Sample table clamp of X-ray diffractometer
By employing a combination of bosses and elastic sheets in the X-ray diffractometer, along with pull ropes and fine-tuning knobs, the problem of fragile glass slides is solved, achieving convenient and stable clamping and precise adjustment, adapting to glass slides of different thicknesses.
Patent Information
- Application Number
- CN202423136520.3
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-12-18
- Publication Date
- 2025-12-05
- Estimated Expiration
- 2034-12-18
AI Technical Summary
The clamps in existing X-ray diffractometers are prone to glass slide breakage due to the bolts being tightened, and the operation is inconvenient.
The system employs a combination of bosses and elastic plates for clamping, utilizing the deformation of the elastic plates and the assistance of pull ropes, along with a fine-tuning knob and ratchet mechanism, to achieve flexible clamping and precise adjustment of the glass slide.
It improves the ease of operation and stability of glass slide clamping, reduces the possibility of glass slide breakage, ensures that the clamping force is within a suitable range, and adapts to the needs of glass slides of different thicknesses.
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Figure CN223637422U_ABST
Abstract
Description
TECHNICAL FIELD
[0001] The present application relates to the field of optical detection equipment, in particular to a sample stage clamp of an X-ray diffractometer. BACKGROUND
[0002] X-ray diffraction utilizes the diffraction phenomenon of X-rays in crystals to obtain the characteristics of the X-ray signal after diffraction, and obtains the diffraction pattern after processing. By performing X-ray diffraction on a material, analyzing the diffraction pattern, and obtaining information such as the composition of the material, the structure or morphology of the atoms or molecules inside the material, etc.
[0003] The X-ray diffractometer is such that the X-ray beam is irradiated on the sample through the soller slit, the divergence slit, the sample stage is located at the center of the goniometer, based on the reflection geometry θs-θd, the X-ray beam occurs diffraction phenomenon in a specific direction when the Bragg's law is satisfied, and finally the collected diffraction pattern is displayed on the analysis software through the data processing system after passing through the anti-scattering slit, the soller slit, the receiving slit and the X-ray detector.
[0004] The traditional diffractometer includes an internal hollow body, a sample stage, an X-ray generator and a detector arranged in the body, and a clamp for clamping a slide, and the detection sample is placed on the slide.
[0005] The existing clamp mostly adopts bolt clamping, but the tightening of the bolt is usually realized manually by workers, and the thickness of the slide is thin and fragile, so the slide is easily broken when the worker tightens it too hard, and the detection sample will also scatter in the body, which has obvious defects. CONTENT OF THE INVENTION
[0006] In order to improve the problem that the slide may be broken due to excessive force when clamping the slide, the present application provides a sample stage clamp of an X-ray diffractometer.
[0007] The sample stage clamp of the X-ray diffractometer provided by the present application adopts the following technical scheme:
[0008] The sample stage clamp of the X-ray diffractometer includes a boss arranged on the inner side wall of the body, and a resilient sheet arranged below the boss in the body, one end of the resilient sheet is used to clamp the slide against the lower surface of the boss, and the other end is arranged on the inner side wall of the body.
[0009] By adopting the above technical scheme, when installing, the worker manually bends the resilient sheet downward, and then inserts the slide between the resilient sheet and the boss. After releasing the resilient sheet, the resilient sheet restores the deformation, so as to clamp the slide against the boss. The boss and the resilient sheet cooperate to clamp the slide, the clamping process is convenient, and the clamping force of the resilient sheet on the slide remains constant, which reduces the possibility of damage of the slide due to excessive force.
[0010] Optionally, the elastic sheet is attached with an elastic layer at the position for abutting against the slide glass.
[0011] By adopting the technical scheme, the elastic layer changes the rigid contact between the elastic sheet and the slide glass into flexible contact, thereby protecting the slide glass.
[0012] Optionally, one end of the elastic sheet is attached with a pull rope relative to the slide glass, and the bottom end of the pull rope is attached with a pull head.
[0013] By adopting the technical scheme, the worker can conveniently deform the elastic sheet through the pull rope.
[0014] Optionally, the pull rope is an elastic rope.
