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Method and apparatus for reclaiming oil from waste plastic

PCT No. PCT/JP97/00572 Sec. 371 Date Jan. 8, 1998 Sec. 102(e) Date Jan. 8, 1998 PCT Filed Feb. 27, 1997 PCT Pub. No. WO97/31990 PCT Pub. Date Sep. 4, 1997This invention provides a method for reclaiming oil from waste plastic in such a way that thermosetting resins and solid foreign matter in the plastic will not pose a problem. This method greatly reduces the burden of presorting the garbage or industrial waste. To achieve this objective when oil is to be reclaimed from a waste plastic containing chlorine compounds, such as vinyl chloride, the plastic must first be stripped of chlorine. Prior to pyrolysis, while being conveyed forward in a continuous stream, the plastic is mixed with heated sand and/or an additive agent to raise its temperature to 250-350 DEG C. This creates a product which is comprised of a mixture of sand and substantially dechlorinated plastic. The product is mixed with heated sand to heat it directly to a temperature of 350-500 DEG C. It is maintained at this temperature until pyrolysis occurs. In order to obtain high-quality oil with a low boiling point, a first gas/liquid separation process separates the product obtained from the aforesaid pyrolysis into liquid high-boiling point oil, gaseous low-boiling point oil and low molecular-weight gases, and recirculates the liquid high-boiling point oil to the pyrolysis process, and a second gas/liquid separation process separates the gaseous low-boiling point oil and low molecular-weight gases into liquid low-boiling point oil and low molecular-weight gases. The first and second gas/liquid separation process are connected in sequence.
Owner:MITSUBISHI HEAVY IND LTD

Organic working fluids

The present invention provides an improved, commercially available organic working fluid, which is operable under a broad range of temperatures, is thermally stable, has a high auto-ignition temperature, low freezing point and high critical temperature and is benign to the environment, and safe for human use. Such an organic working fluid is useful in organic Rankine cycle (ORC) power plants or units and other systems of the like; as an intermediate fluid for heat-recovery wherein heat from various heat sources is transferred using the intermediate fluid to a further working fluid and converted into work, and the intermediate fluid is also exploited to produce electricity. Such organic working fluids are also operable as heat transfer fluids either in ORC power plants or units or in other heat transfer systems. For this purpose the present invention presents a working fluid comprising at least one highly branched, heavy iso-paraffin hydrocarbons, or a mixture of two or more of such hydrocarbons. Preferably, at least one highly branched iso-paraffin hydrocarbon is present as the major component (i.e. at least 50% by volume) in the working fluid. A preferred sub-class of the class of the branched iso-paraffins which are suitable to be incorporated in organic working fluids of the present invention includes 8 to 20 carbon atom-containing hydrocarbons having at least one methyl radical (CH3) arranged to achieve a highly stable compound.
Owner:ORMAT TECH INC

Process for producing carboxylic acid

A process for producing a purified carboxylic acid having “n+1” carbon atoms comprises feeding a carboxylic acid stream containing a carboxylic acid having “n+1” carbon atoms, a hydrogen halide, a lower boiling point (bp) component, a higher bp component, and others to a first distillation column; separating a lower bp fraction containing part of the lower bp component and a higher bp fraction containing part of the higher bp component in the first column; withdrawing a side stream containing at least the carboxylic acid by side cut from the first column; feeding the side stream to a second distillation column; separating a lower bp fraction containing part of the lower bp component and a higher bp fraction containing part of the higher bp component in the second column; and withdrawing a side stream containing the carboxylic acid by side cut from the second column to recover a purified carboxylic acid; and the process further comprises feeding at least one first component (A) selected from the group consisting of an alcohol, corresponding to the carboxylic acid, having “n” carbon atom(s), and an ester of the alcohol with the carboxylic acid to the first column, and if necessary water. Such a process ensures reduction of the concentration of the hydrogen halide in the purified carboxylic acid.
Owner:DAICEL CHEM IND LTD

Fuel cell system with integrated fuel processor

InactiveUS20070122667A1MinimizesMaximize heat utilizationHydrogenOxygen/ozone/oxide/hydroxideBiodieselWater balance
A fuel cell system with fuel processor for integration with a marine vessel propulsion system. The system includes an auto thermal reactor that is the fuel processor for producing hydrogen from a fuel source. The fuel source is preferably ethanol or biodiesel or a mixture thereof, but can also be a sulfur containing fuel like petrodiesel of JP-8. The system further includes a gas-water shift reactor for further production and concentration of the hydrogen from the auto thermal reactor output. The system also includes a hydrogen permeable membrane separator for generating suitable quantities of essentially pure hydrogen to the fuel cell. The system also includes an oxygen permeable membrane separator for concentrating oxygen and reducing nitrogen to improve the partial pressure of hydrogen in subsequent fuel processing steps. The system contemplates the use of a Polymer Electrolyte Membrane (PEM) fuel cell. The system minimizes preheating of catalysts or other components to the extent just needed to initiate the fuel processor. To that end, heat sources and sinks of the system and associated usage systems are matched so as to minimize heat collection, storage and distribution systems. Water is recycled within the system to the extent necessary to maintain a water balance in the fuel processor and the fuel cell stack(s). The system includes cooling of the fuel cell stack(s) and integrated heat recovery with exothermic and endothermic catalysts. The fuel processor/fuel cell system components are configured to conform to and take advantage of the available space and limitations, such as the space constraints and opportunities associated with a marine vessel.
Owner:KELLEY RICHARD H

Method and apparatus for reclaiming oil from waste plastic

This invention provides a method for reclaiming oil from waste plastic in such a way that thermosetting resins and solid foreign matter in the plastic will not pose a problem. This method greatly reduces the burden of presorting the garbage or industrial waste. To achieve this objective when oil is to be reclaimed from a waste plastic containing chlorine compounds, such as vinyl chloride, the plastic must first be stripped of chlorine. Prior to pyrolysis, while being conveyed forward in a continuous stream, the plastic is mixed with heated sand and / or an additive agent to raise its temperature to 250-350° C. This creates a product which is comprised of a mixture of sand and substantially dechlorinated plastic. The product is mixed with heated sand to heat it directly to a temperature of 350-500° C. It is maintained at this temperature until pyrolysis occurs. In order to obtain high-quality oil with a low boiling point, a first gas / liquid separation process separates the product obtained from the aforesaid pyrolysis into liquid high-boiling point oil, gaseous low-boiling point oil and low molecular-weight gases, and recirculates the liquid high-boiling point oil to the pyrolysis process, and a second gas / liquid separation process separates the gaseous low-boiling point oil and low molecular-weight gases into liquid low-boiling point oil and low molecular-weight gases. The first and second gas / liquid separation process are connected in sequence.
Owner:MITSUBISHI HEAVY IND LTD
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