes poly-pyrrolidine dione as the raw material to make crosslink poly-pyrrolidine dione with method of non-even phase suspended emulsion crosslink or non-even phase suspension crosslink and processes poly-asparagic acid resin by hydrolyzation characterizing that the crosslink poly-pyrrolidine dione is prepared by multi-section crosslink reaction, in which, the crosslinker is fed in for 2-4 times in equal volume and equal time interval, the crosslink poly-pyrrolidine dione and the resin are aged and crystallized and quickly dried, A ageing and crystallization process for 1-10 days under room temperature, B, quick drying process is carried out under -54-40deg.C.

The invention relates to an anti-tartar detersive for a quenching oil column of an ethylene unit. In order to solve the problems of the anti-tartar and cleaning of the quenching oil column, the invention provides the anti-tartar detersive for the quenching oil column. The anti-tartar detersive can inhibit the generation of dirt from the source; meanwhile, the detersive can also eliminate the generated dirt in the quenching oil column on line, thus providing necessary conditions for the long period operation of the ethylene unit. The anti-tartar detersive for the quenching oil column of the ethylene unit of the invention is characterized in that according to weight percentage, phenolic antioxidant is 1-18%, phosphorus metal ion deactivator is 8-20%, amine inhibitive substance is 5-35%, thiazolinyl succinimide dispersant is 2-18%, solvent is 30-70%; the substances are put into a container for heating, stirred and mixed evenly and cooled to room temperature, and then filtered to obtain the product.

A low-ash, low-phosphorus lubricant composition suitable for use in a stationary gas engine includes an oil of lubricating viscosity, 1.0 to 8 percent of a succinimide dispersant, 0.8 to 4.0 percent of a hindered, ester-substituted phenol antioxidant, and at least one metal or ammonium-containing sulfonate detergent or metal or ammonium-containing phenate detergent, in an amount which provides 0.1 to 3.0 percent by weight of said sulfonate or phenate moieties exclusive of the weight of the metal or ammonium moieties. The lubricant contains up to 0.08 percent by weight phosphorus and up to 0.2 percent sulfated ash.

A diesel fuel additive package, diesel fuel containing the additive and methods for operating an engine on the diesel fuel and additive. The fuel additive includes a reaction product of (a) a hydrocarbyl substituted dicarboxylic acid or anhydride, and (b) an amine compound or salt thereof of the formula

wherein R is selected from hydrogen and a hydrocarbyl group containing from about 1 to about 15 carbon atoms, and R¹ is selected from hydrogen and a hydrocarbyl group containing from about 1 to about 20 carbon atoms. The reaction product contains at least one amino triazole group. Component (2) of the additive is a hydrocarbyl succinimide dispersant. The additive also includes (3) a C₂ to C₁₀ alkyl alcohol; and (4) optionally, a lubricity additive. In the additive, a weight ratio of component (1) to component (2) in the fuel ranges from about 1:3 to about 1:5.

The invention relates to a bath solution preparing method and a low-concentration weakly alkaline cyanide-free copper plating which can ensure that the bonding force exists between a plating layer and a matrix, the plating solution has best stability, better dispersing capacity and deep plating capacity and simple process maintenance. The low-concentration weakly alkaline cyanide-free copper plating comprises a main salt, a conductive salt, a main complexing agent and a secondary complexing agent, wherein the main salt is copper chloride, the conductive salt comprises a mixture of sodium chloride, potassium chloride and ammonium chloride, the main complexing agent is a mixture of tartrate, citrate, nitrilotris(methylene)]tris-phosphonic acid salt, (1-Hydroxyethylidene)bis-phosphonic acid tetrasodium salt and ethylenediamine tetra(methylenephosphonic acid) salt; and the secondary complexing agent is a mixture of ortho-hydroxybenzoic acid, succinimide and derivatives thereof and dimethyl hydantoin. The invention has the advantages of capability of ensuring the bonding force of the plating and the matrix, best stability and better dispersing capacity and deep plating capacity and simple process maintenance.