[0015] By adopting the technical scheme, since the pull rope itself has elasticity, the deformation degree of the elastic sheet when the worker pulls the pull rope is reduced, thereby reducing the impact of the elastic sheet on the slide glass.
[0016] Optionally, a vertical slide rail strip is arranged on the inner wall of the machine body, a lifting block is slidably arranged on the slide rail strip, the cross sections of the slide rail strip and the lifting block in sliding fit are dovetail-shaped, the elastic sheet is bolted to the lifting block, and a fastening bolt for abutting against the slide rail strip is threadedly connected to the lifting block.
[0017] By adopting the technical scheme, when the thickness of the slide glass to be abutted against changes, the worker adjusts the height of the lifting block and locks the height of the lifting block through the fastening bolt, and then re-adjusts the abutting force of the elastic sheet on the slide glass to a proper size.
[0018] Optionally, polytetrafluoroethylene is coated on the lifting block and the slide rail strip.
[0019] By adopting the technical scheme, the friction coefficient of the polytetrafluoroethylene is small, thereby improving the smoothness of the lifting block in the lifting movement on the slide rail strip.
[0020] Optionally, a fixing block is arranged on the inner wall of the machine body relative to the position below the lifting block, a vertical jack is threadedly connected to the fixing block, the top end of the jack is supported on the bottom of the lifting block, a hollow micro-adjustment knob is rotatably sleeved on the bottom end of the jack, a first ratchet wheel is arranged on the bottom end of the jack, a second ratchet wheel is connected to the inner end face of the micro-adjustment knob away from the lifting block through a compression spring, and the first ratchet wheel is engaged with the second ratchet wheel.
[0021] By adopting the technical scheme, when the pressing height of the elastic sheet is adjusted, the worker first rotates the jacking rod, so that the elastic sheet quickly approaches the boss. After approaching the boss, the fine adjustment knob is rotated, the second ratchet wheel drives the first ratchet wheel to rotate synchronously, the jacking rod rotates and gradually rises, until the elastic sheet presses the glass sheet on the boss, the first ratchet wheel remains stationary, and the second ratchet wheel continues to rotate. At this time, the first ratchet wheel collides with the second ratchet wheel, and the worker will hear the sound of "click, click". At this time, the height of the elastic sheet is adjusted to the right position, and the pressing force is appropriate. The worker manually tightens the fastening bolt.
[0022] Optionally, the outer side wall of the fine adjustment knob is provided with anti-skid lines.
[0023] By adopting the technical scheme, the anti-skid lines can reduce the possibility of slipping when the worker manually rotates the fine adjustment knob.
[0024] In summary, the present application has at least one of the following beneficial technical effects:
[0025] 1. When installing, the worker manually bends the elastic sheet downward, and then inserts the glass sheet between the elastic sheet and the boss. After releasing the elastic sheet, the elastic sheet restores the deformation, so as to press the glass sheet on the boss. In this way, the boss cooperates with the elastic sheet to realize clamping of the glass sheet. The clamping process is convenient to operate, and the pressing force of the elastic sheet on the glass sheet remains constant, reducing the possibility of damage to the glass sheet due to excessive force.
[0026] 2. When the thickness of the pressed glass sheet changes, the worker adjusts the height of the lifting block and locks the height of the lifting block through the fastening bolt, so as to re-adjust the pressing force of the elastic sheet on the glass sheet to an appropriate size.
[0027] 3. When the pressing height of the elastic sheet is adjusted, the worker first rotates the jacking rod, so that the elastic sheet quickly approaches the boss. After approaching the boss, the fine adjustment knob is rotated, the second ratchet wheel drives the first ratchet wheel to rotate synchronously, the jacking rod rotates and gradually rises, until the elastic sheet presses the glass sheet on the boss, the first ratchet wheel remains stationary, and the second ratchet wheel continues to rotate. At this time, the first ratchet wheel collides with the second ratchet wheel, and the worker will hear the sound of "click, click". At this time, the height of the elastic sheet is adjusted to the right position, and the pressing force is appropriate. The worker manually tightens the fastening bolt. BRIEF DESCRIPTION OF DRAWINGS
[0028] Figure 1 is a schematic view of an embodiment of the present application.
[0029] Figure 2 is a sectional view of an embodiment of the present application.
