Diamond anvil cell high pressure in-situ measurement apparatus and method for thermoelectric materials

By designing a diamond anvil cell high-pressure in-situ measurement device, continuous measurement of multiple pressure values ​​of thermoelectric materials under vacuum conditions was achieved, solving the problem of low efficiency in existing technologies and improving experimental convenience and efficiency.

CN122409756APending Publication Date: 2026-07-17SOUTHERN UNIVERSITY OF SCIENCE AND TECHNOLOGY
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
SOUTHERN UNIVERSITY OF SCIENCE AND TECHNOLOGY
Filing Date
2026-04-01
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing in-situ measurement methods are inefficient in measuring the pressure of thermoelectric materials in a vacuum environment. They require frequent disassembly and reassembly of the vacuum chamber, which is time-consuming and labor-intensive, and it is difficult to achieve continuous measurement under multiple pressure values.

Method used

A diamond anvil cell high-pressure in-situ measurement device was designed. By setting an adjustment component on the vacuum chamber, the pressure inside the chamber can be controlled and adjusted. Combined with the pressurization component and the coolant flow channel, it ensures continuous measurement of multiple pressure values ​​of the sample under vacuum conditions.

Benefits of technology

It improves the convenience and efficiency of experimental operation, reduces repeated disassembly and assembly of the device, and enables stable measurement of sample parameters under multiple pressure values ​​under vacuum conditions, saving manpower and supporting in-depth research.

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Abstract

本申请公开了一种热电材料的金刚石对顶砧高压原位测量装置和方法。本申请实施方式的原位测量装置包括真空腔体和位于真空腔体内的加压组件,真空腔体上设有调节件;加压组件包括合围形成压腔的上压力件和下压力件、穿设于上压力件和下压力件的加压件以及位于压腔的对顶砧,上压力件和下压力件两者的至少其一与真空腔体固定连接,加压件与调节件连接;调节件设置为在外力作用下带动加压件拧紧或松开,以调节上压力件和下压力件通过对顶砧向样品施加的压力,如此,原位测量装置能够在真空条件下对压腔内的对顶砧和样品实现可控加压,解决了现有技术中,每次装配真空腔体一次只能测量一个压力值下的数据的局限,提高了操作便利性和工作效率。
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