Apparatus and method for dynamically adjusting the ratio of main elements in a multi-component precursor preparation process

By dynamically adjusting the multi-component precursor preparation device and utilizing a closed-loop control system of a variable frequency centrifugal pump and a potentiometric titrator, the problems of uneven mixing and detection lag in the metal salts in the lithium battery cathode material precursor were solved, achieving uniform mixing and precise adjustment of the metal salt solution, making it suitable for industrial production.

CN122399701APending Publication Date: 2026-07-17NANTONG JINTONG ENERGY STORAGE POWER NEW MATERIAL CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
NANTONG JINTONG ENERGY STORAGE POWER NEW MATERIAL CO LTD
Filing Date
2026-03-20
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing technologies for preparing lithium-ion battery cathode material precursors suffer from problems such as uneven mixing of metal salts, sampling contamination, and lag in detection and fine-tuning, leading to deviations in the proportion of main elements and making them unsuitable for industrial continuous production.

Method used

A dynamic adjustment multi-component precursor preparation device is adopted, which forms an in-tank circulation mixing through a variable frequency centrifugal pump. Combined with online detection by a potentiometric titrator and automatic sampling by a precision flow meter, a closed-loop control system is constructed to achieve uniform mixing and precise adjustment of the metal salt solution.

Benefits of technology

It achieves uniform mixing of molten metal and accurate detection results, reduces ratio deviation and material scrap, is suitable for the preparation of multi-component precursors, meets the needs of industrial production, and reduces production costs.

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Abstract

本发明涉及锂离子电池正极材料制备领域,公开了动态调节多元前驱体制备过程中主元素比例的装置及方法,适配二元、三元、四元锂电前驱体制备。装置含金属液储罐、变频离心泵、电位滴定仪、多组金属盐补液系统,离心泵实现金属液罐内循环混合,电位滴定仪经精密流量计在线采样,与补液系统电性连接形成反馈。方法为关闭阀门使金属液循环1~2h,在线采样检测,达标则供液制备前驱体,偏差则由补液系统定量微调,复检至达标。本发明解决了传统工艺混合不均、人工取样污染、调节滞后的问题,将主元素摩尔比偏差控制在±0.1内,全程自动化,装置为常规组件模块化设计,改造成本低,适配工业化连续生产。
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