Synthesis and application of imidazole derivative monomer for lithium surface coating

By substituting groups into 1-phenyl-3-vinylimidazole, imidazole derivative monomers were prepared and polymer protective films were formed, solving the problems of lithium dendrite growth and easy breakage of SEI films, and realizing the high efficiency and cycle stability of lithium metal batteries and the feasibility of industrial production.

CN122404231APending Publication Date: 2026-07-17CHONGQING UNIV
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2026-02-03
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

In the existing technology, the substitution modification of 1-phenyl-3-vinylimidazolium is mainly concentrated in the fields of electroluminescence and ionic liquids. The synthesis methods have harsh reaction conditions, low product yield and poor purity, which cannot meet the application requirements of lithium metal batteries. In addition, lithium dendrite growth and SEI film rupture lead to poor battery cycle stability.

Method used

By substituting specific groups into 1-phenyl-3-vinylimidazole, a monomer containing polymerizable double bonds was prepared. The reaction was carried out in two steps, N-arylation and N-vinylation, under nitrogen protection. The molar ratio of reactants and the type of catalyst were optimized to form a polymer protective film (PBM film) to improve the compatibility of lithium metal interface.

Benefits of technology

The prepared imidazole derivative monomers have strong adhesion to the lithium metal surface, and the polymer film has good ionic conductivity and mechanical strength, effectively inhibiting lithium dendrite growth and improving battery cycle stability. The synthesis method is mild, with high yield and high purity, making it suitable for industrial production.

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Abstract

锂表面涂覆用咪唑衍生物单体的合成及应用。合成方法包括:将取代咪唑、溴苯、贵金属催化剂、碱剂加入极性非质子溶剂中,在保护气氛下加热进行N‑芳基化反应得到取代型N‑苯基咪唑中间体;将所得取代型N‑苯基咪唑中间体、卤代乙烯、相转移催化剂加入有机溶剂中,在碱性条件及保护气氛下加热进行N‑乙烯基化反应得到所述锂表面涂覆用咪唑衍生物单体。本发明通过对1‑苯基‑3‑乙烯基咪唑进行特定基团取代,制备得到含可聚合双键的咪唑衍生物单体,该单体可通过自由基聚合形成聚合物,将其涂覆在锂金属表面可制备得到PBM膜。所得PBM膜能有效改善锂金属界面相容性,抑制锂枝晶生长,提升锂金属电池的循环稳定性。
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