[0030] Figure 3 is Figure 2 is an enlarged view of part A in
[0031] Explanation of reference signs: 1, machine body; 2, boss; 3, elastic sheet; 5, pull rope; 6, pull head; 7, sliding rail strip; 8, lifting block; 9, fastening bolt; 10, fixed block; 11, jacking rod; 12, fine adjustment knob; 13, first ratchet wheel; 14, second ratchet wheel; 15, compression spring; 16, anti-skid pattern. DETAILED DESCRIPTION
[0032] The following will be described in detail with reference to the accompanying drawings. Figures 1-3 The present application is further described in detail.
[0033] The present application discloses a sample stage clamp of an X-ray diffractometer.
[0034] Reference Figure 1 and Figure 2 The sample stage clamp of the X-ray diffractometer comprises a boss 2 arranged on the inner side wall of a machine body 1, a vertical sliding rail strip 7 is bolted to the position below the boss 2, a lifting block 8 is slid on the sliding rail strip 7, and the cross sections of the sliding rail strip 7 and the lifting block 8 at the sliding fit position are dovetail-shaped.
[0035] Reference Figure 1 and Figure 2 The lifting block 8 and the sliding rail strip 7 are coated with polytetrafluoroethylene, the lifting block 8 is threadedly connected with a fastening bolt 9 for abutting against the sliding rail strip 7, and the fastening bolt 9 is a goat horn bolt in the prior art, which is convenient for workers to manually tighten and loosen.
[0036] Reference Figure 2 The lifting block 8 is bolted with an elastic sheet 3, one end of the elastic sheet 3 away from the lifting block 8 is used to abut a glass sheet against the bottom of the boss 2, and an elastic layer (not shown in the figure) is bonded to the position of the elastic sheet 3 for abutting against the glass sheet, and the elastic layer is made of rubber in the prior art and has soft texture.
[0037] Reference Figure 2 One end of the elastic sheet 3 relative to the glass sheet is bonded with a pull rope 5, the pull rope 5 is made of elastic rope, and the bottom end of the pull rope 5 is bonded with a pull head 6.
[0038] During installation, the worker manually pulls down the pull rope 5, the pull rope 5 is stretched in the process, at the same time, the elastic sheet 3 is bent and deformed downward, and then the end of the glass sheet is inserted between the elastic sheet 3 and the boss 2.
[0039] The worker slowly loosens the pull rope 5, and the elastic sheet 3 gradually recovers the deformation, so that the elastic sheet 3 abuts the glass sheet against the bottom of the boss 2.
[0040] Reference Figure 2 The inner wall of the machine body 1 is bolted with a fixed block 10 below the lifting block 8, a vertical jacking rod 11 is threadedly connected to the fixed block 10, and the top end of the jacking rod 11 supports the bottom of the lifting block.
[0041] Referring to Figure 2 and Figure 3 The bottom end of the top rod 11 is sleeved with a fine adjustment knob 12, the inside of the fine adjustment knob 12 is hollow, the outside wall of the fine adjustment knob 12 is provided with anti-skid lines 16, and the bottom end of the top rod 11 is coaxially integrally formed with a first ratchet wheel 13. The inside of the fine adjustment knob 12 away from the inner end face of the lifting block 8 is bonded with a second ratchet wheel 14 through a compression spring 15, and the first ratchet wheel 13 is engaged with the second ratchet wheel 14.
[0042] Referring to Figure 2 and Figure 3 When the abutting height of the elastic sheet 3 is adjusted, the worker first rotates the top rod 11, so that the elastic sheet 3 quickly approaches the boss 2, so as to realize preliminary coarse adjustment.
[0043] After approaching the boss 2, the worker manually rotates the fine adjustment knob 12, the second ratchet wheel 14 drives the first ratchet wheel 13 to rotate synchronously, the top rod 11 rotates and gradually rises, until the elastic sheet 3 abuts the glass sheet on the boss 2, the first ratchet wheel 13 remains stationary, and the second ratchet wheel 14 continues to rotate.
[0044] At this time, the first ratchet wheel 13 collides with the second ratchet wheel 14, and the worker will hear “click, click” sound, at this time, the height of the elastic sheet 3 is adjusted in place, and the abutting force is appropriate, so as to realize the secondary fine adjustment of the abutting height of the elastic sheet 3.
[0045] When the thickness of the glass sheet changes, the worker can accurately adjust the abutting height of the elastic sheet 3 through the above structure, and the abutting force can always be kept in the appropriate force range, and the flexibility is high.
[0046] The implementation principle of the X-ray diffractometer sample table clamp in the embodiment of the application is as follows:
[0047] When installing, the worker manually deforms the elastic sheet 3 downward through the pull rope 5, and then inserts the glass sheet between the elastic sheet 3 and the boss 2. After the elastic sheet 3 is loosened, the elastic sheet 3 restores the deformation, so as to abut the glass sheet on the boss 2, and the boss 2 and the elastic sheet 3 cooperate to realize clamping of the glass sheet.
[0048] When the abutting height of the elastic sheet 3 is adjusted, the worker first rotates the top rod 11, so that the elastic sheet 3 quickly approaches the boss 2, so as to realize preliminary coarse adjustment. After approaching the boss 2, the worker manually rotates the fine adjustment knob 12, the second ratchet wheel 14 drives the first ratchet wheel 13 to rotate synchronously, the top rod 11 rotates and gradually rises, until the elastic sheet 3 abuts the glass sheet on the boss 2, the first ratchet wheel 13 remains stationary, and the second ratchet wheel 14 continues to rotate. At this time, the first ratchet wheel 13 collides with the second ratchet wheel 14, and the worker will hear “click, click” sound, at this time, the height of the elastic sheet 3 is adjusted in place, and the abutting force is appropriate, so as to realize the secondary fine adjustment of the abutting height of the elastic sheet 3.
[0049] The above are all preferred embodiments of the present application, and do not limit the protection scope of the present application, so that: all equivalent changes made according to the structure, shape, principle of the present application should be covered within the protection scope of the present application.
Claims
1. An X-ray diffractometer sample stage holder comprising a boss (2) arranged on an inner side wall of a body (1), characterised in that: The elastic sheet (3) is arranged in the machine body (1) below the position opposite to the boss (2), one end of the elastic sheet (3) is used to tightly press the glass sheet against the lower surface of the boss (2), and the other end is arranged on the inner side wall of the machine body (1).
2. The X-ray diffractometer sample stage clamp of claim 1, wherein: The elastic sheet (3) is bonded with an elastic layer at the position used to tightly press the glass sheet.
3. The X-ray diffractometer sample stage clamp of claim 1, wherein: The elastic sheet (3) is bonded with a pull rope (5) at one end opposite to the glass sheet, and the bottom end of the pull rope (5) is bonded with a pull head (6).
4. The X-ray diffractometer sample stage clamp of claim 3, wherein: The pull rope (5) is an elastic rope.
5. The X-ray diffractometer sample stage clamp of claim 1, wherein: A vertical slide rail strip (7) is arranged on the inner side wall of the machine body (1), a lifting block (8) is slid on the slide rail strip (7), the cross sections of the slide rail strip (7) and the lifting block (8) at the sliding fit position are dovetail-shaped, the elastic sheet (3) is bolted on the lifting block (8), and the lifting block (8) is threadedly connected with a fastening bolt (9) used to tightly press the slide rail strip (7).
6. The X-ray diffractometer sample stage clamp of claim 5, wherein: The lifting block (8) and the slide rail strip (7) are coated with polytetrafluoroethylene.
7. The X-ray diffractometer sample stage clamp of claim 5, wherein: A fixed block (10) is arranged on the inner wall of the machine body (1) below the position opposite to the lifting block (8), a vertical jack rod (11) is threadedly connected on the fixed block (10), the top end of the jack rod (11) is supported on the bottom of the lifting block, the bottom end of the jack rod (11) is rotatably sleeved with an internally hollow fine adjustment knob (12), the bottom end of the jack rod (11) is arranged with a first ratchet wheel (13), the inner end face of the fine adjustment knob (12) away from the lifting block (8) is connected with a second ratchet wheel (14) through a compression spring (15), and the first ratchet wheel (13) is engaged with the second ratchet wheel (14).
8. The X-ray diffractometer sample stage clamp of claim 7, wherein: Anti-skid lines (16) are arranged on the outer side wall of the fine adjustment knob (12).